ES2074044T3 - Metodo para la fabricacion de hns ii. - Google Patents

Metodo para la fabricacion de hns ii.

Info

Publication number
ES2074044T3
ES2074044T3 ES87202613T ES87202613T ES2074044T3 ES 2074044 T3 ES2074044 T3 ES 2074044T3 ES 87202613 T ES87202613 T ES 87202613T ES 87202613 T ES87202613 T ES 87202613T ES 2074044 T3 ES2074044 T3 ES 2074044T3
Authority
ES
Spain
Prior art keywords
hns
volume density
generally referred
product
raw product
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES87202613T
Other languages
English (en)
Inventor
Anthony Bellamy
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eurenco Bofors AB
Original Assignee
Bofors Explosives AB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bofors Explosives AB filed Critical Bofors Explosives AB
Application granted granted Critical
Publication of ES2074044T3 publication Critical patent/ES2074044T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/16—Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)
  • Pyrrole Compounds (AREA)
  • Detergent Compositions (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

LA INVENCION SE REFIERE A UN METODO PARA LA PRODUCCION DE UN 2,2'',4,4'',6,6''-HEXANITROESTILBENO (HNS) CON DENSIDAD DE VOLUMEN Y PUREZA ESPECIFICADAS, GENERALMENTE REFERIDO COMO UN HNS II, A PARTIR DE UN PRODUCTO CRUDO MENOS PURO CON DENSIDAD DE VOLUMEN MENOR, GENERALMENTE REFERIDO COMO HNS I. DE ACUERDO CON LA INVENCION, EL PRODUCTO CRUDO SE PURIFICA A TRAVES DE UNA RECRISTALIZACION DESDE UN DISOLVENTE, SIENDO LA N-METILPIRROLIDINA LA QUE DA EL MEJOR RESULTADO, MIENTRAS QUE LA DENSIDAD DE VOLUMEN DEL PRODUCTO SE INCREMENTA POR TRATAMIENTO ULTRASONICO DE LOS CRISTALES RESULTANTES, DISMINUYENDO ASI SU LONGITUD
ES87202613T 1987-01-21 1987-12-23 Metodo para la fabricacion de hns ii. Expired - Lifetime ES2074044T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE8700212A SE468434B (sv) 1987-01-21 1987-01-21 Foerfarande foer rening av hns (2,2',4,4',6,6'- hexanitrostilben) och framstaellning av hnsii

Publications (1)

Publication Number Publication Date
ES2074044T3 true ES2074044T3 (es) 1995-09-01

Family

ID=20367229

Family Applications (2)

Application Number Title Priority Date Filing Date
ES87202613T Expired - Lifetime ES2074044T3 (es) 1987-01-21 1987-12-23 Metodo para la fabricacion de hns ii.
ES8800119A Expired ES2007786A6 (es) 1987-01-21 1988-01-20 Metodo para la fabricacion de 2,2', 4,4', 6,6'-hexanitrostilbeno (hns).

Family Applications After (1)

Application Number Title Priority Date Filing Date
ES8800119A Expired ES2007786A6 (es) 1987-01-21 1988-01-20 Metodo para la fabricacion de 2,2', 4,4', 6,6'-hexanitrostilbeno (hns).

Country Status (15)

Country Link
EP (1) EP0277386B1 (es)
JP (1) JP2569345B2 (es)
AR (1) AR244198A1 (es)
AT (1) ATE123757T1 (es)
AU (1) AU611125B2 (es)
BR (1) BR8800160A (es)
CA (1) CA1339470C (es)
DE (1) DE3751347T2 (es)
ES (2) ES2074044T3 (es)
IL (1) IL85103A (es)
IN (1) IN172139B (es)
NO (1) NO169770C (es)
SE (1) SE468434B (es)
YU (1) YU46247B (es)
ZA (1) ZA88150B (es)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100496336B1 (ko) * 2002-06-25 2005-06-20 주식회사 한화 직접 접촉 냉각 결정화법을 이용한 헥사나이트로스틸벤의재결정화 방법
US6844473B1 (en) * 2004-02-18 2005-01-18 Bwxt Pantex, L.L.C. Continuous aspiration process for manufacture of ultra-fine particle HNS
GB0918431D0 (en) 2009-10-21 2009-12-09 Prosonix Ltd Process for improving crystallinity
KR20150040282A (ko) * 2012-08-10 2015-04-14 주식회사 다이셀 불포화 카르복실산아미드 화합물을 포함하는 결정 및 그의 제조 방법
CN103172476A (zh) * 2013-04-08 2013-06-26 中国工程物理研究院化工材料研究所 一种亚微米颗粒1-氧-二氨基-3，5-二硝基吡嗪炸药的制备方法
KR102615219B1 (ko) * 2020-11-09 2023-12-19 한국과학기술원 고순도 헥사나이트로스틸벤의 제조방법
CN116514664A (zh) * 2023-03-30 2023-08-01 中北大学 一种六硝基茋纯化工艺

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3505413A (en) * 1964-05-05 1970-04-07 Us Navy Hexanitrostilbene
US3510266A (en) * 1967-03-29 1970-05-05 Merck & Co Inc Production of crystals in a fluidized bed with ultrasonic vibrations
US3699176A (en) * 1970-10-02 1972-10-17 Del Mar Eng Lab Process for recrystallizing hexanitrostilbene
US4245129A (en) * 1979-08-14 1981-01-13 The United States Of America As Represented By The Secretary Of The Army Process for preparing hexanitrobibenzyl
US4268696A (en) * 1980-01-14 1981-05-19 The United States Of America As Represented By The Secretary Of The Army Method for preparing hexanitrostilbene
US4604489A (en) * 1984-04-20 1986-08-05 The United States Of America As Represented By The Secretary Of The Navy Recrystallization of hexanitrostilbene from dimethylsulfoxide and methanol

Also Published As

Publication number Publication date
SE8700212D0 (sv) 1987-01-21
ES2007786A6 (es) 1989-07-01
DE3751347D1 (de) 1995-07-20
AU1062088A (en) 1988-08-04
IN172139B (es) 1993-04-17
NO880233L (no) 1988-07-22
JPS63301846A (ja) 1988-12-08
JP2569345B2 (ja) 1997-01-08
YU46247B (sh) 1993-05-28
NO169770B (no) 1992-04-27
ATE123757T1 (de) 1995-06-15
CA1339470C (en) 1997-09-23
EP0277386A3 (en) 1990-08-16
NO880233D0 (no) 1988-01-20
IL85103A0 (en) 1988-06-30
EP0277386B1 (en) 1995-06-14
AR244198A1 (es) 1993-10-29
YU9388A (en) 1989-10-31
EP0277386A2 (en) 1988-08-10
ZA88150B (en) 1988-06-28
DE3751347T2 (de) 1996-01-25
IL85103A (en) 1992-12-01
BR8800160A (pt) 1988-08-30
SE8700212L (sv) 1988-07-22
SE468434B (sv) 1993-01-18
NO169770C (no) 1992-08-05
AU611125B2 (en) 1991-06-06

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