EP2872464A1 - Insensitive sprengstoffwirkmasse - Google Patents
Insensitive sprengstoffwirkmasseInfo
- Publication number
- EP2872464A1 EP2872464A1 EP13732834.0A EP13732834A EP2872464A1 EP 2872464 A1 EP2872464 A1 EP 2872464A1 EP 13732834 A EP13732834 A EP 13732834A EP 2872464 A1 EP2872464 A1 EP 2872464A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- explosive
- insensitive
- active material
- chlorinated paraffin
- material according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002360 explosive Substances 0.000 title claims abstract description 93
- 239000013543 active substance Substances 0.000 title claims abstract description 17
- 239000011230 binding agent Substances 0.000 claims abstract description 23
- 239000000203 mixture Substances 0.000 claims abstract description 12
- 239000004800 polyvinyl chloride Substances 0.000 claims abstract description 10
- 229920000915 polyvinyl chloride Polymers 0.000 claims abstract description 8
- 239000012188 paraffin wax Substances 0.000 claims description 28
- 239000011149 active material Substances 0.000 claims description 27
- 239000004014 plasticizer Substances 0.000 claims description 27
- UZGLIIJVICEWHF-UHFFFAOYSA-N octogen Chemical group [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)CN([N+]([O-])=O)C1 UZGLIIJVICEWHF-UHFFFAOYSA-N 0.000 claims description 26
- 239000000028 HMX Substances 0.000 claims description 25
- MKWKGRNINWTHMC-UHFFFAOYSA-N 4,5,6-trinitrobenzene-1,2,3-triamine Chemical compound NC1=C(N)C([N+]([O-])=O)=C([N+]([O-])=O)C([N+]([O-])=O)=C1N MKWKGRNINWTHMC-UHFFFAOYSA-N 0.000 claims description 4
- NDYLCHGXSQOGMS-UHFFFAOYSA-N CL-20 Chemical compound [O-][N+](=O)N1C2N([N+]([O-])=O)C3N([N+](=O)[O-])C2N([N+]([O-])=O)C2N([N+]([O-])=O)C3N([N+]([O-])=O)C21 NDYLCHGXSQOGMS-UHFFFAOYSA-N 0.000 claims description 4
- TZRXHJWUDPFEEY-UHFFFAOYSA-N Pentaerythritol Tetranitrate Chemical compound [O-][N+](=O)OCC(CO[N+]([O-])=O)(CO[N+]([O-])=O)CO[N+]([O-])=O TZRXHJWUDPFEEY-UHFFFAOYSA-N 0.000 claims description 4
- XTFIVUDBNACUBN-UHFFFAOYSA-N 1,3,5-trinitro-1,3,5-triazinane Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)C1 XTFIVUDBNACUBN-UHFFFAOYSA-N 0.000 claims description 2
- QVYSQTANFYDRPQ-UHFFFAOYSA-N NC(=C([N+](=O)[O-])N)[N+](=O)[O-] Chemical group NC(=C([N+](=O)[O-])N)[N+](=O)[O-] QVYSQTANFYDRPQ-UHFFFAOYSA-N 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 238000005660 chlorination reaction Methods 0.000 claims description 2
- FUHQFAMVYDIUKL-UHFFFAOYSA-N fox-7 Chemical compound NC(N)=C([N+]([O-])=O)[N+]([O-])=O FUHQFAMVYDIUKL-UHFFFAOYSA-N 0.000 claims description 2
- 239000002904 solvent Substances 0.000 description 12
- 239000004744 fabric Substances 0.000 description 10
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 9
- 229910052801 chlorine Inorganic materials 0.000 description 9
- 239000000460 chlorine Substances 0.000 description 9
- 239000013256 coordination polymer Substances 0.000 description 9
- 239000007788 liquid Substances 0.000 description 6
- 239000004094 surface-active agent Substances 0.000 description 6
- 238000005474 detonation Methods 0.000 description 4
- 230000005012 migration Effects 0.000 description 4
- 238000013508 migration Methods 0.000 description 4
- 239000004033 plastic Substances 0.000 description 4
- 229920003023 plastic Polymers 0.000 description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- 229920000800 acrylic rubber Polymers 0.000 description 3
- 230000004888 barrier function Effects 0.000 description 3
- 238000009792 diffusion process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- ZFMQKOWCDKKBIF-UHFFFAOYSA-N bis(3,5-difluorophenyl)phosphane Chemical compound FC1=CC(F)=CC(PC=2C=C(F)C=C(F)C=2)=C1 ZFMQKOWCDKKBIF-UHFFFAOYSA-N 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000009477 glass transition Effects 0.000 description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
- 239000008188 pellet Substances 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000000113 differential scanning calorimetry Methods 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- APSBXTVYXVQYAB-UHFFFAOYSA-M sodium docusate Chemical group [Na+].CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC APSBXTVYXVQYAB-UHFFFAOYSA-M 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0033—Shaping the mixture
- C06B21/0041—Shaping the mixture by compression
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B45/00—Compositions or products which are defined by structure or arrangement of component of product
- C06B45/04—Compositions or products which are defined by structure or arrangement of component of product comprising solid particles dispersed in solid solution or matrix not used for explosives where the matrix consists essentially of nitrated carbohydrates or a low molecular organic explosive
- C06B45/06—Compositions or products which are defined by structure or arrangement of component of product comprising solid particles dispersed in solid solution or matrix not used for explosives where the matrix consists essentially of nitrated carbohydrates or a low molecular organic explosive the solid solution or matrix containing an organic component
- C06B45/10—Compositions or products which are defined by structure or arrangement of component of product comprising solid particles dispersed in solid solution or matrix not used for explosives where the matrix consists essentially of nitrated carbohydrates or a low molecular organic explosive the solid solution or matrix containing an organic component the organic component containing a resin
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B45/00—Compositions or products which are defined by structure or arrangement of component of product
- C06B45/18—Compositions or products which are defined by structure or arrangement of component of product comprising a coated component
- C06B45/20—Compositions or products which are defined by structure or arrangement of component of product comprising a coated component the component base containing an organic explosive or an organic thermic component
- C06B45/22—Compositions or products which are defined by structure or arrangement of component of product comprising a coated component the component base containing an organic explosive or an organic thermic component the coating containing an organic compound
Definitions
- the invention relates to an insensitive explosive active material which requires no plasticizer and can nevertheless be realized with a high density.
- a reduction in the density of an explosive active mass reduces its performance as it detonates. It is therefore always trying to produce explosive active materials with the highest possible density.
- an insensitive explosive active composition comprising an explosive and a chlorinated paraffin or a mixture of a chlorinated paraffin and polyvinyl chloride (PVC) as binder is provided.
- the inventors of the present invention have recognized that chloroparaffins have a large
- chloroparaffin With chloroparaffin, it is possible to provide an insensitive explosive active material with only 5 wt .-% binder, without the explosives active mass thereby significantly loses power over the explosive itself. This is because chloroparaffins have a high density and thus the entire
- TMD means "theoretical maximum density” in the unit kg / m 3 .
- Chlorine paraffin was in the above examples in each case by the company Leuna-Tenside GmbH, 06237 Leuna, Germany.
- Polyvinyl chloride was purchased from Solvay SA, Belgium and Oktogen from Nexplo Bofors AB, Karlskoga, Sweden.
- sieved 630 [im” means that the maximum size of the particles it contains is 630.
- CP is the abbreviation for chlorinated paraffin.
- the height of a standardized water column is measured, which is sufficient to transmit a shock wave generated by detonation of a standard explosive charge in the water column on the explosive active mass to be examined, so that they still reliably detonated, and reliably no longer detonated.
- the values are given in mm of the water column.
- the first value under "Gap [mm]” in each case denotes the value at which the explosive active substance to be investigated reliably detonates ("GO") and a second value, the value at which the explosive active substance to be investigated no longer detonates ("NO GO "). The lower these values are, the more insensitive the explosive active mass is.
- the results of the gap test are shown in the table below.
- Example 6 1871 1835 98.1 16/17 GO / NO GO n. G.
- Example 10 1843 1810 98.2 12/14 GO / NO GO -48 Tg means "glass transition temperature", "ng” means “not measured”. The glass transition temperature was measured by differential scanning calorimetry (DSC). The detonation rates calculated for Examples 1 to 10 above
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Dispersion Chemistry (AREA)
- Molecular Biology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
Claims
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102012013961.6A DE102012013961A1 (de) | 2012-07-13 | 2012-07-13 | Insensitive Sprengstoffwirkmasse |
PCT/EP2013/001898 WO2014008986A1 (de) | 2012-07-13 | 2013-06-28 | Insensitive sprengstoffwirkmasse |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2872464A1 true EP2872464A1 (de) | 2015-05-20 |
EP2872464B1 EP2872464B1 (de) | 2018-05-30 |
Family
ID=48741048
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP13732834.0A Not-in-force EP2872464B1 (de) | 2012-07-13 | 2013-06-28 | Insensitive sprengstoffwirkmasse |
Country Status (3)
Country | Link |
---|---|
EP (1) | EP2872464B1 (de) |
DE (1) | DE102012013961A1 (de) |
WO (1) | WO2014008986A1 (de) |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL280149A (de) * | 1961-06-26 | 1900-01-01 | ||
DE1209926B (de) * | 1964-08-31 | 1966-01-27 | Buck K G Chemische Und Tech | Nebelmittel |
US3290190A (en) * | 1965-07-06 | 1966-12-06 | Atlantic Res Corp | Plastisol propellant process with improved dispersion stability |
ES381787A1 (es) * | 1969-08-29 | 1972-11-16 | Knapsack Ag | Procedimiento para la produccion de superficies de raspadorestables frente al agua, para cerillas. |
DE2451701C3 (de) * | 1974-10-31 | 1978-03-09 | Pyrotechnische Fabrik F. Feistel Kg, 6719 Goellheim | Rauch- oder Nebelsatz und Verfahren zu seiner Herstellung |
CH643804A5 (en) * | 1980-07-24 | 1984-06-29 | Oerlikon Buehrle Ag | Explosive and process for its manufacture |
FR2545478B1 (fr) * | 1983-05-03 | 1985-07-05 | Commissariat Energie Atomique | Composition explosive moulable a froid et son procede de preparation |
US4981534B1 (en) * | 1990-03-07 | 1997-02-04 | Atlantic Res Corp | Occupant restraint system and composition useful therein |
US5540794A (en) * | 1992-05-11 | 1996-07-30 | Thiokol Corporation | Energetic binder and thermoplastic elastomer-based low vulnerability ammunition gun propellants with improved mechanical properties |
CA2107256A1 (en) * | 1993-03-12 | 1994-09-13 | Joseph E. Flanagan | High-density insensitive explosives |
EP1342047B1 (de) * | 2000-12-13 | 2006-02-22 | The Secretary of State for Defence | Infrarot-leuchsatz |
US7955452B1 (en) * | 2009-03-10 | 2011-06-07 | The United States Of America As Represented By The Secretary Of The Army | Process for crystalline explosives containing halogenated wax binders |
-
2012
- 2012-07-13 DE DE102012013961.6A patent/DE102012013961A1/de not_active Ceased
-
2013
- 2013-06-28 WO PCT/EP2013/001898 patent/WO2014008986A1/de active Application Filing
- 2013-06-28 EP EP13732834.0A patent/EP2872464B1/de not_active Not-in-force
Non-Patent Citations (1)
Title |
---|
See references of WO2014008986A1 * |
Also Published As
Publication number | Publication date |
---|---|
DE102012013961A1 (de) | 2014-01-16 |
WO2014008986A1 (de) | 2014-01-16 |
EP2872464B1 (de) | 2018-05-30 |
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