EP1330555A4 - Lösungsmittelextraktionsverfahren zur nickel- und cobaltgewinnung aus auslauglösungen - Google Patents

Lösungsmittelextraktionsverfahren zur nickel- und cobaltgewinnung aus auslauglösungen

Info

Publication number
EP1330555A4
EP1330555A4 EP01973802A EP01973802A EP1330555A4 EP 1330555 A4 EP1330555 A4 EP 1330555A4 EP 01973802 A EP01973802 A EP 01973802A EP 01973802 A EP01973802 A EP 01973802A EP 1330555 A4 EP1330555 A4 EP 1330555A4
Authority
EP
European Patent Office
Prior art keywords
cobalt
extraction process
solvent extraction
recovering nickel
leach solutions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP01973802A
Other languages
English (en)
French (fr)
Other versions
EP1330555A1 (de
Inventor
Chu Yong Cheng
Martin Houchin
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Commonwealth Scientific and Industrial Research Organization CSIRO
Original Assignee
Commonwealth Scientific and Industrial Research Organization CSIRO
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from AUPR0169A external-priority patent/AUPR016900A0/en
Priority claimed from AUPR1119A external-priority patent/AUPR111900A0/en
Application filed by Commonwealth Scientific and Industrial Research Organization CSIRO filed Critical Commonwealth Scientific and Industrial Research Organization CSIRO
Publication of EP1330555A1 publication Critical patent/EP1330555A1/de
Publication of EP1330555A4 publication Critical patent/EP1330555A4/de
Withdrawn legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00Obtaining nickel or cobalt
    • C22B23/04Obtaining nickel or cobalt by wet processes
    • C22B23/0453Treatment or purification of solutions, e.g. obtained by leaching
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/38Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
    • C22B3/384Pentavalent phosphorus oxyacids, esters thereof
    • C22B3/3842Phosphinic acid, e.g. H2P(O)(OH)
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00Obtaining nickel or cobalt
    • C22B23/04Obtaining nickel or cobalt by wet processes
    • C22B23/0476Separation of nickel from cobalt
    • C22B23/0484Separation of nickel from cobalt in acidic type solutions
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32Carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/38Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
    • C22B3/384Pentavalent phosphorus oxyacids, esters thereof
    • C22B3/3846Phosphoric acid, e.g. (O)P(OH)3
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
EP01973802A 2000-09-15 2001-09-14 Lösungsmittelextraktionsverfahren zur nickel- und cobaltgewinnung aus auslauglösungen Withdrawn EP1330555A4 (de)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
AUPR0169A AUPR016900A0 (en) 2000-09-15 2000-09-15 Separqtion of manganese from cobalt and nickel by solvent extraction
AUPR016900 2000-09-15
AUPR111900 2000-10-30
AUPR1119A AUPR111900A0 (en) 2000-10-30 2000-10-30 Solvent extraction process for directly recovering nickel and cobalt from leach solutions
PCT/AU2001/001161 WO2002022896A1 (en) 2000-09-15 2001-09-14 Solvent extraction process for recovering nickel and cobalt from leach solutions

Publications (2)

Publication Number Publication Date
EP1330555A1 EP1330555A1 (de) 2003-07-30
EP1330555A4 true EP1330555A4 (de) 2005-08-31

Family

ID=25646443

Family Applications (1)

Application Number Title Priority Date Filing Date
EP01973802A Withdrawn EP1330555A4 (de) 2000-09-15 2001-09-14 Lösungsmittelextraktionsverfahren zur nickel- und cobaltgewinnung aus auslauglösungen

Country Status (5)

Country Link
US (1) US20040050212A1 (de)
EP (1) EP1330555A4 (de)
CA (1) CA2421970A1 (de)
CU (1) CU23103A3 (de)
WO (1) WO2002022896A1 (de)

Families Citing this family (36)

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Publication number Priority date Publication date Assignee Title
AU2005209326B2 (en) * 2004-01-28 2010-08-19 Commonwealth Scientific And Industrial Research Organisation Solvent extraction process for separating cobalt and/or manganese from impurities in leach solutions
EP1716262A4 (de) 2004-01-28 2008-08-13 Commw Scient Ind Res Org Lösungsmittelextraktionsverfahren zur abtrennung von cobalt und/oder nickel aus auslaugungslösungen
BRPI0515145A (pt) * 2004-09-13 2008-07-08 Canopean Pty Ltd processo para preparação de solução de extraente orgánica carregada com nìquel
EP1880029B1 (de) * 2005-05-13 2012-07-04 BHP Billiton SSM Development Pty Ltd Verbessertes verfahren zur haufenauslaugung von nickelhaltigen oxidischen erzen
FI120943B (fi) * 2008-02-19 2010-05-14 Norilsk Nickel Finland Oy Menetelmä sinkin, raudan, kalsiumin, kuparin ja mangaanin erottamiseksi koboltin ja/tai nikkelin vesiliuoksista
TWI401213B (zh) * 2010-02-02 2013-07-11 廢加氫脫硫觸媒中鎳鈷精礦資源化回收方法
US8979976B2 (en) 2010-05-20 2015-03-17 Cesl Limited Solvent extraction process for separating cobalt from nickel in aqueous solution
CN102206834B (zh) * 2011-05-03 2012-12-26 四川省尼科国润新材料有限公司 一种用低冰镍直接生产电解镍的方法
CN102864305A (zh) * 2011-07-08 2013-01-09 浙江盈联科技有限公司 一种钴铜合金浸出液的分离净化工艺
AU2012330140B2 (en) * 2011-10-24 2017-08-31 Sumitomo Metal Mining Co., Ltd. Method for producing high-purity cobalt sulfate aqueous solution
US9896740B2 (en) * 2012-01-13 2018-02-20 Sumitomo Metal Mining Co., Ltd. Method for operating flash vessel
CN104263928B (zh) * 2014-09-05 2016-06-08 昆明理工大学 一种超重力场下溶剂萃取分离镍钴的方法
CN104445424A (zh) * 2014-11-12 2015-03-25 浙江华友钴业股份有限公司 一种含锰废液制取高纯硫酸锰的方法
CN104724864A (zh) * 2015-03-31 2015-06-24 江苏地一环保科技有限公司 一种含镍电镀废水的旋流处理工艺
JP2015212424A (ja) * 2015-07-24 2015-11-26 住友金属鉱山株式会社 硫酸コバルトの製造方法
CN106906369B (zh) * 2015-12-22 2018-10-26 北京有色金属研究总院 一种利用协同萃取技术从重金属废水中回收铜、锌、镍、镉的工艺
CN105692753A (zh) * 2016-02-26 2016-06-22 兰州金川新材料科技股份有限公司 一种含钴酸性废水的处理方法
JP6759882B2 (ja) * 2016-09-05 2020-09-23 住友金属鉱山株式会社 ニッケル、コバルトを含有する溶液の製造方法
CN107904402B (zh) * 2017-10-18 2019-11-22 江苏理工学院 一种分离钴锰废料中钴和锰的方法
CN107841623A (zh) * 2017-10-20 2018-03-27 昆明理工大学 一种利用微流体技术从镍钴溶液中萃取分离锰、锌的方法
JP6766838B2 (ja) * 2018-03-12 2020-10-14 住友金属鉱山株式会社 溶媒抽出方法
CN109097599B (zh) * 2018-09-27 2021-06-04 中南大学 一种协同萃取分离锰与钙、镁的方法
CN109777954B (zh) * 2019-03-13 2021-01-05 荆门市格林美新材料有限公司 一种矿液中离子的提取方法
US11359260B2 (en) * 2019-09-04 2022-06-14 Korea Resources Corporation Method of inhibiting degradation of extractant by anhydrous environment avoiding and metal stripping
CN111187907B (zh) * 2020-02-20 2022-02-08 中国恩菲工程技术有限公司 硫酸锰溶液的提纯方法
CN111206154B (zh) * 2020-02-25 2021-11-02 中国科学院过程工程研究所 一种分离回收废旧三元电池材料中有价金属离子的方法
CN112342387A (zh) * 2020-10-21 2021-02-09 北京博萃循环科技有限公司 一种镍和镁的分离方法及其应用
CN112375912B (zh) * 2020-11-12 2022-02-01 济南大学 一种利用双膦酸类萃取剂从电镀废液中回收镍的方法
CN112458281A (zh) * 2020-11-24 2021-03-09 北京博萃循环科技有限公司 一种利用含镍镁废液制备镍盐的方法
CN112430733A (zh) * 2020-11-30 2021-03-02 北京博萃循环科技有限公司 一种处理红土镍矿的方法
EP4337802A1 (de) * 2021-05-13 2024-03-20 Commonwealth Scientific and Industrial Research Organisation Herstellung von hochreinen nickel- und kobaltverbindungen
GB202108372D0 (en) * 2021-06-11 2021-07-28 Johnson Matthey Plc A recycling method for battery and catalyst materials
US20240102128A1 (en) * 2022-04-19 2024-03-28 Ecopro Materials, Co., Ltd. Solvent extraction method for separation and recovery of nickel, cobalt, manganese, and zinc
CN114774689B (zh) * 2022-05-26 2023-10-31 重庆康普化学工业股份有限公司 一种含有机氧化膦类萃取剂的镍钴协萃体系的萃取剂以及镍钴萃取方法
WO2024042115A1 (en) * 2022-08-24 2024-02-29 Umicore Process for preparing a high-purity nickel sulphate solution
CN115893497A (zh) * 2022-11-14 2023-04-04 广东邦普循环科技有限公司 一种从含钙铜铬硅的锰溶液中制备高纯硫酸锰的方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4528167A (en) * 1981-11-03 1985-07-09 Council For Mineral Technology Selective solvent extraction using organophosphorus and carboxylic acids and a non-chelating aldehyde oxime
AU4089096A (en) * 1995-01-09 1996-07-18 Lionore Australia (Avalon) Pty Ltd The recovery of nickel and cobalt from lateritic ores
WO1998056482A1 (en) * 1997-06-12 1998-12-17 Wmc Resources Limited Pre-equilibration of a cationic extractant

Family Cites Families (4)

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US3455680A (en) * 1966-03-03 1969-07-15 Canadian Patents Dev Mixed extractant and process for separating copper from cobalt and nickel in acid medium
US5228903A (en) * 1990-04-18 1993-07-20 The Curators Of The University Of Missouri Of Columbia Method for stripping metals in solvent extraction
ZA94949B (en) * 1993-03-26 1994-08-25 Mintek The production of cadmium
US6231823B1 (en) * 2000-03-27 2001-05-15 Dynatec Corporation Solvent extraction process for the separation of cobalt from nickel in aqueous sulphate-containing solutions

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4528167A (en) * 1981-11-03 1985-07-09 Council For Mineral Technology Selective solvent extraction using organophosphorus and carboxylic acids and a non-chelating aldehyde oxime
AU4089096A (en) * 1995-01-09 1996-07-18 Lionore Australia (Avalon) Pty Ltd The recovery of nickel and cobalt from lateritic ores
WO1998056482A1 (en) * 1997-06-12 1998-12-17 Wmc Resources Limited Pre-equilibration of a cationic extractant

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
"Nickel/Cobalt Pressure Leaching & Hydrometallurgy Forum, May 1997, Perth, Western Australia", 1997, ALTA METALLURGICAL SERVICES, AUSTRALIA, XP001206859 *
DEVI N B ET AL: "SODIUM SALTS OF D2EHPA, PC-88A AND CYANEX-272 AND THEIR MIXTURES ASEXTRACTANTS FOR COBALT (II)", HYDROMETALLURGY, ELSEVIER SCIENTIFIC PUBLISHING CY. AMSTERDAM, NL, vol. 34, no. 3, January 1994 (1994-01-01), pages 331 - 342, XP000430416, ISSN: 0304-386X *
PRESTON J S ET AL: "SYNERGISTIC EFFECTS IN THE SOLVENT EXTRACTION OF SOME DIVALENT METALS BY MIXTURES OF VERSATIC 10 ACID AND PYRIDINECARBOXYLATE EXTERS", JOURNAL OF CHEMICAL TECHNOLOGY AND BIOTECHNOLOGY. (INTERNATIONAL JOURNAL OF BIOTECHNICAL AND CHEMICAL PROCESSES), ELSEVIER APPLIED SCIENCE PUBLISHERS. BARKING, GB, vol. 61, no. 2, 1 October 1994 (1994-10-01), pages 159 - 165, XP000469822, ISSN: 0268-2575 *
See also references of WO0222896A1 *

Also Published As

Publication number Publication date
CA2421970A1 (en) 2002-03-21
EP1330555A1 (de) 2003-07-30
CU23103A3 (es) 2005-12-20
WO2002022896A1 (en) 2002-03-21
US20040050212A1 (en) 2004-03-18

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