JPS56152457A - Preparation of peroxide - Google Patents
Preparation of peroxideInfo
- Publication number
- JPS56152457A JPS56152457A JP5534980A JP5534980A JPS56152457A JP S56152457 A JPS56152457 A JP S56152457A JP 5534980 A JP5534980 A JP 5534980A JP 5534980 A JP5534980 A JP 5534980A JP S56152457 A JPS56152457 A JP S56152457A
- Authority
- JP
- Japan
- Prior art keywords
- perchloric acid
- hydroperoxide
- aromatic
- alcohol
- hydroxyperoxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To obtain the titled compound useful as a crosslinking agent, decomposer, etc. for high polymer compounds in high yield with small side reactions, by condensing an aromatic alcohol with a hydroperoxide while an aqueous solution of perchloric acid being added gradually to their mixture.
CONSTITUTION: An aromatic alcohol (preferably 9W13C aromatic tertiary alcohol, e.g., α,α'-dihydroxy-m-diisopropylbenzene, etc.) is condensed with a hydroxyperoxide (preferably, 4W8C aliphatic tertiary hydroperoxide, or 9W16C aromatic tertiary hydroperoxide) preferably at 20W60°C for 3W10hr while an aqueous solution of perchloric acid (preferably 40W70wt% concentration) being gradually added to their mixture, to give the desired peroxide. The amount of perchloric acid used is preferably 0.1W1.5mol per equivalent of smaller one of the hydroxyperoxide group or hydroxyl group in the raw materials.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5534980A JPS56152457A (en) | 1980-04-28 | 1980-04-28 | Preparation of peroxide |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5534980A JPS56152457A (en) | 1980-04-28 | 1980-04-28 | Preparation of peroxide |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS56152457A true JPS56152457A (en) | 1981-11-26 |
JPS6318580B2 JPS6318580B2 (en) | 1988-04-19 |
Family
ID=12996016
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP5534980A Granted JPS56152457A (en) | 1980-04-28 | 1980-04-28 | Preparation of peroxide |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS56152457A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102796035A (en) * | 2012-09-07 | 2012-11-28 | 金魏 | Condensation method of m-,p-mixed di-(tert-butyl isopropyl peroxide)benzene |
JP2016527299A (en) * | 2013-08-08 | 2016-09-08 | アルケマ フランス | Process for preparing organic peroxides |
CN106588735A (en) * | 2015-10-20 | 2017-04-26 | 中国石油化工集团公司 | Bis(t-butylperoxyisopropyl)benzene production method |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103058908A (en) * | 2012-12-25 | 2013-04-24 | 宁波东来化工有限公司 | One-step synthetic method for bis(t-butylperoxyisopropyl)benzene |
-
1980
- 1980-04-28 JP JP5534980A patent/JPS56152457A/en active Granted
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102796035A (en) * | 2012-09-07 | 2012-11-28 | 金魏 | Condensation method of m-,p-mixed di-(tert-butyl isopropyl peroxide)benzene |
JP2016527299A (en) * | 2013-08-08 | 2016-09-08 | アルケマ フランス | Process for preparing organic peroxides |
CN106588735A (en) * | 2015-10-20 | 2017-04-26 | 中国石油化工集团公司 | Bis(t-butylperoxyisopropyl)benzene production method |
Also Published As
Publication number | Publication date |
---|---|
JPS6318580B2 (en) | 1988-04-19 |
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