EP1065309A4 - Verfahren zur flammfestausrichtung von textilmaterialien - Google Patents

Verfahren zur flammfestausrichtung von textilmaterialien

Info

Publication number
EP1065309A4
EP1065309A4 EP98920746A EP98920746A EP1065309A4 EP 1065309 A4 EP1065309 A4 EP 1065309A4 EP 98920746 A EP98920746 A EP 98920746A EP 98920746 A EP98920746 A EP 98920746A EP 1065309 A4 EP1065309 A4 EP 1065309A4
Authority
EP
European Patent Office
Prior art keywords
mixture
materials
flame
water
retardant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP98920746A
Other languages
English (en)
French (fr)
Russian (ru)
Other versions
EP1065309A1 (de
EP1065309B1 (de
Inventor
Nina Sergeevna Zubkova
Nataliya Grigorievna Butylkina
Alexandr Alexandrovich Berlin
Nikolai Alexandro Khalturinsky
Leonid Semenovich Galbraikh
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Isle Firestop Ltd
Original Assignee
Isle Firestop Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Isle Firestop Ltd filed Critical Isle Firestop Ltd
Priority to PT98920746T priority Critical patent/PT1065309E/pt
Publication of EP1065309A1 publication Critical patent/EP1065309A1/de
Publication of EP1065309A4 publication Critical patent/EP1065309A4/de
Application granted granted Critical
Publication of EP1065309B1 publication Critical patent/EP1065309B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D161/00—Coating compositions based on condensation polymers of aldehydes or ketones; Coating compositions based on derivatives of such polymers
    • C09D161/20—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
    • C09D161/26—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds
    • C09D161/28—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds with melamine
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402—Amides imides, sulfamic acids
    • D06M13/425—Carbamic or thiocarbamic acids or derivatives thereof, e.g. urethanes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/44—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen containing nitrogen and phosphorus
    • D06M13/447—Phosphonates or phosphinates containing nitrogen atoms
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/39—Aldehyde resins; Ketone resins; Polyacetals
    • D06M15/423—Amino-aldehyde resins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/39—Aldehyde resins; Ketone resins; Polyacetals
    • D06M15/423—Amino-aldehyde resins
    • D06M15/43—Amino-aldehyde resins modified by phosphorus compounds
    • D06M15/432—Amino-aldehyde resins modified by phosphorus compounds by phosphonic acids or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/693—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural or synthetic rubber, or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/30—Flame or heat resistance, fire retardancy properties

Definitions

  • the invention is available on the basis of technology for the manufacture of suitable products, including reactive materials with reduced combustibility, small combustible gas, and Chemicals and heavy materials are used in a variety of ways, including for the manufacture of motor vehicles, which are used in automobiles.
  • suitable products including reactive materials with reduced combustibility, small combustible gas, and Chemicals and heavy materials are used in a variety of ways, including for the manufacture of motor vehicles, which are used in automobiles.
  • Commercials, residences, hospitals Widespread materials are used in everyday life and for the manufacture of work clothing for all practical purposes.
  • the intentionally released chemical fibers and high-temperature materials are highly inflammable. They have a low self-ignition temperature and a high burning rate.
  • Izves ⁇ na ⁇ gnezaschi ⁇ naya ⁇ m ⁇ zitsiya (Zayav ⁇ a ⁇ eli ⁇ b ⁇ i ⁇ anii 2,273,720) for ⁇ b ⁇ ab ⁇ i ⁇ aney, ne ⁇ any ⁇ ma ⁇ e ⁇ ial ⁇ v and ⁇ v ⁇ vy ⁇ products ⁇ eds ⁇ avlyayuschaya s ⁇ b ⁇ y v ⁇ dny ⁇ as ⁇ v ⁇ ne ⁇ ganiches ⁇ i ⁇ s ⁇ ley ( ⁇ s ⁇ a ⁇ amm ⁇ niya, sul ⁇ a ⁇ amm ⁇ niya, b ⁇ mid amm ⁇ niya and i ⁇ ⁇ liches ⁇ ve mixture in 12-20% of s ⁇ s ⁇ ave ⁇ m ⁇ zitsii) and mine ⁇ aln ⁇ y ⁇ isl ⁇ y ( sulfuric acid - 0.4-0.6% of the mass in the composition of the company), which contributes to the increase in the volume of the material and
  • 28 Save 282, 330, 334 on the basis of ammonia treatment units (Combustion retardant converter. ⁇ Budapest ⁇ ⁇ . ⁇ . Comprising ⁇
  • 282 includes a mod- ified small-sized window with 10% of ammonia in combination with melamine and penta-emulsion at a ratio of 1: 1.
  • concentration of the indicated mixture in the aqueous suspension used for the processing of textiles is 500 g / l.
  • composition of a solid substance is 50%.
  • the composition of the Compound 334 includes a modified ammonia unit. Used for absorbing wood, paper and textile. For all specified products, a flame-retardant effect is achieved by introducing combustion retardants into the material in the amount of 30-40%, which results in the deterioration of physical hazards.
  • thermo- (hydroxymethyl) -functional compounds The methods of disintegration of cellulose materials, known on the basis of the use of thermo- (hydroxymethyl) -functional compounds, are known to For ⁇ idaniya ⁇ gnes ⁇ y ⁇ s ⁇ i tsellyul ⁇ znym ma ⁇ e ⁇ ialam ⁇ e ⁇ mu s ⁇ s ⁇ bu ⁇ edva ⁇ i ⁇ eln ⁇ ⁇ v ⁇ di ⁇ sya ⁇ tsess ⁇ li ⁇ ndensatsii between ⁇ S and m ⁇ chevin ⁇ y ⁇ i m ⁇ ln ⁇ m s ⁇ n ⁇ shenii ⁇ m ⁇ nen ⁇ v 1: 1.
  • Patent No. 178 4732789 provides a two-stage process for the processing of containers from a mixture of carbon and polyethylene. Initially, the fabric processes the “God” method, and then for the flameproof or impaired utility there is a utility The fabricated fabric is vulcanized, therefore, in the case of the use of a hexabsamide, it is heated above 182 ° C to melt the flame retardant. The two-stage process and the need for vulcanization, and the high temperature of the process, significantly complicate the use of the unit.
  • the low cost of the product is the low efficiency of the flame retardant for fabrics from a mixture of cellulose and synthetic fibers.
  • a flame retardant has been described which is susceptible to malfunctioning of diamide, which is associated with an increased incidence of diabetes
  • the use of the specified system allows you to receive flame retardant materials from a mixture of cellulose and synthetic waves.
  • the disadvantages of the aforementioned system are: low hydraulic stability of the diamide, metabolic acid, and instability of the aedea of the medium ⁇ 99/41446 ⁇ / ⁇ glycazine (the development of a foreign product, which is favorable for a low-cost industry) Unprotected textile materials can be obtained only with a large content of the combustion retardant on the stove (up to 30% of the material weight).
  • the first aspect of this invention is the production of a flameproof process, which includes the following inquiries:
  • the material can still be washed and dried after processing.
  • Places of resin of melamine type for use in materials at the 1st stage of the process of impregnation may be replaced by brown compounds. Otherwise, these substances (see the melamine type and the most recent interconnections) may be used together.
  • non-hazardous substances may be introduced into the fireproof system.
  • NI is an acid index, the minimum content of oxygen in a mixture with nitrogen, and when it is consumed, a stable combustion of the sample is observed: ⁇ 12.1.044-89). ⁇ ⁇ ° 2.
  • ⁇ I 30.0%. 14.
  • the modified container was choked at a yield of 33.7%, and 160 mm of water was supplied to the plant.

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Fireproofing Substances (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)
  • Surface Treatment Of Glass Fibres Or Filaments (AREA)
  • Macromonomer-Based Addition Polymer (AREA)
EP98920746A 1998-02-13 1998-02-13 Verfahren zur flammfestausrichtung von textilmaterialien Expired - Lifetime EP1065309B1 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PT98920746T PT1065309E (pt) 1998-02-13 1998-02-13 Metodo para o processamento retardador de chama de materiais texteis

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/RU1998/000031 WO1999041446A1 (fr) 1998-02-13 1998-02-13 Procede de traitement ignifuge de materiaux textiles

Publications (3)

Publication Number Publication Date
EP1065309A1 EP1065309A1 (de) 2001-01-03
EP1065309A4 true EP1065309A4 (de) 2001-05-23
EP1065309B1 EP1065309B1 (de) 2003-07-30

Family

ID=20130190

Family Applications (1)

Application Number Title Priority Date Filing Date
EP98920746A Expired - Lifetime EP1065309B1 (de) 1998-02-13 1998-02-13 Verfahren zur flammfestausrichtung von textilmaterialien

Country Status (13)

Country Link
US (1) US6541068B1 (de)
EP (1) EP1065309B1 (de)
JP (1) JP4057239B2 (de)
CN (1) CN1154763C (de)
AT (1) ATE246279T1 (de)
AU (1) AU740774B2 (de)
BR (1) BR9815665A (de)
CA (1) CA2320145C (de)
DE (1) DE69816873T2 (de)
DK (1) DK1065309T3 (de)
EA (1) EA002141B1 (de)
ES (1) ES2203950T3 (de)
WO (1) WO1999041446A1 (de)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE202004012978U1 (de) * 2003-11-29 2004-11-11 Bodet & Horst Gmbh & Co. Kg Schutzbezug für Bettwaren bzw. mit Schutzbezug ausgestattete Bettware
GB2470567A (en) * 2009-05-27 2010-12-01 Rhodia Operations Treatment of Textile Materials
SE534276C2 (sv) * 2009-08-06 2011-06-28 Miljoeslaeckning I Alingsaas Ab Vattenhaltig sammansättning och metod för brandkontroll
DE102010054341B3 (de) * 2010-09-27 2012-01-26 Lufthansa Technik Ag Verfahren zum Aufbringen einer brandschützenden Beschichtung auf ein Substrat und Substrat mit brandschützender Beschichtung
CN102465452A (zh) * 2010-11-15 2012-05-23 香港纺织及成衣研发中心 纤维素织物的阻燃整理方法及得到的织物
US20130130417A1 (en) 2011-11-22 2013-05-23 Jar-Yu WU Manufacturing method of a light-emitting device
CN102094339A (zh) * 2010-11-30 2011-06-15 吴江市凌志纺织有限公司 一种防火防水复合面料
CN102295616B (zh) * 2011-05-18 2013-09-04 杨彦威 具有多羟基结构的氨基树脂及其制备方法
RU2487205C1 (ru) * 2012-03-29 2013-07-10 Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Волгоградский государственный технический университет" (ВолгГТУ) Способ модификации полиэфирных волокон
US9919174B2 (en) 2012-09-30 2018-03-20 Flame Security Sweden Ab Aqueous composition comprising phosphorous and nitrogen for general fire control
CN103113317B (zh) * 2013-02-02 2015-07-29 杨彦威 三甲氧基三丙醇氧基醚化氨基树脂及其制备方法和应用
CN103161074B (zh) * 2013-02-04 2015-03-11 华南理工大学 一种用于织物后整理的含磷、氮、硅阻燃剂及其制备方法
WO2015025948A1 (ja) 2013-08-23 2015-02-26 株式会社カネカ 難燃性布帛、その製造方法、及びそれを含む防火服
CN108505323B (zh) * 2018-04-10 2020-10-27 中国科学技术大学 一种超疏水疏油阻燃涂层整理基材的方法
CN112359597B (zh) * 2020-12-07 2022-02-18 东华大学 一种有机/无机杂化薄膜包覆棉纺织品及其制备方法

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GB1317468A (en) * 1969-09-30 1973-05-16 Cotton Producers Inst Process for rendering cellulosic textile material flame retardant
US3632297A (en) * 1970-03-12 1972-01-04 Stevens & Co Inc J P Process for rendering cellulose-containing fabrics durably flame-retardant by wet-curing a melamine resin and a phosphoric acid amide on the fabric
BE788586A (fr) * 1971-09-10 1973-03-08 Ciba Geigy Procede d'obtention de produits de condensation contenant du phosphore,les produits obtenus et leur utilisation comme agent ignifuges
DE2253663A1 (de) * 1972-11-02 1974-05-16 Hoechst Ag Amidgruppen enthaltende phosphorverbindungen und deren verwendung als flammenschutzmittel
CA1000457A (en) * 1972-11-27 1976-11-30 Marshall W. Duke Fire retardant fabrics and method for preparation thereof
SU632702A1 (ru) * 1977-05-31 1978-11-15 Московский Ордена Трудового Красного Знамени Текстильный Институт Замещенный диамид этилфосфоновой кислоты в качестве антипирена
SU1427017A1 (ru) * 1986-06-25 1988-09-30 Московский Текстильный Институт Им.А.Н.Косыгина Состав дл огнезащитной обработки текстильных материалов
FR2707308B1 (fr) * 1993-07-09 1995-09-29 Protex Manuf Prod Chimiq Procédé d'ignifugation non permanent de textiles à l'aide de solutions de sels d'acides alkylaminométhylènephosphoniques.

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No further relevant documents disclosed *

Also Published As

Publication number Publication date
CN1285014A (zh) 2001-02-21
CA2320145A1 (en) 1999-08-19
CA2320145C (en) 2007-06-12
JP4057239B2 (ja) 2008-03-05
DE69816873T2 (de) 2004-05-27
EP1065309A1 (de) 2001-01-03
JP2002503771A (ja) 2002-02-05
DE69816873D1 (de) 2003-09-04
AU7352198A (en) 1999-08-30
EP1065309B1 (de) 2003-07-30
ATE246279T1 (de) 2003-08-15
EA200000794A1 (ru) 2000-12-25
WO1999041446A8 (fr) 2001-02-22
AU740774B2 (en) 2001-11-15
US6541068B1 (en) 2003-04-01
DK1065309T3 (da) 2003-11-24
EA002141B1 (ru) 2001-12-24
ES2203950T3 (es) 2004-04-16
WO1999041446A1 (fr) 1999-08-19
CN1154763C (zh) 2004-06-23
BR9815665A (pt) 2000-10-17

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