ES2108968T3 - Metodo para la preparacion continua de una mezcla de cicloalcanona, un cicloalcanol y un hidroperoxido de cicloalquilo. - Google Patents

Metodo para la preparacion continua de una mezcla de cicloalcanona, un cicloalcanol y un hidroperoxido de cicloalquilo.

Info

Publication number
ES2108968T3
ES2108968T3 ES94903137T ES94903137T ES2108968T3 ES 2108968 T3 ES2108968 T3 ES 2108968T3 ES 94903137 T ES94903137 T ES 94903137T ES 94903137 T ES94903137 T ES 94903137T ES 2108968 T3 ES2108968 T3 ES 2108968T3
Authority
ES
Spain
Prior art keywords
mixture
cycloalcanol
cycloalcanone
continuous preparation
cyclloalkyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES94903137T
Other languages
English (en)
Inventor
Johannes Gerardus Hub Housmans
Ubaldus Franciscus Kragten
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Koninklijke DSM NV
Original Assignee
DSM NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DSM NV filed Critical DSM NV
Application granted granted Critical
Publication of ES2108968T3 publication Critical patent/ES2108968T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/48Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups
    • C07C29/50Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups with molecular oxygen only
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00Preparation of peroxy compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C409/00Peroxy compounds
    • C07C409/02Peroxy compounds the —O—O— group being bound between a carbon atom, not further substituted by oxygen atoms, and hydrogen, i.e. hydroperoxides
    • C07C409/14Peroxy compounds the —O—O— group being bound between a carbon atom, not further substituted by oxygen atoms, and hydrogen, i.e. hydroperoxides the carbon atom belonging to a ring other than a six-membered aromatic ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/12Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14The ring being saturated
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/18Systems containing only non-condensed rings with a ring being at least seven-membered
    • C07C2601/20Systems containing only non-condensed rings with a ring being at least seven-membered the ring being twelve-membered

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

METODO PARA LA PREPARACION CONTINUA DE UNA MEZCLA DE UNA CICLOALCANONA, UN CICLOALCANOL Y UN CICLOALKILHIDROPEROXIDO, DE ACUERDO CON LO CUAL EL CICLOALCANO CORRESPONDIENTE SE OXIDA DONDE EL ALCANO CICLICO TIENE ENTRE 5 Y 20 ATOMOS DE CARBONO, EN UN PROCESO CONTINUO CON LA AYUDA DE UN GAS QUE CONTIENE OXIGENO, EN AUSENCIA DE UN CATALIZADOR DE METAL, A UNA TEMPERATURA DE ENTRE 130 A 200 (GRADOS) C, SIENDO LA OXIDACION AL MENOS PARCIALMENTE REALIZADA EN PRESENCIA DE ENTRE 0.002 Y 2 MMOLES DE UN COMPUESTO FENOLICO POR KG DE MEZCLA DE REACCION (MMOL/KG).
ES94903137T 1992-12-16 1993-12-02 Metodo para la preparacion continua de una mezcla de cicloalcanona, un cicloalcanol y un hidroperoxido de cicloalquilo. Expired - Lifetime ES2108968T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
BE9201101A BE1006451A3 (nl) 1992-12-16 1992-12-16 Werkwijze voor de continue bereiding van een mengsel van een cycloalkanon, cycloalkanol en een cycloalkylhydroperoxide.

Publications (1)

Publication Number Publication Date
ES2108968T3 true ES2108968T3 (es) 1998-01-01

Family

ID=3886588

Family Applications (1)

Application Number Title Priority Date Filing Date
ES94903137T Expired - Lifetime ES2108968T3 (es) 1992-12-16 1993-12-02 Metodo para la preparacion continua de una mezcla de cicloalcanona, un cicloalcanol y un hidroperoxido de cicloalquilo.

Country Status (16)

Country Link
US (1) US5406001A (es)
EP (1) EP0674613B1 (es)
JP (1) JPH08504437A (es)
KR (1) KR100299587B1 (es)
CN (1) CN1058478C (es)
AT (1) ATE158271T1 (es)
BE (1) BE1006451A3 (es)
BR (1) BR9307663A (es)
DE (1) DE69314054T2 (es)
ES (1) ES2108968T3 (es)
MX (1) MX9308018A (es)
PL (1) PL174275B1 (es)
RU (1) RU2116290C1 (es)
TW (1) TW277055B (es)
UA (1) UA35602C2 (es)
WO (1) WO1994013613A1 (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3050869B1 (de) * 2015-01-30 2019-10-02 Symrise AG Verfahren zur Herstellung von substituierten Alkylcycloalkanonen
EP3746418A1 (en) * 2018-01-30 2020-12-09 Basf Se Method for oxidation of cycloalkanes
RU2747484C1 (ru) * 2020-10-27 2021-05-05 Публичное акционерное общество "КуйбышевАзот" Способ получения гидропероксида циклогексила

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU197555A1 (ru) * 1965-06-16 1983-09-15 Государственный Научно-Исследовательский Институт Органических Полупродуктов И Красителей Способ получени альдегидов или кетонов
US3949004A (en) * 1971-03-16 1976-04-06 Atlantic Richfield Company Hydroperoxide production
SU686329A1 (ru) * 1977-12-15 1982-05-07 Предприятие П/Я Р-6603 Способ получени гидроперекиси циклододецила Б.Я.Ладыгина
SU799325A1 (ru) * 1978-01-30 1982-05-07 Предприятие П/Я Р-6603 Способ получени гидроперекисей циклоалкилов Б.Я.Ладыгина
US5220075A (en) * 1992-07-17 1993-06-15 Abb Lummus Crest Inc. Initiated peroxidation of secondary carbon in alkanes and cycloalkanes

Also Published As

Publication number Publication date
KR100299587B1 (ko) 2001-11-22
KR950704223A (ko) 1995-11-17
UA35602C2 (uk) 2001-04-16
DE69314054T2 (de) 1998-04-02
PL309345A1 (en) 1995-10-02
TW277055B (es) 1996-06-01
ATE158271T1 (de) 1997-10-15
BE1006451A3 (nl) 1994-08-30
EP0674613B1 (en) 1997-09-17
DE69314054D1 (de) 1997-10-23
BR9307663A (pt) 1999-06-29
JPH08504437A (ja) 1996-05-14
EP0674613A1 (en) 1995-10-04
WO1994013613A1 (en) 1994-06-23
CN1058478C (zh) 2000-11-15
CN1096026A (zh) 1994-12-07
US5406001A (en) 1995-04-11
RU95114380A (ru) 1997-06-10
RU2116290C1 (ru) 1998-07-27
PL174275B1 (pl) 1998-07-31
MX9308018A (es) 1994-08-31

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