YU46247B - Postupak za dobijanje 2,2',4,4',6,6'-heksanitrostilbena specifične čistoće i nasipne mase - Google Patents

Postupak za dobijanje 2,2',4,4',6,6'-heksanitrostilbena specifične čistoće i nasipne mase

Info

Publication number
YU46247B
YU46247B YU9388A YU9388A YU46247B YU 46247 B YU46247 B YU 46247B YU 9388 A YU9388 A YU 9388A YU 9388 A YU9388 A YU 9388A YU 46247 B YU46247 B YU 46247B
Authority
YU
Yugoslavia
Prior art keywords
hexanitrostilbene
obtaining
bulk mass
specific purity
purity
Prior art date
Application number
YU9388A
Other languages
English (en)
Other versions
YU9388A (en
Inventor
A. Bellamy
Original Assignee
Nobel Kemi Ab.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nobel Kemi Ab. filed Critical Nobel Kemi Ab.
Publication of YU9388A publication Critical patent/YU9388A/xx
Publication of YU46247B publication Critical patent/YU46247B/sh

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • C07C201/16Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Pyrrole Compounds (AREA)
  • Saccharide Compounds (AREA)

Abstract

iz nečistijeg sirovog proizvoda, opšte poznatog kao HNS I, naznačen time, što se gornji sirovi proizvod rekristališe iz N-metilpirolidona (1-metil-2-pirolidona). -Prijava sadrži još 13 zavisnih zahteva.
YU9388A 1987-01-21 1988-01-20 Postupak za dobijanje 2,2',4,4',6,6'-heksanitrostilbena specifične čistoće i nasipne mase YU46247B (sh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE8700212A SE468434B (sv) 1987-01-21 1987-01-21 Foerfarande foer rening av hns (2,2',4,4',6,6'- hexanitrostilben) och framstaellning av hnsii

Publications (2)

Publication Number Publication Date
YU9388A YU9388A (en) 1989-10-31
YU46247B true YU46247B (sh) 1993-05-28

Family

ID=20367229

Family Applications (1)

Application Number Title Priority Date Filing Date
YU9388A YU46247B (sh) 1987-01-21 1988-01-20 Postupak za dobijanje 2,2',4,4',6,6'-heksanitrostilbena specifične čistoće i nasipne mase

Country Status (15)

Country Link
EP (1) EP0277386B1 (sh)
JP (1) JP2569345B2 (sh)
AR (1) AR244198A1 (sh)
AT (1) ATE123757T1 (sh)
AU (1) AU611125B2 (sh)
BR (1) BR8800160A (sh)
CA (1) CA1339470C (sh)
DE (1) DE3751347T2 (sh)
ES (2) ES2074044T3 (sh)
IL (1) IL85103A (sh)
IN (1) IN172139B (sh)
NO (1) NO169770C (sh)
SE (1) SE468434B (sh)
YU (1) YU46247B (sh)
ZA (1) ZA88150B (sh)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100496336B1 (ko) * 2002-06-25 2005-06-20 주식회사 한화 직접 접촉 냉각 결정화법을 이용한 헥사나이트로스틸벤의재결정화 방법
US6844473B1 (en) * 2004-02-18 2005-01-18 Bwxt Pantex, L.L.C. Continuous aspiration process for manufacture of ultra-fine particle HNS
GB0918431D0 (en) 2009-10-21 2009-12-09 Prosonix Ltd Process for improving crystallinity
JP6231479B2 (ja) * 2012-08-10 2017-11-15 株式会社ダイセル 不飽和カルボン酸アミド化合物を含む結晶、及びその製造方法
CN103172476A (zh) * 2013-04-08 2013-06-26 中国工程物理研究院化工材料研究所 一种亚微米颗粒1-氧-二氨基-3,5-二硝基吡嗪炸药的制备方法
KR102615219B1 (ko) * 2020-11-09 2023-12-19 한국과학기술원 고순도 헥사나이트로스틸벤의 제조방법
CN116514664A (zh) * 2023-03-30 2023-08-01 中北大学 一种六硝基茋纯化工艺

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3505413A (en) * 1964-05-05 1970-04-07 Us Navy Hexanitrostilbene
US3510266A (en) * 1967-03-29 1970-05-05 Merck & Co Inc Production of crystals in a fluidized bed with ultrasonic vibrations
US3699176A (en) * 1970-10-02 1972-10-17 Del Mar Eng Lab Process for recrystallizing hexanitrostilbene
US4245129A (en) * 1979-08-14 1981-01-13 The United States Of America As Represented By The Secretary Of The Army Process for preparing hexanitrobibenzyl
US4268696A (en) * 1980-01-14 1981-05-19 The United States Of America As Represented By The Secretary Of The Army Method for preparing hexanitrostilbene
US4604489A (en) * 1984-04-20 1986-08-05 The United States Of America As Represented By The Secretary Of The Navy Recrystallization of hexanitrostilbene from dimethylsulfoxide and methanol

Also Published As

Publication number Publication date
NO880233D0 (no) 1988-01-20
NO169770B (no) 1992-04-27
NO880233L (no) 1988-07-22
YU9388A (en) 1989-10-31
ES2007786A6 (es) 1989-07-01
ATE123757T1 (de) 1995-06-15
AU1062088A (en) 1988-08-04
BR8800160A (pt) 1988-08-30
SE468434B (sv) 1993-01-18
SE8700212L (sv) 1988-07-22
IN172139B (sh) 1993-04-17
SE8700212D0 (sv) 1987-01-21
DE3751347T2 (de) 1996-01-25
JP2569345B2 (ja) 1997-01-08
IL85103A (en) 1992-12-01
EP0277386B1 (en) 1995-06-14
EP0277386A2 (en) 1988-08-10
IL85103A0 (en) 1988-06-30
CA1339470C (en) 1997-09-23
ES2074044T3 (es) 1995-09-01
DE3751347D1 (de) 1995-07-20
NO169770C (no) 1992-08-05
EP0277386A3 (en) 1990-08-16
AU611125B2 (en) 1991-06-06
ZA88150B (en) 1988-06-28
AR244198A1 (es) 1993-10-29
JPS63301846A (ja) 1988-12-08

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