ES2055244T3 - Procedimiento para concentrar acido sulfurico que contiene sulfatos metalicos. - Google Patents

Procedimiento para concentrar acido sulfurico que contiene sulfatos metalicos.

Info

Publication number
ES2055244T3
ES2055244T3 ES90115375T ES90115375T ES2055244T3 ES 2055244 T3 ES2055244 T3 ES 2055244T3 ES 90115375 T ES90115375 T ES 90115375T ES 90115375 T ES90115375 T ES 90115375T ES 2055244 T3 ES2055244 T3 ES 2055244T3
Authority
ES
Spain
Prior art keywords
sulfuric acid
metallic sulphates
evaporators
sulphates
vapors
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES90115375T
Other languages
English (en)
Inventor
Gunter Dr Lailach
Rudolf Dr Gerken
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Application granted granted Critical
Publication of ES2055244T3 publication Critical patent/ES2055244T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/90—Separation; Purification
    • C01B17/901—Recovery from spent acids containing metallic ions, e.g. hydrolysis acids, pickling acids
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00—Chemistry of inorganic compounds
    • Y10S423/01—Waste acid containing iron
    • Y10S423/02—Sulfuric acid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)

Abstract

EL ACIDO SULFURICO SE RECUPERA A PARTIR DE ACIDOS DILUIDOS (17) QUE CONTIENEN SULFATOS METALICOS, POR CONCENTRACION EN EVAPORADORES DE VACIO (1,4,7) Y SEPARACION DE LOS SULFATOS METALICOS DE LAS SUSPENSIONES (32) PRODUCIDAS AL EVAPORAR. EN ESTE PROCESO, LOS VAPORES (34) QUE SALEN DE LOS EVAPORADORES (1,4,7) Y QUE CONTIENEN ACIDO SULFURICO, CON CONTENIDOS DE SULFATOS METALICOS Y SULFATOS METALICOS SOLIDOS, SON CONDENSADOS POR CONTACTO DIRECTO CON ACIDO SULFURICO Y CON EL CONDENSADO DE VAPORES (10) QUE CONTIENEN ACIDO SULFURICO CON SULFATOS METALICOS EN DISOLUCION. LA REFRIGERACION DE ESTE CONDENSADO DE VAPORES (37) QUE, CIRCULANDO EN CIRCUITO CERRADO, SE UTILIZA COMO MEDIO DE REGRIGERACION, TIENE LUGAR POR EVAPORACION DE AGUA EN UN EVAPORADOR DE FLASH (12) AL TIEMPO QUE SE CONCENTRA EL ACIDO SULFURICO Y LOS SULFUROS METALICOS. PREFERENTEMENTE, LOS VAPORES CONCENTRADOS (37), CON UN CONTENIDO DE ACIDO SULFURICO DEL 1 AL 30 % EN PESO, SE SEPARAN DEL CIRCUITO DE REFRIGERACION, SIENDO LLEVADOS DENUEVO A LOS EVAPORADORES (1,4,7).
ES90115375T 1989-08-23 1990-08-10 Procedimiento para concentrar acido sulfurico que contiene sulfatos metalicos. Expired - Lifetime ES2055244T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE3927751A DE3927751A1 (de) 1989-08-23 1989-08-23 Verfahren zum konzentrieren metallsulfathaltiger schwefelsaeure

Publications (1)

Publication Number Publication Date
ES2055244T3 true ES2055244T3 (es) 1994-08-16

Family

ID=6387647

Family Applications (1)

Application Number Title Priority Date Filing Date
ES90115375T Expired - Lifetime ES2055244T3 (es) 1989-08-23 1990-08-10 Procedimiento para concentrar acido sulfurico que contiene sulfatos metalicos.

Country Status (6)

Country Link
US (1) US5061472A (es)
EP (1) EP0418544B1 (es)
JP (1) JP2889337B2 (es)
CA (1) CA2023688A1 (es)
DE (2) DE3927751A1 (es)
ES (1) ES2055244T3 (es)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4029737C1 (es) * 1990-09-20 1991-12-05 Metallgesellschaft Ag, 6000 Frankfurt, De
JP2968877B2 (ja) * 1991-11-08 1999-11-02 日鉄鉱業株式会社 金属硫酸塩含有の廃硫酸から硫酸を回収する方法
US5275701A (en) * 1993-03-15 1994-01-04 Air Products And Chemicals, Inc. Process for purification and concentration of sulfuric acid
AU709404B2 (en) * 1995-07-24 1999-08-26 Kerr-Mcgee Pigments Gmbh & Co. Kg Process for the recovery of sulphuric acid from spent acids containing metal sulphates
US5603839A (en) * 1995-09-18 1997-02-18 Cecebe Technologies Inc. Process for the recovery of waste sulphuric acid
GB9816464D0 (en) * 1998-07-30 1998-09-23 Tioxide Group Services Ltd Process for the concentration of dilute sulphuric acid solutions
DE19920695A1 (de) * 1999-05-05 2000-11-16 Metallgesellschaft Ag Verfahren zur Aufkonzentrierung von Dünnsäure
IL147144A0 (en) * 1999-06-18 2002-08-14 Advanced Res & Tech Inst Cardiomyocytes with enhanced proliferative potential and methods for preparing and using the same
US20030116290A1 (en) * 2001-12-20 2003-06-26 3M Innovative Properties Company Continuous process for controlled evaporation of black liquor
US6869501B2 (en) 2001-12-20 2005-03-22 3M Innovative Properties Company Continuous process for controlled concentration of colloidal solutions
CN105399168B (zh) * 2015-12-18 2018-01-02 许达人 含硫酸及其盐溶液的多效蒸发浓缩装置及工艺
CN105858621B (zh) * 2016-04-12 2017-10-27 钮德明 一种采用气液接触法浓缩钛白废酸的方法
WO2018015138A1 (en) * 2016-07-21 2018-01-25 Haldor Topsøe A/S Method for production of sulfuric acid from sulfur containing feeds with gas quenching
CN108751147A (zh) * 2018-09-18 2018-11-06 攀枝花学院 太阳能与空气能互补的钛白废酸浓缩装置
CN110255506A (zh) * 2019-07-15 2019-09-20 湖北兴福电子材料有限公司 一种电子级硫酸生产的装置与方法
CN113277480A (zh) * 2021-06-08 2021-08-20 安徽金星钛白（集团）有限公司 一种钛白粉废酸处理方法
CN114455552B (zh) * 2022-03-07 2023-03-31 盛隆资源再生（无锡）有限公司 一种高cod废酸的处理装置和处理方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE972412C (de) * 1951-06-01 1959-07-16 Metallgesellschaft Ag Verfahren zum Eindampfen von Schwefelsaeure oder sich aehnlich verhaltenden Loesungen
FR1241856A (fr) * 1959-08-13 1960-09-23 Kestner App Evaporateurs Procédé de concentration d'acide sulfurique à haute teneur
US3948624A (en) * 1974-02-04 1976-04-06 Union Carbide Corporation Removal of sulfur compounds from gas streams
DE2632989A1 (de) * 1976-07-22 1978-02-02 Hoechst Ag Verfahren zum regenerieren von schwefelsaeure
DE2656236C3 (de) * 1976-12-11 1980-11-06 Hoechst Ag, 6000 Frankfurt Verfahren zum Regenerieren von Abfallschwefelsäure
DE3327769A1 (de) * 1983-08-02 1985-02-14 Bayer Ag, 5090 Leverkusen Verfahren zur aufarbeitung von duennsaeuren
DE3511479A1 (de) * 1985-03-14 1986-09-18 Bayer Ag, 5090 Leverkusen Verfahren zur rezirkulierung metallsulfathaltiger schwefelsaeure

Also Published As

Publication number Publication date
JPH0393610A (ja) 1991-04-18
EP0418544A1 (de) 1991-03-27
CA2023688A1 (en) 1991-02-24
DE59001358D1 (de) 1993-06-09
DE3927751A1 (de) 1991-02-28
US5061472A (en) 1991-10-29
JP2889337B2 (ja) 1999-05-10
EP0418544B1 (de) 1993-05-05

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