ES2053615T3 - Procedimiento mejorado para la preparacion de di-metil-eter puro. - Google Patents

Procedimiento mejorado para la preparacion de di-metil-eter puro.

Info

Publication number
ES2053615T3
ES2053615T3 ES88107118T ES88107118T ES2053615T3 ES 2053615 T3 ES2053615 T3 ES 2053615T3 ES 88107118 T ES88107118 T ES 88107118T ES 88107118 T ES88107118 T ES 88107118T ES 2053615 T3 ES2053615 T3 ES 2053615T3
Authority
ES
Spain
Prior art keywords
pure
eter
methyl
preparation
improved procedure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES88107118T
Other languages
English (en)
Inventor
Ewald Meisenburg
Horst Dr Dornhagen
Hartmut Dr Hammer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wintershall Dea Deutschland AG
Original Assignee
RWE Dea AG fuer Mineraloel und Chemie
RWE Dea AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by RWE Dea AG fuer Mineraloel und Chemie, RWE Dea AG filed Critical RWE Dea AG fuer Mineraloel und Chemie
Application granted granted Critical
Publication of ES2053615T3 publication Critical patent/ES2053615T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/09—Preparation of ethers by dehydration of compounds containing hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
    • C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/09—Plural feed
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/20—Power plant

Abstract

LA PATENTE AFECTA A UN PROCESO MEJORADO DE DIMETILETER PURO MEDIANTE DESHIDRATACION CATALITICA DE METANOL A TRAVES DE UN CATALIZADOR (TAU)-AL2O3 (QUE CONTIENE PREFERENTEMENTE PEQUEÑAS CANTIDADES DE SIO2) Y MEDIANTE PURIFICACION DEL PRODUCTO DE DESHIDRATACION PARA OBTENER DIMETILETER PURO EN DETERMINADOS FONDOS DE ESTA COLUMNA DE DESTILACION, Y POR EXTRACCION DE DIMETILETER POR ENCIMA DE DETERMINADOS FONDOS DE LA MISMA COLUMNA, APLICANDOSE ADEMAS DEL PRODUCTO DE DESHIDRATACION UN FLUIDO DE LAVADO.
ES88107118T 1988-05-04 1988-05-04 Procedimiento mejorado para la preparacion de di-metil-eter puro. Expired - Lifetime ES2053615T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP88107118A EP0340324B1 (de) 1988-05-04 1988-05-04 Verbessertes Verfahren zur Herstellung von reinem Dimethylether

Publications (1)

Publication Number Publication Date
ES2053615T3 true ES2053615T3 (es) 1994-08-01

Family

ID=8198946

Family Applications (1)

Application Number Title Priority Date Filing Date
ES88107118T Expired - Lifetime ES2053615T3 (es) 1988-05-04 1988-05-04 Procedimiento mejorado para la preparacion de di-metil-eter puro.

Country Status (14)

Country Link
US (1) US5037511A (es)
EP (2) EP0340324B1 (es)
JP (1) JPH0262838A (es)
AT (1) ATE83475T1 (es)
AU (1) AU618806B2 (es)
BR (1) BR8902105A (es)
DD (1) DD282909A5 (es)
DE (1) DE3876790D1 (es)
DK (1) DK216989A (es)
ES (1) ES2053615T3 (es)
FI (1) FI892110A (es)
NO (1) NO170971C (es)
PL (1) PL279266A1 (es)
ZA (1) ZA893149B (es)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4132993A1 (de) * 1991-10-04 1993-04-08 Rwe Dea Ag Verfahren zur herstellung von dimethylether
DE4208028A1 (de) * 1992-03-13 1993-09-16 Leuna Werke Ag Verfahren zur herstellung von hochreinem dimethylether
DE4321871A1 (de) * 1993-07-01 1995-02-23 Basf Ag Verfahren zur Herstellung von Alkoxy-carbonsäureestern
US5616217A (en) * 1995-08-17 1997-04-01 Texaco Chemical Inc. Controlled alkali treatment in the recovery of methyl tertiary butyl ether
US5684213A (en) * 1996-03-25 1997-11-04 Chemical Research & Licensing Company Method for the preparation of dialkyl ethers
US6800665B1 (en) 1996-05-13 2004-10-05 Jfe Holdings, Inc. Method for producing dimethyl ether
DE19625284A1 (de) * 1996-06-25 1998-01-02 Hoechst Ag Verfahren zur Trennung von Gemischen aus Dimethylether und Chlormethan
CN1095457C (zh) * 1998-08-12 2002-12-04 中国科学院大连化学物理研究所 一种由合成气制取二甲醚工艺
DK173614B1 (da) 1999-02-02 2001-04-30 Topsoe Haldor As Fremgangsmåde til fremstilling af methanol/dimethyletherblanding fra syntesegas
DE19943219A1 (de) * 1999-09-09 2001-03-15 Axiva Gmbh Verfahren zur Herstellung von Dimethylether
JP4706812B2 (ja) * 2000-12-25 2011-06-22 三菱瓦斯化学株式会社 ジメチルエーテルの製造方法
US7393990B2 (en) * 2001-06-26 2008-07-01 Exxonmobil Chemical Patents Inc. Production of light olefins from oxygenate using framework gallium-containing medium pore molecular sieve
KR100501922B1 (ko) * 2003-02-19 2005-07-18 에스케이 주식회사 메탄올로부터 디메틸에테르의 제조방법
JP4824917B2 (ja) * 2004-08-30 2011-11-30 東洋エンジニアリング株式会社 ジメチルエーテルの製造方法および装置ならびに軽質成分の分離方法および装置
CN101448765A (zh) 2006-05-19 2009-06-03 国际壳牌研究有限公司 环烯烃的烷基化方法
WO2007135053A1 (en) 2006-05-19 2007-11-29 Shell Internationale Research Maatschappij B.V. Process for the preparation of c5 and/or c6 olefins
KR100812099B1 (ko) 2006-11-28 2008-03-12 한국가스공사 디메틸에테르 제조용 혼합촉매, 이의 제조방법 및 이를 이용한 디메틸에테르 제조방법
EP2022774B1 (en) * 2007-08-07 2010-03-10 Research Institute of Petroleum Industry (RIPI) A method for the production of dimethyl ehter
US9139503B2 (en) * 2007-09-10 2015-09-22 Lummus Technology Inc. Method for the production of dimethyl ether
CA2704996A1 (en) 2007-11-19 2009-05-28 Shell Internationale Research Maatschappij B.V. Process for the preparation of an olefin
CN101896261B (zh) 2007-11-19 2014-01-29 国际壳牌研究有限公司 制备烯烃产品的方法
WO2009117851A1 (zh) * 2008-03-26 2009-10-01 中国石油化工股份有限公司 一种从甲醇生产二甲醚的方法
EP2373602B1 (en) 2008-12-22 2013-08-21 Shell Internationale Research Maatschappij B.V. Process to prepare methanol and/or dimethylether
US20100258446A1 (en) * 2009-04-03 2010-10-14 Board Of Regents Of The Nevada System Of Higher Education, On Behalf Of The University Of Nevada Systems including nanotubular arrays for converting carbon dioxide to an organic compound
US8378150B2 (en) * 2009-08-12 2013-02-19 Catalytic Distillation Technologies Process for the production of dimethyl ether
BR112012010865A2 (pt) 2009-11-10 2019-09-24 Shell International Res Maatshappij B V "processo para a produção de óxido de etileno".
EP2499219A2 (en) 2009-11-10 2012-09-19 Shell Internationale Research Maatschappij B.V. Process for producing olefins
CA2778363A1 (en) 2009-11-10 2011-05-19 Shell Internationale Research Maatschappij B.V. Process for producing olefins
CN102858720A (zh) 2010-04-23 2013-01-02 国际壳牌研究有限公司 生产芳族烃和乙烯的方法
EP2695946A1 (de) 2012-08-09 2014-02-12 Methapower Biogas GmbH Verfahren und Anlage zur Herstellung von Dimethylether
CN103012076A (zh) * 2012-12-24 2013-04-03 新奥科技发展有限公司 二甲醚精馏及回收不凝气中二甲醚的方法及装置
US20140275634A1 (en) * 2013-03-15 2014-09-18 Gas Technologies Llc Ether Blends Via Reactive Distillation
US9505690B2 (en) * 2013-05-31 2016-11-29 Shell Oil Company Systems and methods for recovering dimethyl ether from gas mixtures and liquid mixtures
DK3710562T3 (da) 2017-11-15 2023-12-18 Gas Technology Inst Fremgangsmåde til reformering af methan og lette carbonhydrider til flydende carbonhydridbrændstoffer
JP2022534527A (ja) * 2019-05-27 2022-08-01 カウンシル オブ サイエンティフィック アンド インダストリアル リサーチ ステップ円錐形の反応器を用いたジアルキルエーテル合成の強化方法
EP4204355A1 (en) 2020-08-26 2023-07-05 GTI Energy Liquid phase reforming of oxygenates for hydrogen production

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1050750B (de) * 1959-02-19 Esso Research And Engineering Company, Elizabeth, N. J. (V. St. A.) Verfahren zur Reinigung von Alkyläthern
GB332756A (es) *
FR701335A (fr) * 1929-08-01 1931-03-14 Bataafsche Petroleum Procédé de préparation des éthers à partir des alcools
GB350010A (en) * 1930-03-05 1931-06-05 Bataafsche Petroleum Process for the manufacture of ethers from alcohols
GB403402A (en) * 1931-05-28 1933-11-30 Du Pont Improvements in or relating to the production of aliphatic ethers
DE680328C (de) * 1934-12-29 1939-08-29 Wacker Chemie Gmbh Verfahren zur Herstellung von AEthern
US3296314A (en) * 1963-11-12 1967-01-03 Du Pont Process for purifying methyl ether
US3356590A (en) * 1967-01-13 1967-12-05 Phillips Petroleum Co Controlling a distillation operation to maintain specified product purities with optimum feed enthalpy
US3847756A (en) * 1972-11-09 1974-11-12 Eastman Kodak Co Recovery of diethyl ether from an olefin hydration product stream by extractive distillation with water
IT972655B (it) * 1972-12-20 1974-05-31 Snam Progetti Procedimento per la produzione di dimetil etere
IT1065295B (it) * 1976-12-23 1985-02-25 Snam Progetti Processo per la produzione di dimetil etere e catalizzatore utilizzabile in detto processo
US4156698A (en) * 1977-05-05 1979-05-29 Mobil Oil Corporation Conversion of alcohols or ethers using rare earth crystalline aluminosilicate in an alumina matrix
NZ199035A (en) * 1981-02-20 1984-09-28 Mobil Oil Corp Catalyst of co-precipitated cu,zu and a1 components:conversion of syngas into dimethyl ether
IT1137176B (it) * 1981-06-02 1986-09-03 Anic Spa Procedimento per la produzione di dimetiletere
CA1231724A (en) * 1982-07-01 1988-01-19 E. I. Du Pont De Nemours And Company Catalytic preparation of dimethyl ether
JPS59199648A (ja) * 1983-04-27 1984-11-12 Mitsubishi Chem Ind Ltd ジメチルエ−テルの製造法
US4665249A (en) * 1984-12-19 1987-05-12 Mobil Oil Corporation Method for feeding an MTG conversion reactor
US4722769A (en) * 1986-04-24 1988-02-02 Allied Corporation Process for recovery of acetone
AU603070B2 (en) * 1986-11-18 1990-11-08 Rwe-Dea Aktiengesellschaft Fur Mineraloel Und Chemie Process for the purification of dimethylether
DE3642845A1 (de) * 1986-12-16 1988-06-30 Union Rheinische Braunkohlen Verfahren zur herstellung von dimethylether und dazu verwendeter katalysator
US4802956A (en) * 1986-11-20 1989-02-07 Horst Dornhagen Process for the purification of dimethylether by distillation

Also Published As

Publication number Publication date
EP0340324A3 (en) 1990-06-13
ATE83475T1 (de) 1993-01-15
US5037511A (en) 1991-08-06
EP0340576A3 (de) 1991-05-08
ZA893149B (en) 1990-01-31
NO891836D0 (no) 1989-05-03
DE3876790D1 (de) 1993-01-28
NO170971B (no) 1992-09-28
EP0340576A2 (de) 1989-11-08
EP0340324A2 (de) 1989-11-08
EP0340324B1 (de) 1992-12-16
AU618806B2 (en) 1992-01-09
PL279266A1 (en) 1990-01-08
FI892110A0 (fi) 1989-05-03
DK216989D0 (da) 1989-05-03
DD282909A5 (de) 1990-09-26
AU3400289A (en) 1989-11-09
FI892110A (fi) 1989-11-05
BR8902105A (pt) 1989-12-05
NO170971C (no) 1993-01-06
DK216989A (da) 1989-11-05
NO891836L (no) 1989-11-06
JPH0262838A (ja) 1990-03-02

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