ES2134785T3 - Procedimiento para la obtencion de lactamas n-substituidas. - Google Patents

Procedimiento para la obtencion de lactamas n-substituidas.

Info

Publication number
ES2134785T3
ES2134785T3 ES92119690T ES92119690T ES2134785T3 ES 2134785 T3 ES2134785 T3 ES 2134785T3 ES 92119690 T ES92119690 T ES 92119690T ES 92119690 T ES92119690 T ES 92119690T ES 2134785 T3 ES2134785 T3 ES 2134785T3
Authority
ES
Spain
Prior art keywords
group
equivalent
procedure
obtaining
xey
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES92119690T
Other languages
English (en)
Inventor
Hans-Jurgen Dr Weyer
Rolf Dr Fischer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2134785T3 publication Critical patent/ES2134785T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
    • C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D207/18—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D207/22—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D207/24—Oxygen or sulfur atoms
    • C07D207/26—2-Pyrrolidones
    • C07D207/263—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms
    • C07D207/267—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to the ring nitrogen atom

Abstract

PROCEDIMIENTO PARA LA OBTENCION DE LACTAMAS N AS, DE LA FORMULA GENERAL I EN LA QUE Z EQUIVALE A UN GRUPO C2 NO O NAFTILENO, Y R1 ES UN GRUPO C1 C6 DE LA TRANSFORMACION HIDRATANTE DE UN COMPUESTO DE FORMULA GENERAL II CON UNA AMINA, EN LA QUE W EQUIVALE A UN GRUPO C2 C10 ALQUILENO, UN GRUPO C2 CUAL LOS GRUPOS X E Y JUNTOS, FORMAN UN PUENTE OXA O IMIDO, DE LAS FORMULAS O ALTERNATIVAMENTE SON IGUALES O DIFERENTES Y EQUIVALEN A UN GRUPO HIDROXILO, UN GRUPO C1 GRUPO C6 EN EL QUE, EN CASO DE QUE X E Y SEAN DIFERENTES, Y ADEMAS DEL SIGNIFICADO DADO ARRIBA, TIENE TAMBIEN EL SIGNIFICADO DE HIDROGENO, A PRESION ELEVADA Y A TEMPERATURA ELEVADA, EN PRESENCIA DE UN CATALIZADOR, EN EL QUE SE USAN AMINAS SECUNDARIAS Y/O TERCIARIAS, DE FORMULA III, EN LA QUE EL RESTO R1 TIENE EL SIGNIFICADO DADO ARRIBA, Y EL INDICE N EQUIVALE A 0 O 1, O MEZCLAS DE ESTAS AMINAS SECUNDARIAS Y/O TERCIARIAS, CON UNA AMINA PRIMARIA, DE FORMULA IV UTILIZADA COMO MATERIAL DE PARTIDA, Y SE LLEVA A CABO LA TRANSFORMACION BAJO ADICION DE AGUA Y/O AMONIACO.
ES92119690T 1991-11-30 1992-11-19 Procedimiento para la obtencion de lactamas n-substituidas. Expired - Lifetime ES2134785T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4139607A DE4139607A1 (de) 1991-11-30 1991-11-30 Verfahren zur herstellung von n-substituierten lactamen

Publications (1)

Publication Number Publication Date
ES2134785T3 true ES2134785T3 (es) 1999-10-16

Family

ID=6446030

Family Applications (1)

Application Number Title Priority Date Filing Date
ES92119690T Expired - Lifetime ES2134785T3 (es) 1991-11-30 1992-11-19 Procedimiento para la obtencion de lactamas n-substituidas.

Country Status (5)

Country Link
US (1) US5276165A (es)
EP (1) EP0545150B1 (es)
JP (1) JP3202364B2 (es)
DE (2) DE4139607A1 (es)
ES (1) ES2134785T3 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5698579A (en) * 1993-07-02 1997-12-16 Celgene Corporation Cyclic amides
MY113899A (en) * 1995-03-01 2002-06-29 Dsm Ip Assets Bv Process for the preparation of (permittivy)-caprolactam and (permittivy)-caprolactam precursors
DE19520258A1 (de) * 1995-06-02 1996-12-05 Bayer Ag Verfahren zur Herstellung von 2-Pyrrolidonen
FR2751963B1 (fr) * 1996-07-31 1998-09-04 Poudres & Explosifs Ste Nale Procede de preparation de lactames n-substitues
US6603021B2 (en) 2001-06-18 2003-08-05 Battelle Memorial Institute Methods of making pyrrolidones
DE10129336A1 (de) * 2001-06-19 2003-01-02 Basf Ag Verfahren zur Herstellung von Pyrrolidonen
US7199250B2 (en) * 2002-12-20 2007-04-03 Battelle Memorial Institute Process for producing cyclic compounds
US6916842B2 (en) * 2003-03-24 2005-07-12 E. I. Du Pont De Nemours And Company Production of 5-methyl-n-(methyl aryl)-2-pyrrolidone, 5-methyl-n-(methyl cycloalkyl)-2-pyrrolidone and 5-methyl-n-alkyl-2-pyrrolidone by reductive amination of levulinic acid esters with cyano compounds
US6743819B1 (en) * 2003-03-24 2004-06-01 E. I. Du Ponte De Nemours And Company Production of 5-methyl-N-aryl-2-pyrrolidone and 5-methyl-N-cycloalkyl-2-pyrrolidone by reductive amination of levulinic acid with aryl amines

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2112970A (en) * 1931-10-01 1938-04-05 Du Pont Synthesis of amines
DE609245C (de) * 1933-03-02 1935-02-11 Commercial Solvents Corp Verfahren zur Herstellung von niederen Methylaminen aus Trimethylamin
DE626923C (de) * 1933-04-20 1936-03-05 I G Farbenindustrie Akt Ges Verfahren zur UEberfuehrung von sekundaeren und tertiaeren Aminen in niedrigere Substitutionsstufen
US2192523A (en) * 1937-03-08 1940-03-05 Sharples Solvents Corp Ammonolysis of secondary and tertiary amines
GB596006A (en) * 1944-07-15 1947-12-24 Du Pont Improvements in and relating to processes for the production of amines and/or imines
US3109005A (en) * 1961-05-15 1963-10-29 Halcon International Inc Process for making 2-pyrrolidone from maleic anhydride
US4014933A (en) * 1969-10-23 1977-03-29 Basf Aktiengesellschaft Production of amines from alcohols
BE757840A (fr) * 1969-10-23 1971-04-22 Basf Ag Procede de preparation d'amines a partir d'alcools
US3726925A (en) * 1970-06-24 1973-04-10 Union Oil Co Preparation of trialkylamines
CA943965A (en) * 1971-01-21 1974-03-19 Sun Research And Development Co. Preparation of cyclic amides
US3884936A (en) * 1971-01-21 1975-05-20 Sun Research Development Preparation of 2-pyrrolidone
DE2321101C2 (de) * 1973-04-26 1982-07-22 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung im wesentlichen trägerfreier Kobaltkatalysatoren
JPS5412314A (en) * 1977-06-24 1979-01-30 Mitsubishi Gas Chem Co Inc Preparation of dimethylformamide
JPS54157519A (en) * 1978-06-01 1979-12-12 Mitsubishi Gas Chem Co Inc Preparation of dimethylformamide
DE3027890A1 (de) * 1980-07-23 1982-03-04 Basf Ag, 6700 Ludwigshafen Hydrierkatalysatoren fuer die herstellung von propandiolen und verfahren zur herstellung von propandiolen mit solchen katalysatoren
US4645837A (en) * 1981-07-31 1987-02-24 Sri International Catalyst system for amine transalkylation
US4550185A (en) * 1983-12-22 1985-10-29 E. I. Du Pont De Nemours And Company Process for making tetrahydrofuran and 1,4-butanediol using Pd/Re hydrogenation catalyst
US4609636A (en) * 1983-12-22 1986-09-02 E. I. Du Pont De Nemours And Company Pd/Re hydrogenation catalyst for making tetrahydrofuran and 1,4-butanediol
US4731454A (en) * 1986-06-09 1988-03-15 Mitsubishi Chemical Industries Limited Process for producing lactams
DE3622759A1 (de) * 1986-07-07 1988-01-28 Huels Chemische Werke Ag Verfahren zur herstellung von c(pfeil abwaerts)1(pfeil abwaerts)- bis c(pfeil abwaerts)6(pfeil abwaerts)-n-alkylpyrrolidonen aus bernsteinsaeureanhydrid bzw. c(pfeil abwaerts)1(pfeil abwaerts)- bis c(pfeil abwaerts)6(pfeil abwaerts)-n-alkylsuccinimid
US4851546A (en) * 1987-10-01 1989-07-25 The Standard Oil Company Preparation of pyrrolidones by catalytic hydrogenation of maleimides
DE3903367A1 (de) * 1989-02-04 1990-08-16 Basf Ag Katalysator und verfahren zur hydrierenden aminierung von alkoholen
DE3904083A1 (de) * 1989-02-11 1990-08-16 Basf Ag Kobaltkatalysatoren
DE4018243A1 (de) * 1990-06-07 1991-12-12 Basf Ag Verfahren zur herstellung von n-substituierten pyrrolidonen

Also Published As

Publication number Publication date
EP0545150A1 (de) 1993-06-09
EP0545150B1 (de) 1999-06-30
US5276165A (en) 1994-01-04
DE4139607A1 (de) 1993-06-03
JPH05221970A (ja) 1993-08-31
DE59209719D1 (de) 1999-08-05
JP3202364B2 (ja) 2001-08-27

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