EP2493835A4 - Procédé pour la préparation de composés aromatiques deutérés - Google Patents

Procédé pour la préparation de composés aromatiques deutérés

Info

Publication number
EP2493835A4
EP2493835A4 EP09850996.1A EP09850996A EP2493835A4 EP 2493835 A4 EP2493835 A4 EP 2493835A4 EP 09850996 A EP09850996 A EP 09850996A EP 2493835 A4 EP2493835 A4 EP 2493835A4
Authority
EP
European Patent Office
Prior art keywords
aromatic compounds
deuterated aromatic
preparing deuterated
preparing
compounds
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP09850996.1A
Other languages
German (de)
English (en)
Other versions
EP2493835A1 (fr
Inventor
Eric Maurice Smith
Kalindi Dogra
Christina M Older
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of EP2493835A1 publication Critical patent/EP2493835A1/fr
Publication of EP2493835A4 publication Critical patent/EP2493835A4/fr
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B59/00—Introduction of isotopes of elements into organic compounds ; Labelled organic compounds per se
    • C07B59/001—Acyclic or carbocyclic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B59/00—Introduction of isotopes of elements into organic compounds ; Labelled organic compounds per se
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/20—Polycyclic condensed hydrocarbons
    • C07C15/24—Polycyclic condensed hydrocarbons containing two rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/20—Polycyclic condensed hydrocarbons
    • C07C15/27—Polycyclic condensed hydrocarbons containing three rings
    • C07C15/30—Phenanthrenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/05—Isotopically modified compounds, e.g. labelled
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2531/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • C07C2531/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • C07C2531/025—Sulfonic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/04—Ortho- or ortho- and peri-condensed systems containing three rings
    • C07C2603/22—Ortho- or ortho- and peri-condensed systems containing three rings containing only six-membered rings
    • C07C2603/24—Anthracenes; Hydrogenated anthracenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/40—Ortho- or ortho- and peri-condensed systems containing four condensed rings
    • C07C2603/42—Ortho- or ortho- and peri-condensed systems containing four condensed rings containing only six-membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/40—Ortho- or ortho- and peri-condensed systems containing four condensed rings
    • C07C2603/42—Ortho- or ortho- and peri-condensed systems containing four condensed rings containing only six-membered rings
    • C07C2603/48—Chrysenes; Hydrogenated chrysenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/40—Ortho- or ortho- and peri-condensed systems containing four condensed rings
    • C07C2603/42—Ortho- or ortho- and peri-condensed systems containing four condensed rings containing only six-membered rings
    • C07C2603/50—Pyrenes; Hydrogenated pyrenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/52—Ortho- or ortho- and peri-condensed systems containing five condensed rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Indole Compounds (AREA)
EP09850996.1A 2009-10-26 2009-12-21 Procédé pour la préparation de composés aromatiques deutérés Withdrawn EP2493835A4 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US25484309P 2009-10-26 2009-10-26
PCT/US2009/068924 WO2011053334A1 (fr) 2009-10-26 2009-12-21 Procédé pour la préparation de composés aromatiques deutérés

Publications (2)

Publication Number Publication Date
EP2493835A1 EP2493835A1 (fr) 2012-09-05
EP2493835A4 true EP2493835A4 (fr) 2015-07-15

Family

ID=43922420

Family Applications (1)

Application Number Title Priority Date Filing Date
EP09850996.1A Withdrawn EP2493835A4 (fr) 2009-10-26 2009-12-21 Procédé pour la préparation de composés aromatiques deutérés

Country Status (6)

Country Link
EP (1) EP2493835A4 (fr)
JP (1) JP5662461B2 (fr)
KR (1) KR101538534B1 (fr)
CN (1) CN102574753B (fr)
TW (1) TW201114735A (fr)
WO (1) WO2011053334A1 (fr)

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8759818B2 (en) 2009-02-27 2014-06-24 E I Du Pont De Nemours And Company Deuterated compounds for electronic applications
JP5567656B2 (ja) 2009-04-03 2014-08-06 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 電気活性材料
KR20120091144A (ko) 2009-09-29 2012-08-17 이 아이 듀폰 디 네모아 앤드 캄파니 발광 응용을 위한 중수소화된 화합물
EP2493887A4 (fr) 2009-10-29 2013-06-19 Du Pont Composés deutérés pour des applications électroniques
US8617720B2 (en) 2009-12-21 2013-12-31 E I Du Pont De Nemours And Company Electroactive composition and electronic device made with the composition
TW201229204A (en) 2010-12-17 2012-07-16 Du Pont Anthracene derivative compounds for electronic applications
WO2012083301A1 (fr) 2010-12-17 2012-06-21 E. I. Du Pont De Nemours And Company Composés dérivés de l'anthracène pour applications électroniques
US9293716B2 (en) 2010-12-20 2016-03-22 Ei Du Pont De Nemours And Company Compositions for electronic applications
KR20140015298A (ko) 2010-12-20 2014-02-06 이 아이 듀폰 디 네모아 앤드 캄파니 전자적 응용을 위한 전기활성 조성물
JP2014507401A (ja) 2010-12-20 2014-03-27 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 電子技術応用のためのトリアジン誘導体
JP5926286B2 (ja) 2010-12-21 2016-05-25 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ ピリミジン化合物を含む電子デバイス
WO2014130597A1 (fr) 2013-02-25 2014-08-28 E. I. Du Pont De Nemours And Company Dispositif électronique comprenant un dérivé de diazachrysène
US10134988B2 (en) 2013-12-13 2018-11-20 E I Du Pont De Nemours And Company System for forming an electroactive layer
CN104198631B (zh) * 2014-08-11 2017-01-18 贾明宏 一种提高蛋白质在氘代试剂中氢氘原子交换效率的方法
US9944846B2 (en) 2014-08-28 2018-04-17 E I Du Pont De Nemours And Company Compositions for electronic applications
CN107074763B (zh) 2014-10-20 2021-01-05 株式会社Lg化学 蓝色发光化合物
US10804473B2 (en) 2015-05-21 2020-10-13 Lg Chem, Ltd. Electron transport materials for electronic applications
JP6789594B2 (ja) 2016-07-20 2020-11-25 エルジー・ケム・リミテッド 電気活性材料
KR102627027B1 (ko) * 2019-11-29 2024-01-18 주식회사 엘지화학 중수소화 안트라센계 화합물의 제조 방법 및 이로부터 제조된 중수소화 안트라센계 화합물을 포함하는 유기 발광 소자
KR102594845B1 (ko) * 2019-12-23 2023-10-27 주식회사 엘지화학 방향족 화합물의 제조방법
CN115362148A (zh) * 2020-04-10 2022-11-18 德山新勒克斯有限公司 用于有机电气元件的化合物、使用所述化合物的有机电气元件及其电子装置
KR20210126822A (ko) * 2020-04-10 2021-10-21 덕산네오룩스 주식회사 유기전기소자용 화합물, 이를 이용한 유기전기소자 및 그 전자 장치
KR20210128205A (ko) * 2020-04-16 2021-10-26 덕산네오룩스 주식회사 유기전기소자용 화합물, 이를 이용한 유기전기소자 및 그 전자 장치
CN113555519A (zh) 2020-04-24 2021-10-26 罗门哈斯电子材料韩国有限公司 有机电致发光装置
KR102657636B1 (ko) 2020-06-09 2024-04-15 주식회사 엘지화학 안트라센계 화합물, 이를 포함하는 코팅조성물 및 유기 발광 소자
CN113896734A (zh) 2020-07-06 2022-01-07 罗门哈斯电子材料韩国有限公司 有机电致发光化合物、多种主体材料和包含其的有机电致发光装置
KR102657637B1 (ko) 2020-07-08 2024-04-15 주식회사 엘지화학 안트라센계 화합물, 이를 포함하는 코팅조성물 및 유기 발광 소자
KR20220065451A (ko) 2020-11-13 2022-05-20 주식회사 엘지화학 화합물 및 이를 포함하는 유기 발광 소자
KR20220065449A (ko) 2020-11-13 2022-05-20 주식회사 엘지화학 화합물 및 이를 포함하는 유기 발광 소자
KR20220065453A (ko) 2020-11-13 2022-05-20 주식회사 엘지화학 화합물 및 이를 포함하는 유기 발광 소자
KR20220065950A (ko) 2020-11-13 2022-05-23 주식회사 엘지화학 화합물 및 이를 포함하는 유기 발광 소자
KR102630972B1 (ko) 2021-01-08 2024-01-29 주식회사 엘지화학 안트라센계 화합물, 및 이를 포함하는 유기 발광 소자
KR102629146B1 (ko) 2021-01-08 2024-01-24 주식회사 엘지화학 안트라센계 화합물, 및 이를 포함하는 유기 발광 소자
DE102022112831A1 (de) * 2021-05-26 2022-12-01 Rohm And Haas Electronic Materials Korea Ltd. Verfahren zur herstellung von deuterierten organischen verbindungen
CN117480168A (zh) 2021-07-07 2024-01-30 株式会社Lg化学 化合物及包含其的有机发光器件
KR20230018162A (ko) 2021-07-29 2023-02-07 주식회사 엘지화학 화합물 및 이를 포함하는 유기 발광 소자
KR20230018160A (ko) 2021-07-29 2023-02-07 주식회사 엘지화학 화합물 및 이를 포함하는 유기 발광 소자
KR20230018159A (ko) 2021-07-29 2023-02-07 주식회사 엘지화학 화합물 및 이를 포함하는 유기 발광 소자
US20230255102A1 (en) 2022-01-20 2023-08-10 Rohm And Haas Electronic Materials Korea Ltd. Plurality of host materials and organic electroluminescent device comprising the same
EP4231804A3 (fr) 2022-02-16 2023-09-20 Universal Display Corporation Matériaux et dispositifs électroluminescents organiques
US20240107880A1 (en) 2022-08-17 2024-03-28 Universal Display Corporation Organic electroluminescent materials and devices

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3989705A (en) * 1974-04-01 1976-11-02 Canadian Patents And Development Limited Processes for the deuteration and/or tritiation of organic substrates by hydrogen substitution
WO2011059463A1 (fr) * 2009-10-29 2011-05-19 E. I. Du Pont De Nemours And Company Composés deutérés pour des applications électroniques

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3389705A (en) * 1966-04-29 1968-06-25 Levavi David Cigarette smoke filter device
JPS6153228A (ja) * 1984-08-22 1986-03-17 Nippon Sheet Glass Co Ltd 芳香族化合物に高選択的に水素同位体を導入する方法
JPH0653693B2 (ja) * 1986-07-24 1994-07-20 ユニチカ株式会社 重水素化フエノ−ル類の製造方法
JPH06228014A (ja) * 1993-01-28 1994-08-16 Tosoh Corp 重水素化芳香族化合物の製造法
JP2789084B2 (ja) * 1995-11-24 1998-08-20 勝 中原 重水素化化合物の製造方法
JP2004010550A (ja) * 2002-06-07 2004-01-15 Japan Science & Technology Corp 重水素化芳香族化合物の製造方法
TW200404054A (en) * 2002-07-26 2004-03-16 Wako Pure Chem Ind Ltd Method for deuteration of aromatic ring
TW200413273A (en) * 2002-11-15 2004-08-01 Wako Pure Chem Ind Ltd Heavy hydrogenation method of heterocyclic rings
TW200413274A (en) * 2002-12-27 2004-08-01 Wako Pure Chem Ind Ltd Deuteration or tritiation method
WO2005070853A1 (fr) * 2004-01-23 2005-08-04 Wako Pure Chemical Industries, Ltd. Procede de deuteration utilisant un catalyseur mixte
JP5464395B2 (ja) * 2008-02-01 2014-04-09 大陽日酸株式会社 重水素化された芳香環又は複素環を有する化合物の製造方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3989705A (en) * 1974-04-01 1976-11-02 Canadian Patents And Development Limited Processes for the deuteration and/or tritiation of organic substrates by hydrogen substitution
WO2011059463A1 (fr) * 2009-10-29 2011-05-19 E. I. Du Pont De Nemours And Company Composés deutérés pour des applications électroniques

Non-Patent Citations (6)

* Cited by examiner, † Cited by third party
Title
BOIX C ET AL: "Efficient H-D Exchange of Aromatic Compounds in Near-Critical D2O Catalysed by a Polymer-Supported Sulphonic Acid", TETRAHEDRON LETTERS, PERGAMON, GB, vol. 40, no. 23, 4 June 1999 (1999-06-04), pages 4433 - 4436, XP004164668, ISSN: 0040-4039, DOI: 10.1016/S0040-4039(99)00765-0 *
KAI LIU ET AL: "Solid-state deuterium NMR of imidazole ligands in cytochrome c peroxidase", JOURNAL OF THE AMERICAN CHEMICAL SOCIETY [H.W. WILSON - GS], 7 October 1998 (1998-10-07), pages 10199, XP055172193, Retrieved from the Internet <URL:http://search.proquest.com/docview/220740304> *
OBA Y ET AL: "Biosynthesis of luciferin in the sea firefly, Cypridina hilgendorfii: l-tryptophan is a component in Cypridina luciferin", TETRAHEDRON LETTERS, PERGAMON, GB, vol. 43, no. 13, 25 March 2002 (2002-03-25), pages 2389 - 2392, XP004342984, ISSN: 0040-4039, DOI: 10.1016/S0040-4039(02)00257-5 *
See also references of WO2011053334A1 *
SVETLANA V. EVCHENKO ET AL: "Efficient synthesis of deuterium-labelled ferrocenes", JOURNAL OF LABELLED COMPOUNDS AND RADIOPHARMACEUTICALS, vol. 48, no. 3, 15 March 2005 (2005-03-15), pages 209 - 218, XP055192538, ISSN: 0362-4803, DOI: 10.1002/jlcr.916 *
VAIDYANATHAN S ET AL: "Microwave mediated hydrogen deuterium exchange: a rapid synthesis of <2>H-substituted benzimidazole", TETRAHEDRON LETTERS, PERGAMON, GB, vol. 46, no. 31, 1 August 2005 (2005-08-01), pages 5195 - 5197, XP027863382, ISSN: 0040-4039, [retrieved on 20050801] *

Also Published As

Publication number Publication date
KR101538534B1 (ko) 2015-07-21
CN102574753B (zh) 2015-07-08
JP5662461B2 (ja) 2015-01-28
KR20120101029A (ko) 2012-09-12
WO2011053334A1 (fr) 2011-05-05
JP2013508360A (ja) 2013-03-07
CN102574753A (zh) 2012-07-11
EP2493835A1 (fr) 2012-09-05
TW201114735A (en) 2011-05-01

Similar Documents

Publication Publication Date Title
EP2493835A4 (fr) Procédé pour la préparation de composés aromatiques deutérés
IL214600A0 (en) Process for preparing substituted 2-nitrobiphenyls
IL220357A0 (en) Process for preparing substituted 1-o-acyl-2-deoxy-2-fluoro-4-thio-beta-d-arabinofuranoses
EP2412786A4 (fr) Procédé de production d&#39;un hydrocarbure aromatique
EP2548867A4 (fr) Procédé de préparation de diphénylurée deutérée
ZA201102424B (en) Process for preparing 2-alkyl-3-aroyl-5-nitro-benzofurans
EP2412785A4 (fr) Procédé de fabrication d&#39;hydrocarbures aromatiques
EP2534127A4 (fr) Procédé de préparation de (r)-2-acétamido-n-benzyl-3-méthoxypropionamide
SI2358674T1 (sl) Postopek za pripravo 4-(2-(2-fluorofenoksimetil)fenil)piperidinskih spojin
PT2507204E (pt) Processo para a produção de formamidas aromáticas
EP2619169A4 (fr) Procédé de préparation de bromourée
HRP20150775T1 (en) Method for preparing hypoallergens
PL2456741T3 (pl) Sposób wytwarzania fluorowanych związków olefinowych
IL218140A0 (en) Process for preparing 1-phenylpyrazoles
EP2594552A4 (fr) Procédé de préparation de la ramaline
IL208514A0 (en) Process for preparing substituted biphenylanilides
PL2595943T3 (pl) Sposób wytwarzania węglowodorów aromatycznych z metanu
IL211307A0 (en) Process for preparing cinacalcet
HK1150163A1 (en) Method for preparing trifluoromethanesulphinic acid
EP2471795A4 (fr) Procédé pour la préparation de prasugrel
IL225776A0 (en) A method for preparing combertastatin
EP2383273A4 (fr) Composé aromatique et son procédé de production
PL2271605T3 (pl) Proces wytwarzania związków fluorowych
IL207222A0 (en) Process for preparing hebivolol
EP2155759A4 (fr) Méthodes de préparation de composés de diorganozinc

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20120411

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO SE SI SK SM TR

DAX Request for extension of the european patent (deleted)
RA4 Supplementary search report drawn up and despatched (corrected)

Effective date: 20150612

RIC1 Information provided on ipc code assigned before grant

Ipc: C07C 5/00 20060101AFI20150608BHEP

Ipc: C07B 59/00 20060101ALI20150608BHEP

Ipc: C07C 15/24 20060101ALI20150608BHEP

RAP1 Party data changed (applicant data changed or rights of an application transferred)

Owner name: E. I. DU PONT DE NEMOURS AND COMPANY

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: THE APPLICATION HAS BEEN WITHDRAWN

18W Application withdrawn

Effective date: 20161027