ES2158645T3 - Procedimiento para la preparacion de 1,4-butanodiol, butirolactona y tetrahidrofurano. - Google Patents

Procedimiento para la preparacion de 1,4-butanodiol, butirolactona y tetrahidrofurano.

Info

Publication number
ES2158645T3
ES2158645T3 ES98302163T ES98302163T ES2158645T3 ES 2158645 T3 ES2158645 T3 ES 2158645T3 ES 98302163 T ES98302163 T ES 98302163T ES 98302163 T ES98302163 T ES 98302163T ES 2158645 T3 ES2158645 T3 ES 2158645T3
Authority
ES
Spain
Prior art keywords
point
organic solvent
elevated
derivative
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES98302163T
Other languages
English (en)
Inventor
Michael William Marshall Tuck
Philip Henry Donald Eastland
Andrew George Hiles
Graham Reed
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2158645T3 publication Critical patent/ES2158645T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/17—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds
    • C07C29/172—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds with the obtention of a fully saturated alcohol
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
    • C07C29/149—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/04—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
    • C07D307/06—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms
    • C07D307/08—Preparation of tetrahydrofuran

Abstract

LA INVENCION SE REFIERE A UN PROCEDIMIENTO PARA LA PRODUCCION DE AL MENOS UN BUTANO - 1,4 - DIOL, GA - BUTIROLACTONA Y TETRAHIDROFURANO, MEDIANTE HIDROGENACION EN FASE DE VAPOR DE UN DERIVADO DE ACIDO DICARBOXILICO C 4 SELECCIONADO A PARTIR DE ANHIDRIDO MALEICO Y ESTERES DE DI - (ALQUILO C 1 C 4 ) DE UN ACIDO DICARBOXILICO C 1 - C 4 . EN DICHO PROCESO, UNA CORRIENTE EN FASE DE VAPOR QUE CONTIENE VAPOR DE ANHIDRIDO MALEICO, VAPOR DE AGUA Y OXIDOS DE CARBONO, SE PONE EN CONTACTO EN UNA ZONA DE ABSORCION CON UN PRIMER DISOLVENTE ORGANICO DE ELEVADO PUNTO DE EBULLICION, QUE TIENE UN PUNTO DE EBULLICION A PRESION ATMOSFERICA QUE ES AL MENOS APROX. 30 C SUPERIOR AL DEL ANHIDRIDO MALEICO. A PARTIR DE LA ZONA DE ABSORCION SE RECUPERA UNA CORRIENTE GASEOSA RESIDUAL QUE CONTIENE UNA CANTIDAD MENOR DE DICHO DISOLVENTE ORGANICO DE ELEVADO PUNTO DE EBULLICION, LA CUAL SE PONE EN CONTACTO EN UNA ZONA DE LAVADO CON UN SEGUNDO DISOLVENTE ORGANICO DE ELEVADO PUNTO DE EBULLICION QUE TIENE UN PUNTO DE EBULLICION A PRESION ATMOSFERICA AL MENOS 30 C SUPERIOR AL DEL PRIMER DISOLVENTE ORGANICO DE ELEVADO PUNTO DE EBULLICION. EL GAS RESIDUAL LAVADO PROCEDENTE DE LA ZONA DE LAVADO SE PURGA. LA SOLUCION RESULTANTE DEL PRIMER DISOLVENTE ORGANICO DE ELEVADO PUNTO DE EBULLICION EN EL SEGUNDO DISOLVENTE ORGANICO DE ELEVADO PUNTO DE EBULLICION SE TRATA PARA RECUPERAR EL PRIMER DISOLVENTE ORGANICO DE ELEVADO PUNTO DE EBULLICION, A FIN DE RECICLARLO A LA ZONA DE ABSORCION, MIENTRAS QUE EL SEGUNDO DISOLVENTE DE ELEVADO PUNTO DE EBULLICION RESULTANTE SE RECICLA A LA ZONA DE LAVADO. EL ANHIDRIDO MALEICO CONTENIDO EN LA SOLUCION PROCEDENTE DE LA ZONA DE ABSORCION SE COVIERTE, SI ES NECESARIO, EN UN ESTER DE DI - (ALQUILO C 1 - C 4 ) DE ACIDO MALEICO O ACIDO FUMARICO. LA SOLUCION DEL DERIVADO DICARBOXILICO C 4 EN EL PRIMER DISOLVENTE DE ELEVADO PUNTO DE EBULLICION SE PONE EN CONTACTO CON UNA CORRIENTE GASEOSA QUE CONTIENE HIDROGENO, PARA EXTRAER ASI DICHO DERIVADO DE ACIDO DICARBOXILICO C 4 DE LA MISMA, Y PARA FORMAR UNA CORRIENTE EN FASE DE VAPOR QUE COMPRENDE HIDROGENO Y DICHO DERIVADO DE ACIDO DICARBOXILICO C 4 , EL CUAL SE CONVIERTE, MEDIANTE HIDROGENACION, EN BUTANO - 1,4 - DIOL, GA - BUTIROLACTONA Y/O TETRAHIDROFURANO.
ES98302163T 1998-03-23 1998-03-23 Procedimiento para la preparacion de 1,4-butanodiol, butirolactona y tetrahidrofurano. Expired - Lifetime ES2158645T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP98302163A EP0962438B1 (en) 1998-03-23 1998-03-23 Process for the preparation of 1,4-butanediol, butyrolactone and tetrahydrofuran.

Publications (1)

Publication Number Publication Date
ES2158645T3 true ES2158645T3 (es) 2001-09-01

Family

ID=8234727

Family Applications (1)

Application Number Title Priority Date Filing Date
ES98302163T Expired - Lifetime ES2158645T3 (es) 1998-03-23 1998-03-23 Procedimiento para la preparacion de 1,4-butanodiol, butirolactona y tetrahidrofurano.

Country Status (17)

Country Link
US (1) US6274743B1 (es)
EP (1) EP0962438B1 (es)
JP (1) JP2002507587A (es)
CN (1) CN1158233C (es)
AR (1) AR015737A1 (es)
AU (1) AU751399B2 (es)
BR (1) BR9908993A (es)
CA (1) CA2325499A1 (es)
DE (1) DE69800886T2 (es)
ES (1) ES2158645T3 (es)
ID (1) ID26243A (es)
MY (1) MY124354A (es)
NO (1) NO20004695D0 (es)
SA (1) SA99200188B1 (es)
TW (1) TW557294B (es)
WO (1) WO1999048852A1 (es)
ZA (1) ZA200002941B (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19818340A1 (de) * 1998-04-23 1999-10-28 Basf Ag Verfahren zur Herstellung von Gemischen aus 1,4-Butandiol, Tetrahydrofuran und gamma-Butyrolacton
MY139259A (en) * 1999-10-12 2009-09-30 Kvaerner Process Tech Ltd Process
TWI266760B (en) * 2000-03-20 2006-11-21 Kvaerner Process Tech Ltd Process for the preparation of propane-1,3-diol
GB0117090D0 (en) 2001-07-12 2001-09-05 Kvaerner Process Tech Ltd Process
KR100495335B1 (ko) * 2002-11-15 2005-06-14 주식회사 엘지화학 스팀의 직접접촉을 이용한 고분자 회수방법
GB0325526D0 (en) 2003-10-31 2003-12-03 Davy Process Techn Ltd Process
GB0325530D0 (en) 2003-10-31 2003-12-03 Davy Process Techn Ltd Process
GB0421928D0 (en) 2004-10-01 2004-11-03 Davy Process Techn Ltd Process
US9186599B2 (en) 2010-09-24 2015-11-17 Basf Se Process for isolating tetrahydrofuran
MY157438A (en) 2010-09-24 2016-06-15 Basf Se Process for the production of tetrahydrofuran
US9040756B2 (en) 2011-11-25 2015-05-26 Conser Spa Process for producing 1,4-butanediol by hydrogenating dialkyl maleate in mixed liquid/vapor phase
WO2022190141A1 (en) 2021-03-12 2022-09-15 Conser S.P.A. Process for the co-production of dialkyl succinate and 1,4-butanediol by hydrogenating dialkyl maleate in two stages.

Family Cites Families (30)

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US2638481A (en) 1950-05-26 1953-05-12 Hercules Powder Co Ltd Maleic acid manufacture
GB727828A (en) 1952-12-09 1955-04-06 Chempatents Inc Recovery of polycarboxylic acid anhydrides
GB763339A (en) 1953-03-23 1956-12-12 Chempatents Inc Improvements in recovery of maleic and phthalic acid anhydrides
FR1089012A (fr) 1953-10-08 1955-03-14 Chempatents Procédé de récupération des anhydrides d'acides polycarboxyliques à partir de mélanges gazeux dilués
BE547079A (es) 1955-04-20
US2893924A (en) 1956-04-17 1959-07-07 Saint Gobain Separation and purification of anhydrides of organic diacids
US3040059A (en) 1959-07-02 1962-06-19 Foster Wheeler Corp Recovery of the anhydrides of polycarboxylic acids
BE792879A (fr) 1971-12-17 1973-03-30 Chevron Res Procede d'isolement de l'anhydride maleique
US3891680A (en) 1972-11-29 1975-06-24 Chevron Res Maleic anhydride recovery using nonaqueous medium
US3850758A (en) 1973-07-02 1974-11-26 Allied Chem Purification of crude maleic anhydride by treatment with dimethylbenzophenone
DE2444824A1 (de) 1974-09-19 1976-04-08 Basf Ag Verfahren zur gewinnung von maleinsaeureanhydrid
US4071540A (en) 1976-07-08 1978-01-31 Chevron Research Company Anhydride separation process
US4118403A (en) 1976-11-18 1978-10-03 Monsanto Company Recovery of maleic anhydride
GB8331793D0 (en) 1983-11-29 1984-01-04 Davy Mckee Ltd Process
BR8507068A (pt) 1984-11-21 1987-07-14 Davy Mckee London Processo para a producao de butano-1,4-diol
GB8514002D0 (en) 1985-06-04 1985-07-10 Davy Mckee Ltd Process
GB8618890D0 (en) 1986-08-01 1986-09-10 Davy Mckee Ltd Process
GB8618888D0 (en) 1986-08-01 1986-09-10 Davy Mckee Ltd Process
WO1988000937A1 (en) * 1986-08-01 1988-02-11 Davy Mckee (London) Limited Process for the co-production of butane-1,4-diol and gamma-butyrolactone
GB8717993D0 (en) 1987-07-29 1987-09-03 Davy Mckee Ltd Process
GB8717992D0 (en) 1987-07-29 1987-09-03 Davy Mckee Ltd Process
US4932104A (en) 1988-09-30 1990-06-12 Adolf Kowal Separable buckle
JP2596604B2 (ja) 1988-12-14 1997-04-02 東燃株式会社 １，４−ブタンジオールおよびテトラヒドロフランの製造方法
DE69027304T2 (de) 1989-01-17 1997-01-23 Davy Process Techn Ltd Kontinuierliches Verfahren zur Herstellung von Carbonsäureestern
GB8917864D0 (en) 1989-08-04 1989-09-20 Davy Mckee London Process
GB8917859D0 (en) 1989-08-04 1989-09-20 Davy Mckee London Process
GB8917862D0 (en) 1989-08-04 1989-09-20 Davy Mckee London Process
US5347021A (en) 1990-04-16 1994-09-13 Isp Investments Inc. Process of vapor phase catalytic hydrogenation of maleic anhydride to gamma-butyrolactone in high conversion and high selectivity using an activated catalyst
ZA973972B (en) * 1996-05-14 1998-03-23 Kvaerner Process Tech Ltd A process for the production of at least one C4 compound selected from butane-1,4-diol, gamma-butyrolactone and tetrahydrofuran.
ZA973971B (en) * 1996-05-15 1998-03-23 Kvaerner Process Tech Ltd A process for the production of at least one C4 compound selected from butane-1,4-diol, gamma-butyrolactone and tetrahydrofuran.

Also Published As

Publication number Publication date
WO1999048852A1 (en) 1999-09-30
AU751399B2 (en) 2002-08-15
BR9908993A (pt) 2000-12-12
TW557294B (en) 2003-10-11
DE69800886T2 (de) 2001-10-11
AR015737A1 (es) 2001-05-16
SA99200188B1 (ar) 2006-11-20
ID26243A (id) 2000-12-07
AU3156099A (en) 1999-10-18
CN1158233C (zh) 2004-07-21
ZA200002941B (en) 2001-07-25
NO20004695L (no) 2000-09-20
EP0962438A1 (en) 1999-12-08
DE69800886D1 (de) 2001-07-12
CN1294571A (zh) 2001-05-09
MY124354A (en) 2006-06-30
CA2325499A1 (en) 1999-09-30
NO20004695D0 (no) 2000-09-20
JP2002507587A (ja) 2002-03-12
EP0962438B1 (en) 2001-06-06
US6274743B1 (en) 2001-08-14

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