ES2147014T3 - Metodo y aparato para producir dioxido de titanio. - Google Patents
Metodo y aparato para producir dioxido de titanio.Info
- Publication number
- ES2147014T3 ES2147014T3 ES97934143T ES97934143T ES2147014T3 ES 2147014 T3 ES2147014 T3 ES 2147014T3 ES 97934143 T ES97934143 T ES 97934143T ES 97934143 T ES97934143 T ES 97934143T ES 2147014 T3 ES2147014 T3 ES 2147014T3
- Authority
- ES
- Spain
- Prior art keywords
- reactor
- titanium tetrachloride
- introduction
- introduction set
- oxidizing gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 title abstract 4
- 239000004408 titanium dioxide Substances 0.000 title abstract 2
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 abstract 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 4
- 230000001590 oxidative effect Effects 0.000 abstract 4
- 239000001301 oxygen Substances 0.000 abstract 4
- 229910052760 oxygen Inorganic materials 0.000 abstract 4
- 239000007789 gas Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/07—Producing by vapour phase processes, e.g. halide oxidation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
PROCEDIMIENTO Y REACTOR (10) QUE PERMITEN HACER REACCIONAR VAPORES DE TETRACLORURO DE TITANIO CON OXIGENO PARA PRODUCIR DIOXIDO DE TITANIO. DE ACUERDO CON EL PROCEDIMIENTO, SE INTRODUCE OXIGENO EN EL REACTOR POR AL MENOS DOS PUNTOS, UN PRIMER CONJUNTO DE INTRODUCCION (12) DEL GAS OXIDANTE Y UN SEGUNDO CONJUNTO DE INTRODUCCION (26) DEL GAS OXIDANTE. LA TEMPERATURA DEL OXIGENO INTRODUCIDO EN EL REACTOR POR EL SEGUNDO CONJUNTO DE INTRODUCCION (26) DEL GAS OXIDANTE, ES SUPERIOR, INFERIOR O IGUAL A LA DEL OXIGENO INTRODUCIDO POR EL PRIMER CONJUNTO DE INTRODUCCION (12). EL SEGUNDO CONJUNTO DE INTRODUCCION (26) DEL GAS OXIDANTE PUEDE ESTAR SITUADO ANTES O DESPUES DE LA INTRODUCCION DE LA TOTALIDAD DEL TETRACLORURO DE TITANIO EN EL REACTOR (10). SE INTRODUCE EL TETRACLORURO DE TITANIO EN EL REACTOR (10) A UNA TEMPERATURA RELATIVAMENTE BAJA, INFERIOR A 427 C APROXIMADAMENTE, POR MEDIO DE UN PRIMER CONJUNTO DE INTRODUCCION (20) DE TETRACLORURO DE TITANIO. LA TEMPERATURA DE REACCION EN EL REACTOR ES DE AL MENOS 700 C APROXIMADAMENTE. EVENTUALMENTE PUEDE INTRODUCIRSE UNA SEGUNDA CANTIDAD DE TETRACLORURO DE TITANIO EN EL REACTOR (10) POR MEDIO DE UN SEGUNDO CONJUNTO DE INTRODUCCION (34) DE TETRACLORURO DE TITANIO.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/687,280 US5840112A (en) | 1996-07-25 | 1996-07-25 | Method and apparatus for producing titanium dioxide |
| US08/887,649 US6207131B1 (en) | 1996-07-25 | 1997-07-03 | Method and apparatus for producing titanium dioxide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2147014T3 true ES2147014T3 (es) | 2000-08-16 |
Family
ID=27103970
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES97934143T Expired - Lifetime ES2147014T3 (es) | 1996-07-25 | 1997-07-24 | Metodo y aparato para producir dioxido de titanio. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | USRE39068E1 (es) |
| EP (1) | EP0852568B1 (es) |
| JP (1) | JP2000509700A (es) |
| CN (1) | CN1199385A (es) |
| AU (1) | AU716808B2 (es) |
| DE (1) | DE69702236T2 (es) |
| ES (1) | ES2147014T3 (es) |
| MX (1) | MX9802344A (es) |
| PL (1) | PL187022B1 (es) |
| RU (1) | RU2180321C2 (es) |
| TW (1) | TW382619B (es) |
| WO (1) | WO1998004500A1 (es) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2163385C2 (ru) * | 1998-12-21 | 2001-02-20 | Институт геологии Дагестанского научного центра РАН | Способ предсказания силы и места землетрясения |
| JP4095272B2 (ja) * | 2001-09-25 | 2008-06-04 | 株式会社東芝 | 微粒子製造方法および微粒子製造装置 |
| DE10210189B4 (de) * | 2002-03-07 | 2013-09-19 | Kronos International, Inc. | Verfahren zum Beeinflussen der Pigmenteigenschaften von Titandioxid durch Salzzugabe in der Brennkammer |
| US7182931B2 (en) * | 2003-02-25 | 2007-02-27 | Tronox Llc | Process for making titanium dioxide |
| GB2427860B (en) * | 2003-12-31 | 2009-03-25 | Council Scient Ind Res | Synthesis of ultrafine rutile phase titanium dioxide particles at low temperature |
| US7413726B2 (en) | 2004-03-26 | 2008-08-19 | Council Of Scientific And Industrial Research | Synthesis of ultrafine rutile phase titanium dioxide particles |
| DE602005024723D1 (de) * | 2005-09-16 | 2010-12-23 | Tronox Llc | Verfahren zur steuerung der teilchengrösse von nach dem chloridverfahren hergestelltem titandioxid |
| US7476378B2 (en) * | 2005-10-27 | 2009-01-13 | E.I. Dupont Denemours & Company | Process for producing titanium dioxide |
| US20070245924A1 (en) * | 2006-04-20 | 2007-10-25 | Hofmann Michael A | Reduced abrasion of titanium dioxide pigments produced from the chloride process |
| KR100800129B1 (ko) * | 2006-06-28 | 2008-01-31 | 카운슬 오브 사이언티픽 앤드 인더스트리얼 리서치 | 저온에서 극미세 루타일 상 이산화티타늄 입자의 합성 방법 |
| RU2321543C1 (ru) * | 2006-08-17 | 2008-04-10 | Михаил Алексеевич Горовой | Способ синтеза нанодиоксида титана |
| RU2322393C1 (ru) * | 2006-11-20 | 2008-04-20 | ООО "Научно-производственное предприятие ЭЛСТИН-Сельэлектросетьстрой" | Способ получения диоксида титана |
| DE102007048553A1 (de) * | 2006-12-20 | 2008-06-26 | Kronos International, Inc. | Verfahren zur Herstellung von Titandioxid durch Oxidation von Titantetrachlorid |
| DE102007049297A1 (de) | 2007-10-12 | 2009-04-23 | Kronos International, Inc. | Verfahren zur Herstellung von Titandioxid |
| DE102007049296A1 (de) * | 2007-10-12 | 2009-04-16 | Kronos International, Inc. | Mehrstufiges Verfahren zur Herstellung von Titandioxid |
| DE102009009780A1 (de) | 2009-02-20 | 2010-08-26 | Kronos International, Inc. | Mehrstufiges Verfahren zur Herstellung von Titandioxid |
| AU2014212155B2 (en) * | 2013-01-31 | 2017-06-15 | Tronox Llc | Titanium dioxide production, and methods of controlling particle size thereof |
| CN103663553B (zh) * | 2013-12-09 | 2016-06-29 | 云南冶金新立钛业有限公司 | 制备二氧化钛的方法 |
| CN103663550B (zh) * | 2013-12-09 | 2016-07-06 | 云南冶金新立钛业有限公司 | 制备二氧化钛的方法 |
| CN103663549B (zh) * | 2013-12-09 | 2016-02-10 | 云南冶金新立钛业有限公司 | 制备二氧化钛的方法 |
| CN103880075B (zh) * | 2013-12-09 | 2016-02-24 | 云南冶金新立钛业有限公司 | 制备二氧化钛的方法和系统 |
| CN106241870A (zh) * | 2016-09-05 | 2016-12-21 | 攀钢集团攀枝花钢铁研究院有限公司 | 一种用于制备二氧化钛的装置及制备二氧化钛的方法 |
| RU2759314C1 (ru) * | 2021-01-26 | 2021-11-11 | федеральное государственное автономное образовательное учреждение высшего образования «Национальный исследовательский Томский политехнический университет» | Устройство для получения нанокристаллического диоксида титана со структурой анатаза |
| CN114029025A (zh) * | 2021-11-15 | 2022-02-11 | 攀钢集团攀枝花钢铁研究院有限公司 | 一种氯化法钛白氧化反应装置 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2437171A (en) * | 1943-11-10 | 1948-03-02 | Pittsburgh Plate Glass Co | Composite titanium dioxide-metal oxide pigment |
| US3120427A (en) * | 1960-11-01 | 1964-02-04 | Thann Fab Prod Chem | Preparation of titanium dioxide |
| NL134895C (es) * | 1962-01-30 | |||
| FR93459E (fr) * | 1965-08-03 | 1969-04-04 | Prod Chim De Thann & De Mulhou | Procédé et appareillage pour l'oxydation des halogénures métalliques en phase gazeuse et produits en résultant. |
| GB1170924A (en) * | 1965-10-19 | 1969-11-19 | Laporte Titanium Ltd | Improvements in and relating to the Manufacture of Titanium Dioxide. |
| US3512219A (en) * | 1965-10-19 | 1970-05-19 | American Potash & Chem Corp | Injection reactor for titanium dioxide production |
| US3505091A (en) * | 1968-07-29 | 1970-04-07 | Du Pont | Production of titanium dioxide pigments |
| BE792503A (fr) * | 1971-12-10 | 1973-06-08 | Montedison Spa | Procede de preparation d'un bioxyde de titane d'une taille de particules controlee |
| US4053577A (en) * | 1972-02-18 | 1977-10-11 | Tioxide Group Limited | Process for the gaseous phase production of metal oxide particles |
| IN152047B (es) * | 1978-12-04 | 1983-10-01 | Du Pont | |
| DE2948731A1 (de) * | 1979-12-04 | 1981-06-11 | E.I. Du Pont De Nemours And Co., Wilmington, Del. | Verfahren zur oxidation von titantetrachlorid |
| US4803056A (en) * | 1983-07-22 | 1989-02-07 | Kerr-Mcgee Chemical Corporation | System for increasing the capacity of a titanium dioxide producing process |
| US5204083A (en) * | 1988-05-23 | 1993-04-20 | Kerr-Mcgee Chemical Corporation | Process for preparing titanium dioxide |
| GB9216933D0 (en) * | 1992-08-10 | 1992-09-23 | Tioxide Group Services Ltd | Oxidation of titanium tetrachloride |
| US5840112A (en) * | 1996-07-25 | 1998-11-24 | Kerr Mcgee Chemical Corporation | Method and apparatus for producing titanium dioxide |
-
1997
- 1997-07-24 AU AU37269/97A patent/AU716808B2/en not_active Expired
- 1997-07-24 DE DE69702236T patent/DE69702236T2/de not_active Expired - Lifetime
- 1997-07-24 PL PL97325835A patent/PL187022B1/pl not_active IP Right Cessation
- 1997-07-24 WO PCT/US1997/012207 patent/WO1998004500A1/en not_active Ceased
- 1997-07-24 ES ES97934143T patent/ES2147014T3/es not_active Expired - Lifetime
- 1997-07-24 CN CN97191153.3A patent/CN1199385A/zh active Pending
- 1997-07-24 EP EP97934143A patent/EP0852568B1/en not_active Expired - Lifetime
- 1997-07-24 JP JP10508847A patent/JP2000509700A/ja not_active Ceased
- 1997-07-24 RU RU98107846/12A patent/RU2180321C2/ru not_active IP Right Cessation
- 1997-07-25 TW TW086110624A patent/TW382619B/zh not_active IP Right Cessation
-
1998
- 1998-03-25 MX MX9802344A patent/MX9802344A/es unknown
-
2003
- 2003-03-14 US US10/389,636 patent/USRE39068E1/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| PL325835A1 (en) | 1998-08-03 |
| MX9802344A (es) | 1998-11-29 |
| RU2180321C2 (ru) | 2002-03-10 |
| AU3726997A (en) | 1998-02-20 |
| AU716808B2 (en) | 2000-03-09 |
| DE69702236T2 (de) | 2001-02-15 |
| USRE39068E1 (en) | 2006-04-18 |
| CN1199385A (zh) | 1998-11-18 |
| JP2000509700A (ja) | 2000-08-02 |
| TW382619B (en) | 2000-02-21 |
| WO1998004500A1 (en) | 1998-02-05 |
| DE69702236D1 (de) | 2000-07-13 |
| EP0852568A1 (en) | 1998-07-15 |
| EP0852568B1 (en) | 2000-06-07 |
| PL187022B1 (pl) | 2004-04-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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