JPS56152457A - Preparation of peroxide - Google Patents

Preparation of peroxide

Info

Publication number
JPS56152457A
JPS56152457A JP5534980A JP5534980A JPS56152457A JP S56152457 A JPS56152457 A JP S56152457A JP 5534980 A JP5534980 A JP 5534980A JP 5534980 A JP5534980 A JP 5534980A JP S56152457 A JPS56152457 A JP S56152457A
Authority
JP
Japan
Prior art keywords
perchloric acid
hydroperoxide
aromatic
alcohol
hydroxyperoxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP5534980A
Other languages
Japanese (ja)
Other versions
JPS6318580B2 (en
Inventor
Kenichi Mizuno
Tetsuhiro Matsumoto
Michio Tanaka
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Petrochemical Industries Ltd
Original Assignee
Mitsui Petrochemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Petrochemical Industries Ltd filed Critical Mitsui Petrochemical Industries Ltd
Priority to JP5534980A priority Critical patent/JPS56152457A/en
Publication of JPS56152457A publication Critical patent/JPS56152457A/en
Publication of JPS6318580B2 publication Critical patent/JPS6318580B2/ja
Granted legal-status Critical Current

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURPOSE: To obtain the titled compound useful as a crosslinking agent, decomposer, etc. for high polymer compounds in high yield with small side reactions, by condensing an aromatic alcohol with a hydroperoxide while an aqueous solution of perchloric acid being added gradually to their mixture.
CONSTITUTION: An aromatic alcohol (preferably 9W13C aromatic tertiary alcohol, e.g., α,α'-dihydroxy-m-diisopropylbenzene, etc.) is condensed with a hydroxyperoxide (preferably, 4W8C aliphatic tertiary hydroperoxide, or 9W16C aromatic tertiary hydroperoxide) preferably at 20W60°C for 3W10hr while an aqueous solution of perchloric acid (preferably 40W70wt% concentration) being gradually added to their mixture, to give the desired peroxide. The amount of perchloric acid used is preferably 0.1W1.5mol per equivalent of smaller one of the hydroxyperoxide group or hydroxyl group in the raw materials.
COPYRIGHT: (C)1981,JPO&Japio
JP5534980A 1980-04-28 1980-04-28 Preparation of peroxide Granted JPS56152457A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP5534980A JPS56152457A (en) 1980-04-28 1980-04-28 Preparation of peroxide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP5534980A JPS56152457A (en) 1980-04-28 1980-04-28 Preparation of peroxide

Publications (2)

Publication Number Publication Date
JPS56152457A true JPS56152457A (en) 1981-11-26
JPS6318580B2 JPS6318580B2 (en) 1988-04-19

Family

ID=12996016

Family Applications (1)

Application Number Title Priority Date Filing Date
JP5534980A Granted JPS56152457A (en) 1980-04-28 1980-04-28 Preparation of peroxide

Country Status (1)

Country Link
JP (1) JPS56152457A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102796035A (en) * 2012-09-07 2012-11-28 金魏 Condensation method of m-,p-mixed di-(tert-butyl isopropyl peroxide)benzene
JP2016527299A (en) * 2013-08-08 2016-09-08 アルケマ フランス Process for preparing organic peroxides
CN106588735A (en) * 2015-10-20 2017-04-26 中国石油化工集团公司 Bis(t-butylperoxyisopropyl)benzene production method

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103058908A (en) * 2012-12-25 2013-04-24 宁波东来化工有限公司 One-step synthetic method for bis(t-butylperoxyisopropyl)benzene

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102796035A (en) * 2012-09-07 2012-11-28 金魏 Condensation method of m-,p-mixed di-(tert-butyl isopropyl peroxide)benzene
JP2016527299A (en) * 2013-08-08 2016-09-08 アルケマ フランス Process for preparing organic peroxides
CN106588735A (en) * 2015-10-20 2017-04-26 中国石油化工集团公司 Bis(t-butylperoxyisopropyl)benzene production method

Also Published As

Publication number Publication date
JPS6318580B2 (en) 1988-04-19

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