ES2145371T3 - Procedimiento para la esterificacion de acido (met)acrilico con un alcanol. - Google Patents
Procedimiento para la esterificacion de acido (met)acrilico con un alcanol.Info
- Publication number
- ES2145371T3 ES2145371T3 ES96120074T ES96120074T ES2145371T3 ES 2145371 T3 ES2145371 T3 ES 2145371T3 ES 96120074 T ES96120074 T ES 96120074T ES 96120074 T ES96120074 T ES 96120074T ES 2145371 T3 ES2145371 T3 ES 2145371T3
- Authority
- ES
- Spain
- Prior art keywords
- met
- waste
- esterification
- acid
- acrylic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/62—Use of additives, e.g. for stabilisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
- C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
- C07C69/54—Acrylic acid esters; Methacrylic acid esters
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
EN UN PROCEDIMIENTO PARA LA ESTERIFICACION DE ACIDO (MET)ACRILICO CON UN ALCANOL EN PRESENCIA DE UN CATALIZADOR DE ESTERIFICACION, EN EL QUE SE SEPARAN POR DESTILACION LOS COMPUESTOS DE PARTIDA QUE NO HAN REACCIONADO Y EL ESTER DEL ACIDO (MET)ACRILICO FORMADO, Y EN EL QUE SE FORMA UN RESIDUO QUE CONTIENE OXIESTER, SE SEPARA ESTE RESIDUO, Y, O ESTE RESIDUO SE HACE REACCIONAR DIRECTAMENTE CON ACIDO (MET)ACRILICO OLIGOMERICO Y DESPUES SE DEGRADAN LOS OXIESTERES DEL RESIDUO EN PRESENCIA DE DIFERENTES CATALIZADORES ACIDOS DEL ACIDO (MET)ACRILICO OLIGOMERICO CON LA ACCION DE ELEVADA TEMPERATURA, O LOS OXIESTERES SE SEPARAN PRIMERO DEL RESIDUO POR DESTILACION, SE HACE REACCIONAR EL DESTILADO CON ACIDO (MET)ACRILICO OLIGOMERICO, Y ENTONCES SE DEGRADAN EN PRESENCIA DE DIFERENTES CATALIZADORES DE ACIDO (MET)ACRILICO OLIGOMERICO BAJO LA ACCION DE ELEVADA TEMPERATURA.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19547485A DE19547485A1 (de) | 1995-12-19 | 1995-12-19 | Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2145371T3 true ES2145371T3 (es) | 2000-07-01 |
Family
ID=7780594
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES96120074T Expired - Lifetime ES2145371T3 (es) | 1995-12-19 | 1996-12-13 | Procedimiento para la esterificacion de acido (met)acrilico con un alcanol. |
Country Status (13)
Country | Link |
---|---|
EP (1) | EP0780359B1 (es) |
JP (1) | JP3830595B2 (es) |
KR (1) | KR100460248B1 (es) |
CN (1) | CN1095827C (es) |
BR (1) | BR9703408A (es) |
CA (1) | CA2193408A1 (es) |
CZ (1) | CZ369096A3 (es) |
DE (2) | DE19547485A1 (es) |
DK (1) | DK0780359T3 (es) |
ES (1) | ES2145371T3 (es) |
MX (1) | MX9606243A (es) |
MY (1) | MY118758A (es) |
SG (1) | SG79928A1 (es) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19536191A1 (de) * | 1995-09-28 | 1997-04-03 | Basf Ag | Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol |
DE19536184A1 (de) * | 1995-09-28 | 1997-04-03 | Basf Ag | Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol |
DE19536183A1 (de) * | 1995-09-28 | 1997-04-03 | Basf Ag | Verfahren zur Herstellung von Alkylestern der (Meth)acrylsäure |
SG81213A1 (en) * | 1995-12-15 | 2001-06-19 | Rohm & Haas | Process for producing butyle acrylate |
DE19701737A1 (de) * | 1997-01-20 | 1998-07-23 | Basf Ag | Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol |
US5877345A (en) | 1997-02-07 | 1999-03-02 | Rohm And Haas Company | Process for producing butyl acrylate |
MY120051A (en) | 1997-07-30 | 2005-08-30 | Mitsubishi Rayon Co | Process for purification of (meth)acrylic acid |
DE19814387A1 (de) * | 1998-03-31 | 1999-10-07 | Basf Ag | Verfahren zur Herstellung von Acrylsäure und Acrylsäureestern |
DE19851983A1 (de) * | 1998-11-11 | 2000-05-18 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure |
DE19851984A1 (de) * | 1998-11-11 | 2000-05-18 | Basf Ag | Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol |
DE19922722A1 (de) | 1999-05-18 | 2000-11-23 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
DE10007213A1 (de) * | 2000-02-17 | 2001-08-23 | Basf Ag | Verfahren zur Herstellung von Estern alpha,beta-ungesättigter Carbonsäuren |
DE10127941A1 (de) | 2001-06-08 | 2002-05-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
WO2005007609A1 (de) | 2003-07-11 | 2005-01-27 | Basf Aktiengesellschaft | Thermisches trennverfahren zur abtrennung wenigstens eines (meth)acrylmonomere angereichert enthaltenden stoffstroms |
EP4015498B1 (de) | 2020-12-18 | 2024-04-24 | Basf Se | Verfahren zur kontinuierlichen herstellung von acrylsäure-n-butylester |
CN117299040B (zh) * | 2023-11-30 | 2024-03-12 | 万华化学集团股份有限公司 | 一种同时制备乙酸丁酯和丙烯酸丁酯的装置系统及其方法 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB923595A (en) | 1960-12-03 | 1963-04-18 | Distillers Co Yeast Ltd | Improvements in and relating to the production of acrylic esters |
US3868410A (en) * | 1972-08-03 | 1975-02-25 | Celanese Corp | Conversion of oligomeric acrylates to acrylate monomers |
DE2339529A1 (de) | 1973-08-03 | 1975-02-13 | Ardie Werk Gmbh | Kraftstoffeinspritzpumpenverstellvorrichtung |
JPS5762229A (en) | 1980-10-02 | 1982-04-15 | Mitsubishi Petrochem Co Ltd | Recovery of useful component from heavy substance obtained as by-product in preparation of acrylic ester |
CN1058390A (zh) | 1990-07-13 | 1992-02-05 | 梁效成 | 含烷氧基丙酸酯废液的处理方法 |
JPH0768168B2 (ja) | 1991-07-12 | 1995-07-26 | 東亞合成株式会社 | アクリル酸エステルのミカエル付加物の分解方法 |
CN1026104C (zh) | 1992-03-17 | 1994-10-05 | 侯玉里 | 丙烯酸酯类废油再生工艺 |
JP2943523B2 (ja) | 1992-08-12 | 1999-08-30 | 東亞合成株式会社 | アクリル酸エステルのミカエル付加物から有用化合物を製造する方法 |
-
1995
- 1995-12-19 DE DE19547485A patent/DE19547485A1/de not_active Withdrawn
-
1996
- 1996-12-09 MX MX9606243A patent/MX9606243A/es unknown
- 1996-12-09 MY MYPI96005168A patent/MY118758A/en unknown
- 1996-12-13 ES ES96120074T patent/ES2145371T3/es not_active Expired - Lifetime
- 1996-12-13 EP EP96120074A patent/EP0780359B1/de not_active Expired - Lifetime
- 1996-12-13 DE DE59605038T patent/DE59605038D1/de not_active Expired - Lifetime
- 1996-12-13 DK DK96120074T patent/DK0780359T3/da active
- 1996-12-16 JP JP33583696A patent/JP3830595B2/ja not_active Expired - Lifetime
- 1996-12-16 CZ CZ963690A patent/CZ369096A3/cs unknown
- 1996-12-17 SG SG9611746A patent/SG79928A1/en unknown
- 1996-12-18 CA CA002193408A patent/CA2193408A1/en not_active Abandoned
- 1996-12-18 KR KR1019960067283A patent/KR100460248B1/ko not_active IP Right Cessation
- 1996-12-18 CN CN96121570A patent/CN1095827C/zh not_active Expired - Lifetime
-
1997
- 1997-05-27 BR BR9703408A patent/BR9703408A/pt not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
CZ369096A3 (en) | 1997-07-16 |
CN1158841A (zh) | 1997-09-10 |
MX9606243A (es) | 1998-04-30 |
KR100460248B1 (ko) | 2005-01-15 |
DE19547485A1 (de) | 1996-05-09 |
BR9703408A (pt) | 1999-01-05 |
SG79928A1 (en) | 2001-04-17 |
MY118758A (en) | 2005-01-31 |
JP3830595B2 (ja) | 2006-10-04 |
DE59605038D1 (de) | 2000-05-31 |
CN1095827C (zh) | 2002-12-11 |
JPH09183752A (ja) | 1997-07-15 |
CA2193408A1 (en) | 1997-06-20 |
KR970042477A (en) | 1997-07-24 |
DK0780359T3 (da) | 2000-08-07 |
EP0780359B1 (de) | 2000-04-26 |
EP0780359A1 (de) | 1997-06-25 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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