EP1746174B1 - Aluminium alloy extruded product, method of manufacturing the same, heat exchanger multi-port tube, and method of manufacturing heat exchanger including the multi-port tube - Google Patents
Aluminium alloy extruded product, method of manufacturing the same, heat exchanger multi-port tube, and method of manufacturing heat exchanger including the multi-port tube Download PDFInfo
- Publication number
- EP1746174B1 EP1746174B1 EP06015199A EP06015199A EP1746174B1 EP 1746174 B1 EP1746174 B1 EP 1746174B1 EP 06015199 A EP06015199 A EP 06015199A EP 06015199 A EP06015199 A EP 06015199A EP 1746174 B1 EP1746174 B1 EP 1746174B1
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- EP
- European Patent Office
- Prior art keywords
- ingot
- aluminum alloy
- port tube
- heat treatment
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229910000838 Al alloy Inorganic materials 0.000 title claims description 69
- 235000012438 extruded product Nutrition 0.000 title claims description 38
- 238000004519 manufacturing process Methods 0.000 title claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 92
- 229910000765 intermetallic Inorganic materials 0.000 claims description 30
- 238000005219 brazing Methods 0.000 claims description 28
- 239000011159 matrix material Substances 0.000 claims description 27
- 238000000265 homogenisation Methods 0.000 claims description 24
- 230000007423 decrease Effects 0.000 claims description 23
- 238000005266 casting Methods 0.000 claims description 13
- 230000001747 exhibiting effect Effects 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 9
- 238000005304 joining Methods 0.000 claims description 8
- 230000008018 melting Effects 0.000 claims description 6
- 238000002844 melting Methods 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 4
- 229910052804 chromium Inorganic materials 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 claims description 2
- 229910052726 zirconium Inorganic materials 0.000 claims description 2
- 238000001125 extrusion Methods 0.000 description 34
- 229910045601 alloy Inorganic materials 0.000 description 28
- 239000000956 alloy Substances 0.000 description 28
- 238000005260 corrosion Methods 0.000 description 24
- 230000007797 corrosion Effects 0.000 description 24
- 229910052748 manganese Inorganic materials 0.000 description 20
- 229910052710 silicon Inorganic materials 0.000 description 20
- 230000003247 decreasing effect Effects 0.000 description 17
- 239000000463 material Substances 0.000 description 15
- 238000012360 testing method Methods 0.000 description 15
- 230000004907 flux Effects 0.000 description 12
- 230000000694 effects Effects 0.000 description 11
- 238000001192 hot extrusion Methods 0.000 description 11
- 239000007787 solid Substances 0.000 description 9
- 229910018473 Al—Mn—Si Inorganic materials 0.000 description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- 239000006185 dispersion Substances 0.000 description 6
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
- 238000009826 distribution Methods 0.000 description 5
- 229910052700 potassium Inorganic materials 0.000 description 5
- 239000011591 potassium Substances 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 239000000470 constituent Substances 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 description 3
- 239000001569 carbon dioxide Substances 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 238000005192 partition Methods 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 239000003507 refrigerant Substances 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 229910001635 magnesium fluoride Inorganic materials 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000007711 solidification Methods 0.000 description 2
- 230000008023 solidification Effects 0.000 description 2
- 229910018131 Al-Mn Inorganic materials 0.000 description 1
- 229910018461 Al—Mn Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000010191 image analysis Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000013077 target material Substances 0.000 description 1
- 238000009864 tensile test Methods 0.000 description 1
Images
Classifications
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F1/00—Tubular elements; Assemblies of tubular elements
- F28F1/02—Tubular elements of cross-section which is non-circular
- F28F1/022—Tubular elements of cross-section which is non-circular with multiple channels
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/08—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of copper or alloys based thereon
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F21/00—Constructions of heat-exchange apparatus characterised by the selection of particular materials
- F28F21/08—Constructions of heat-exchange apparatus characterised by the selection of particular materials of metal
- F28F21/081—Heat exchange elements made from metals or metal alloys
- F28F21/084—Heat exchange elements made from metals or metal alloys from aluminium or aluminium alloys
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F2255/00—Heat exchanger elements made of materials having special features or resulting from particular manufacturing processes
- F28F2255/16—Heat exchanger elements made of materials having special features or resulting from particular manufacturing processes extruded
Definitions
- a fourth aspect of the present invention provides a method of manufacturing an aluminum alloy extruded product exhibiting excellent surface properties, the method comprising: melting and casting an aluminum alloy having the above composition to obtain an ingot; subjecting the ingot to homogenization which includes a first-stage heat treatment in which the ingot is maintained at 550 to 650°C for two hours or more and a second-stage heat treatment in which the ingot is cooled to room temperature, heated to 400 to 500°C at an average temperature increase rate of 20 to 60°C/h, and maintained at that temperature for three hours or more; heating the ingot at 480 to 560°C; and extruding the ingot.
- a fifth aspect of the present invention provides a method of manufacturing a heat exchanger comprising extruding a heat exchanger multi-port tube using the above method, and joining the multi-port tube to a heat exchanger by brazing.
- Mg improves the strength of the alloy when contained in an amount of 0.2% or less. Moreover, when manufacturing an automotive heat exchanger by brazing using a fluoride-type flux containing potassium fluoroaluminate, excellent brazeability can be stably obtained. If the Mg content exceeds 0.2%, when manufacturing an automotive heat exchanger by brazing, a fluoride-type flux containing potassium fluoroaluminate which is melted during heating for brazing reacts with Mg in the material to produce compounds such as MgF 2 and KMgF 3 . This reduces the activity of the flux, whereby brazeability deteriorates. Moreover, the extrudability of the alloy decreases when the Mg content exceeds 0.2%.
- the first-stage heat treatment performed at a high temperature is effective for decomposing, granulating, or redissolving coarse crystals formed during casting/solidification.
- the first-stage heat treatment promotes dissolution of Mn and Si (solute elements) in the matrix. If the solid solubility of these solute elements in the matrix is high, the moving speed of dislocation in the matrix decreases, whereby the deformation resistance of the aluminum alloy increases. Therefore, the extrudability of the aluminum alloy decreases when the aluminum alloy is hot-extruded after homogenization including only the first-stage heat treatment.
- the second-stage heat treatment is performed at 400 to 500°C for three hours or more. If the temperature is less than 400°C, only a small amount of Al-Mn-Si intermetallic compounds precipitate, whereby the effect of decreasing the deformation resistance becomes insufficient. If the temperature exceeds 500°C, the intermetallic compounds precipitate to only a small extent, whereby the effect of decreasing the deformation resistance becomes insufficient. If the treatment time is less than three hours, since precipitation does not sufficiently proceed, the effect of decreasing the deformation resistance becomes insufficient. The reaction proceeds to a larger extent as the treatment time increases. On the other hand, a further effect cannot be obtained even if the treatment is performed for more than 24 hours. This is disadvantageous from the viewpoint of cost. The treatment time is still more preferably 5 to 15 hours.
- the temperature decrease rate from the first-stage heat treatment temperature to the second-stage heat treatment temperature (the temperature increase rate from room temperature to the second-stage heat treatment temperature when the billet is cooled to room temperature after the first-stage heat treatment) in order to precipitate Mn and Si dissolved in the matrix to decrease the solid solubility of Mn and Si and to achieve the above dispersion state of the intermetallic compounds.
- the average temperature decrease rate from the first-stage heat treatment temperature to the second-stage heat treatment temperature is 20 to 60°C/h.
- the heating temperature is less than 480°C, deformation resistance is increased due to too low a temperature, whereby the extrudability of the aluminum alloy is decreased.
- the heating temperature is still more preferably 480 to 530°C.
- the holding time at the above heating temperature is preferably 30 minutes or less. If the holding time exceeds 30 minutes, the intermetallic compounds precipitated during homogenization are redissolved to increase the solid solubility in the matrix. This results in an increase in deformation resistance during hot extrusion, whereby the extrudability of the aluminum alloy is decreased.
- the holding time is still more preferably 10 minutes or less.
- test specimens 1 to 5 according to the present invention exhibited excellent extrudability, did not show adhesion of deposit to the surface, and exhibited excellent brazeability, intergranular corrosion resistance, and strength.
- test specimens 6 to 9 and the test specimen 10 (known alloy) were inferior in at least one of extrudability, adhesion of deposit, strength, brazeability, and intergranular corrosion resistance.
- An aluminum alloy having the composition A shown in Table 1 was melted and cast by semicontinuous casting to obtain a billet.
- the resulting billet was homogenized under the conditions shown in Table 3.
- the billet was homogenized by increasing the temperature of the billet to a first-stage heat treatment temperature at an average temperature increase rate of 50°C/h, maintaining the billet at the first-stage heat treatment temperature, decreasing the temperature of the billet to a second-stage heat treatment temperature, maintaining the billet at the second-stage heat treatment temperature, and decreasing the temperature of the billet to 300°C at an average temperature decrease rate of 50°C/h.
- Table 3 shows the first-stage heat treatment temperature, the average temperature decrease rate from the first-stage heat treatment temperature to the second-stage heat treatment temperature, and the second-stage heat treatment temperature.
- the billet was hot-extruded under the conditions shown in Table 3 to obtain a multi-port tube shown in FIG. 1 .
- the resulting multi-port tube was used as a test specimen.
- the extrudability of the aluminum alloy during hot extrusion was evaluated in the same manner as in Example 1. Likewise, the number of deposit portions adhering to the surface of the extruded multi-port tube was calculated, and the gloss of the multi-port tube was observed. The distribution of intermetallic compounds precipitated and dispersed in the matrix was also determined.
- the multi-port tube was subjected to joining by brazing, and brazeability, tensile strength after heating for brazing, and intergranular corrosion susceptibility were evaluated. The results are shown in Table 4. In Tables 3 and 4, values outside the conditions according to the present invention are underlined.
- test specimens 11 to 15 homogenized under the conditions outside the conditions according to the present invention were inferior in at least one of extrudability, number of deposit portions, strength, brazeability, and intergranular corrosion resistance.
- An aluminum alloy containing 0.6% of Si, 0.2% of Fe, and 1.0% of Mn (Mn%/Si%: 1.7) was melted and cast by semicontinuous casting to obtain a billet.
- the resulting billet was homogenized under the conditions shown in Table 5.
- the billet was homogenized by increasing the temperature of the billet to a first-stage heat treatment temperature at an average temperature increase rate of 50°C/h, maintaining the billet at the first-stage heat treatment temperature, decreasing the temperature of the billet to room temperature, increasing the temperature of the billet to a second-stage heat treatment temperature, maintaining the billet at the second-stage heat treatment temperature, and decreasing the temperature of the billet to 300°C at an average temperature decrease rate of 50°C/h.
- the extrudability of the aluminum alloy during hot extrusion was evaluated in the same manner as in Example 1. Likewise, the number of deposit portions adhering to the surface of the extruded multi-port tube was calculated, and the gloss of the multi-port tube was observed. The distribution of intermetallic compounds precipitated and dispersed in the matrix was also determined.
- the multi-port tube was subjected to joining by brazing, and brazeability, tensile strength after heating for brazing, and intergranular corrosion susceptibility were evaluated. The results are shown in Table 6. In Tables 5 and 6, values outside the conditions according to the present invention are underlined.
- test specimen 16 according to the present invention exhibited excellent extrudability, did not show adhesion of deposit to the surface, and exhibited excellent brazeability, intergranular corrosion resistance, and strength.
- test specimens 17 to 21 were inferior in at least one of extrudability, adhesion of deposit, strength, brazeability, and intergranular corrosion resistance.
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- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Geometry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Extrusion Of Metal (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2005212069A JP4824358B2 (ja) | 2005-07-22 | 2005-07-22 | 表面性状に優れたアルミニウム合金押出材とその製造方法、および熱交換器用多孔管ならびに該多孔管を組み込んだ熱交換器の製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1746174A1 EP1746174A1 (en) | 2007-01-24 |
EP1746174B1 true EP1746174B1 (en) | 2008-06-25 |
Family
ID=37188799
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP06015199A Active EP1746174B1 (en) | 2005-07-22 | 2006-07-21 | Aluminium alloy extruded product, method of manufacturing the same, heat exchanger multi-port tube, and method of manufacturing heat exchanger including the multi-port tube |
Country Status (5)
Country | Link |
---|---|
US (2) | US20070017605A1 (zh) |
EP (1) | EP1746174B1 (zh) |
JP (1) | JP4824358B2 (zh) |
CN (1) | CN100582274C (zh) |
DE (1) | DE602006001552D1 (zh) |
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EP1983272A1 (en) * | 2007-04-18 | 2008-10-22 | Aic S.A. | Fired heat exchanger bundle |
JP5409125B2 (ja) * | 2009-05-29 | 2014-02-05 | アイシン軽金属株式会社 | 耐scc性に優れる7000系アルミニウム合金押出材及びその製造方法 |
JP5632140B2 (ja) * | 2009-06-24 | 2014-11-26 | 株式会社Uacj | アルミニウム合金製自動車用熱交換器およびその製造方法 |
JP5614829B2 (ja) * | 2009-06-24 | 2014-10-29 | 株式会社Uacj | アルミニウム合金製熱交換器 |
CN101713039B (zh) * | 2009-09-29 | 2011-08-24 | 金龙精密铜管集团股份有限公司 | 一种铝合金及其制品 |
US8313590B2 (en) * | 2009-12-03 | 2012-11-20 | Rio Tinto Alcan International Limited | High strength aluminium alloy extrusion |
JP5750237B2 (ja) | 2010-05-25 | 2015-07-15 | 株式会社Uacj | アルミニウム合金製熱交換器の製造方法 |
JP5670100B2 (ja) * | 2010-05-25 | 2015-02-18 | 株式会社Uacj | アルミニウム合金製熱交換器の製造方法 |
EP2514555A1 (en) | 2011-04-21 | 2012-10-24 | Aleris Aluminum Koblenz GmbH | Extruded aluminium alloy tube product |
JP5916314B2 (ja) * | 2011-08-12 | 2016-05-11 | 三菱アルミニウム株式会社 | 熱交換器用アルミニウム合金製タンク等の押出パイプ部材 |
JP5906113B2 (ja) | 2012-03-27 | 2016-04-20 | 三菱アルミニウム株式会社 | 熱交換器用押出伝熱管と熱交換器および熱交換器用押出伝熱管の製造方法 |
US20150075756A1 (en) * | 2012-03-28 | 2015-03-19 | Carrier Corporation | Surface treatment for corrosion resistance of aluminum |
CN102796976B (zh) * | 2012-08-22 | 2014-05-28 | 北京有色金属研究总院 | 一种改善含Zr的7xxx系铝合金组织与性能的阶段均匀化热处理方法 |
US10661395B2 (en) | 2014-07-30 | 2020-05-26 | Uacj Corporation | Aluminum-alloy brazing sheet |
WO2016056306A1 (ja) * | 2014-10-09 | 2016-04-14 | 株式会社Uacj | アルミニウム合金ブレージングシートおよびろう付け方法 |
WO2016093017A1 (ja) | 2014-12-11 | 2016-06-16 | 株式会社Uacj | ろう付方法 |
CN104858260B (zh) * | 2015-05-26 | 2016-08-17 | 中南大学 | 一种超长铝镁合金管的制备方法 |
JP6799951B2 (ja) * | 2015-08-11 | 2020-12-16 | 株式会社Uacj | 内面防食性に優れたアルミニウム押出扁平多穴管及びそれを用いてなるアルミニウム製熱交換器 |
CN105202960A (zh) * | 2015-10-10 | 2015-12-30 | 安陆火凤凰铝材有限责任公司 | 一种铝管式换热器 |
JP6186455B2 (ja) | 2016-01-14 | 2017-08-23 | 株式会社Uacj | 熱交換器及びその製造方法 |
ES2870139T3 (es) | 2016-04-29 | 2021-10-26 | Rio Tinto Alcan Int Ltd | Aleación resistente a la corrosión para productos extruidos y soldados con soldadura fuerte |
JP6263574B2 (ja) | 2016-05-30 | 2018-01-17 | 株式会社Uacj | ブレージングシート及びその製造方法並びにアルミニウム構造体のろう付方法 |
JP6312968B1 (ja) | 2016-11-29 | 2018-04-18 | 株式会社Uacj | ブレージングシート及びその製造方法 |
JPWO2018147375A1 (ja) * | 2017-02-13 | 2019-12-12 | 株式会社Uacj | ろう付け性及び外面防食性に優れたアルミニウム押出扁平多穴管及びそれを用いてなるアルミニウム製熱交換器 |
JP7053281B2 (ja) | 2017-03-30 | 2022-04-12 | 株式会社Uacj | アルミニウム合金クラッド材及びその製造方法 |
JP6916715B2 (ja) | 2017-11-08 | 2021-08-11 | 株式会社Uacj | ブレージングシート及びその製造方法 |
DE112019004536T5 (de) | 2018-09-11 | 2021-06-02 | Uacj Corporation | Verfahren zum herstellen eines hartlotblechs |
CN111647774A (zh) * | 2020-02-17 | 2020-09-11 | 海德鲁挤压解决方案股份有限公司 | 生产耐腐蚀和耐高温材料的方法 |
JP2021195582A (ja) * | 2020-06-11 | 2021-12-27 | 株式会社Uacj | 熱交換器用アルミニウム合金押出多穴チューブ及びその製造方法 |
CN111876675A (zh) * | 2020-07-08 | 2020-11-03 | 甘肃酒钢集团宏兴钢铁股份有限公司 | 一种低成本高层建筑结构用钢板及其生产方法 |
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JP2004339582A (ja) * | 2003-05-16 | 2004-12-02 | Mitsubishi Alum Co Ltd | 熱交換器用チューブ及び熱交換器 |
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2005
- 2005-07-22 JP JP2005212069A patent/JP4824358B2/ja active Active
-
2006
- 2006-07-20 US US11/489,941 patent/US20070017605A1/en not_active Abandoned
- 2006-07-21 EP EP06015199A patent/EP1746174B1/en active Active
- 2006-07-21 DE DE602006001552T patent/DE602006001552D1/de active Active
- 2006-07-24 CN CN200610107433.2A patent/CN100582274C/zh active Active
-
2011
- 2011-01-18 US US12/930,793 patent/US20110114228A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
US20070017605A1 (en) | 2007-01-25 |
EP1746174A1 (en) | 2007-01-24 |
JP2007031730A (ja) | 2007-02-08 |
US20110114228A1 (en) | 2011-05-19 |
DE602006001552D1 (de) | 2008-08-07 |
CN100582274C (zh) | 2010-01-20 |
JP4824358B2 (ja) | 2011-11-30 |
CN1900335A (zh) | 2007-01-24 |
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