AR011635A1 - Procedimiento para la generacion de hexametilendiamina a partir de mezclas que contienen hexametilendiamina - Google Patents
Procedimiento para la generacion de hexametilendiamina a partir de mezclas que contienen hexametilendiaminaInfo
- Publication number
- AR011635A1 AR011635A1 ARP980100509A ARP980100509A AR011635A1 AR 011635 A1 AR011635 A1 AR 011635A1 AR P980100509 A ARP980100509 A AR P980100509A AR P980100509 A ARP980100509 A AR P980100509A AR 011635 A1 AR011635 A1 AR 011635A1
- Authority
- AR
- Argentina
- Prior art keywords
- mixture
- hexametilendiamina
- procedure
- generation
- distillation
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
- C07C209/84—Purification
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/20—Power plant
Abstract
Procedimiento para la generacion de hexametilendiamina (I) a partir de una mezcla (II) que contiene: (I) hexametilendiamina; (III) hexametilenimina(IV)un compuesto seleccionado del grupo que comprende 2-aminometil-ciclopentil amina y 1,2-diaminociclohexano; (V) una imina; (VI) adipodinitrilo y nitrilo deácido 6-aminocapronico, en cuyo procedimiento (a)se somete una mezcla (II) a una destilacion, obteniéndose (a1) una fraccion de bajo punto de ebullicion quecontiene substancialmente (III); (a2) una fraccion de punto de ebullicion mediano (VII) que contiene (I), (IV), (V) y (a3) una fraccion de alto puntode ebullicion que contiene (V) y (VI); (b) se somete una mezcla (VII) a una destilacion, obteniéndose (b1) un productode cabezas que contiene,substancialmente (IV) y (b2) una mezcla (VIII) que contiene (I) y (V) como producto de fondo, y (c) se somete una mezcla (VIII) a una destilacion,obteniéndose (c1)(I) como cabezas y (c2) un producto de fondo que contienela parte sustancial de (V).
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19704612A DE19704612A1 (de) | 1997-02-07 | 1997-02-07 | Verfahren zur Gewinnung von Hexamethylendiamin aus Hexamethylendiamin enthaltenden Mischungen |
Publications (1)
Publication Number | Publication Date |
---|---|
AR011635A1 true AR011635A1 (es) | 2000-08-30 |
Family
ID=7819564
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP980100509A AR011635A1 (es) | 1997-02-07 | 1998-02-05 | Procedimiento para la generacion de hexametilendiamina a partir de mezclas que contienen hexametilendiamina |
Country Status (15)
Country | Link |
---|---|
US (1) | US6139693A (es) |
EP (1) | EP0961767B1 (es) |
JP (1) | JP2001511166A (es) |
KR (1) | KR100527321B1 (es) |
CN (1) | CN1227216C (es) |
AR (1) | AR011635A1 (es) |
AU (1) | AU6618098A (es) |
BR (2) | BR9807166A (es) |
CA (1) | CA2280889C (es) |
DE (2) | DE19704612A1 (es) |
ES (1) | ES2175682T3 (es) |
ID (1) | ID23371A (es) |
MY (1) | MY127867A (es) |
TW (1) | TW512139B (es) |
WO (1) | WO1998034903A1 (es) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AU4456397A (en) * | 1996-09-10 | 1998-04-02 | Basf Aktiengesellschaft | Process for the separation of 2-aminomethylcylopentylamine from a mixture containing hexamethyldiamine and 2-aminomethylcyclopentylamine |
DE19839338A1 (de) * | 1998-08-28 | 2000-03-02 | Basf Ag | Verbessertes Verfahren zur gleizeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
DE10029187A1 (de) * | 2000-06-19 | 2001-12-20 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronitril aus Gemischen, die 6-Aminocapronitril, Adipodinitril und Hexamethylendiamin enthalten |
US20050000790A1 (en) * | 2001-11-16 | 2005-01-06 | Karl Beck | Method for isolating amines from aqueous solutions |
US6599398B1 (en) * | 2002-07-17 | 2003-07-29 | E. I. Du Pont De Nemours And Company | Recovery of adiponitrile from a mixture of adiponitrile, aminocapronitrile and hexamethylenediamine |
US6887352B2 (en) * | 2003-03-07 | 2005-05-03 | Invista North America S.A.R.L. | Distillative method for separating hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
FR2857965B1 (fr) * | 2003-07-25 | 2005-08-26 | Rhodia Polyamide Intermediates | Procede de fabrication et de separation de composes dinitriles |
US7468119B2 (en) * | 2004-09-10 | 2008-12-23 | Invista North America S.A.R.L. | Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
US7208632B2 (en) * | 2004-09-10 | 2007-04-24 | Invista North America S.A R.L. | Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
FR2902425B1 (fr) * | 2006-06-20 | 2008-07-18 | Rhodia Recherches & Tech | Procede de fabrication de diamines primaires |
FR2922207B1 (fr) * | 2007-10-11 | 2009-12-04 | Rhodia Operations | Procede de purification d'hexamethylene diamine |
JP5767220B2 (ja) | 2009-07-31 | 2015-08-19 | ダウ グローバル テクノロジーズ エルエルシー | 1つ又はそれ以上の脂肪族ジアミンを還元的アミノ化反応溶媒及び不純物から分離する方法 |
US20210002205A1 (en) * | 2018-02-27 | 2021-01-07 | Basf Se | Process for the separation of alkanolamine from a mixture comprising an aliphatic primary diamine |
Family Cites Families (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2208598A (en) * | 1938-09-24 | 1940-07-23 | Du Pont | Aliphatic amino-nitriles and process of producing them |
DE848654C (de) * | 1950-08-19 | 1952-09-08 | Basf Ag | Verfahren zur Herstellung von partiellen Hydrierungsprodukten des Adipinsaeuredinitrils |
GB731819A (en) * | 1951-04-11 | 1955-06-15 | Du Pont | Improvements in or relating to the production of hexamethylene diamine and salts thereof |
DE954416C (de) * | 1952-11-04 | 1956-12-20 | Basf Ag | Verfahren zur Herstellung von Aminonitrilen und Diaminen |
US2762835A (en) * | 1953-03-12 | 1956-09-11 | Celanese Corp | Preparation of amino nitriles |
DE1204681B (de) * | 1959-04-15 | 1965-11-11 | Monsanto Co | Verfahren zur Entfernung geringer Mengen ungesaettigter Verbindungen aus raffiniertem Hexamethylendiamin |
US3775258A (en) * | 1972-04-27 | 1973-11-27 | Du Pont Canada | Purification of adiponitrile |
US4282381A (en) * | 1980-08-21 | 1981-08-04 | E. I. Du Pont De Nemours And Company | Process for purifying hexamethylenediamine |
US4389348A (en) * | 1981-10-26 | 1983-06-21 | Allied Corporation | Selective hydrogenation of dinitrile to omega-aminonitrile and supported rhodium-containing catalyst therefor |
DE3300341A1 (de) * | 1983-01-07 | 1984-07-12 | Chemische Werke Hüls AG, 4370 Marl | Aliphatische ether des cyclododecen-2-ols, verfahren zu ihrer herstellung sowie ihre verwendung zur herstellung von riechstoffkompositionen |
US4601859A (en) * | 1984-05-04 | 1986-07-22 | Allied Corporation | Selective hydrogenation of aliphatic dinitriles to omega-aminonitriles in ammonia with supported, finely dispersed rhodium-containing catalyst |
US4803304A (en) * | 1987-04-15 | 1989-02-07 | E. I. Du Pont De Nemours And Company | Recovery of bis(hexamethylene)triamine |
US5133838A (en) * | 1991-02-28 | 1992-07-28 | E. I. Du Pont De Nemours And Company | Purification of 6-aminocapronitrile |
US5151543A (en) * | 1991-05-31 | 1992-09-29 | E. I. Du Pont De Nemours And Company | Selective low pressure hydrogenation of a dinitrile to an aminonitrile |
WO1993001207A1 (en) * | 1991-07-12 | 1993-01-21 | Gist-Brocades N.V. | Process for the purification of serum albumin |
DE4235466A1 (de) * | 1992-10-21 | 1994-04-28 | Bayer Ag | Verfahren zur Herstellung von (cyclo)aliphatischen Aminonitrilen |
DE4446893A1 (de) * | 1994-12-27 | 1996-07-04 | Basf Ag | Verfahren zur Herstellung von aliphatischen alpha,omega-Aminonitrilen |
DE19500222A1 (de) * | 1995-01-05 | 1996-07-11 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin |
DE19548289A1 (de) * | 1995-12-22 | 1997-06-26 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin |
US5961788A (en) * | 1998-10-09 | 1999-10-05 | E. I. Du Pont De Nemours And Company | Sequential distillation process for removing tetrahydroazepine from aminocapronitrile and/or hexamethylenediamine |
-
1997
- 1997-02-07 DE DE19704612A patent/DE19704612A1/de not_active Withdrawn
-
1998
- 1998-01-30 KR KR10-1999-7007156A patent/KR100527321B1/ko not_active IP Right Cessation
- 1998-01-30 US US09/367,070 patent/US6139693A/en not_active Expired - Lifetime
- 1998-01-30 BR BR9807166-1A patent/BR9807166A/pt not_active IP Right Cessation
- 1998-01-30 JP JP53372798A patent/JP2001511166A/ja not_active Withdrawn
- 1998-01-30 ES ES98908025T patent/ES2175682T3/es not_active Expired - Lifetime
- 1998-01-30 CN CNB988038749A patent/CN1227216C/zh not_active Expired - Fee Related
- 1998-01-30 AU AU66180/98A patent/AU6618098A/en not_active Abandoned
- 1998-01-30 DE DE59803738T patent/DE59803738D1/de not_active Expired - Lifetime
- 1998-01-30 ID IDW990846A patent/ID23371A/id unknown
- 1998-01-30 EP EP98908025A patent/EP0961767B1/de not_active Expired - Lifetime
- 1998-01-30 CA CA002280889A patent/CA2280889C/en not_active Expired - Fee Related
- 1998-01-30 BR BRPI9807196-3A patent/BR9807196B1/pt not_active IP Right Cessation
- 1998-01-30 WO PCT/EP1998/000506 patent/WO1998034903A1/de active IP Right Grant
- 1998-02-05 AR ARP980100509A patent/AR011635A1/es unknown
- 1998-02-06 MY MYPI98000479A patent/MY127867A/en unknown
- 1998-02-07 TW TW087101638A patent/TW512139B/zh not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
KR100527321B1 (ko) | 2005-11-09 |
ES2175682T3 (es) | 2002-11-16 |
MY127867A (en) | 2006-12-29 |
AU6618098A (en) | 1998-08-26 |
DE19704612A1 (de) | 1998-08-13 |
CN1227216C (zh) | 2005-11-16 |
BR9807196A (pt) | 2000-05-23 |
CA2280889C (en) | 2005-07-19 |
BR9807166A (pt) | 2000-01-25 |
US6139693A (en) | 2000-10-31 |
WO1998034903A1 (de) | 1998-08-13 |
CN1251568A (zh) | 2000-04-26 |
EP0961767B1 (de) | 2002-04-10 |
CA2280889A1 (en) | 1998-08-13 |
ID23371A (id) | 2000-04-20 |
EP0961767A1 (de) | 1999-12-08 |
DE59803738D1 (de) | 2002-05-16 |
JP2001511166A (ja) | 2001-08-07 |
TW512139B (en) | 2002-12-01 |
BR9807196B1 (pt) | 2009-01-13 |
KR20000070891A (ko) | 2000-11-25 |
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Legal Events
Date | Code | Title | Description |
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FB | Suspension of granting procedure |