EP0838289B1 - Verfahren zur Herstellung massiver Magnetkörper - Google Patents

Verfahren zur Herstellung massiver Magnetkörper Download PDF

Info

Publication number
EP0838289B1
EP0838289B1 EP97117634A EP97117634A EP0838289B1 EP 0838289 B1 EP0838289 B1 EP 0838289B1 EP 97117634 A EP97117634 A EP 97117634A EP 97117634 A EP97117634 A EP 97117634A EP 0838289 B1 EP0838289 B1 EP 0838289B1
Authority
EP
European Patent Office
Prior art keywords
die
alloy
magnet bodies
hydrogen
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP97117634A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP0838289A1 (de
Inventor
Stefan Dr. Roth
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Institut fuer Festkoerper und Werkstofforschung Dresden eV
Original Assignee
Institut fuer Festkoerper und Werkstofforschung Dresden eV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institut fuer Festkoerper und Werkstofforschung Dresden eV filed Critical Institut fuer Festkoerper und Werkstofforschung Dresden eV
Publication of EP0838289A1 publication Critical patent/EP0838289A1/de
Application granted granted Critical
Publication of EP0838289B1 publication Critical patent/EP0838289B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/12Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
    • H01F1/14Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
    • H01F1/147Alloys characterised by their composition

Definitions

  • the invention relates to a method for producing massive Magnetic body made of materials with soft magnetic Properties using the die casting process.
  • the method is applicable for the production of soft magnetic Magnetic bodies for relays, transformers, solenoid valves, actuators and other electromagnetic products.
  • the invention is based on the object of a method create with the massive magnetic body made of materials soft magnetic properties using the Die casting process can be produced efficiently.
  • the process is characterized in that An alloy is used as the starting material Alloy components of the soft magnetic material and additionally one or more of the melting point depressants Elements consist of boron, carbon and phosphorus.
  • the added additional elements in such an amount that the Melting point of the soft magnetic material to a Temperature ⁇ 1400 ° C, preferably ⁇ 1300 ° C is lowered.
  • the die-cast from this alloy Magnetic bodies are then retrofitted using a Heat treatment in a reactive atmosphere the additional Elements at least partially removed.
  • the die-cast magnetic body can be used for the heat treatment
  • Hydrogen can be used as a reactive atmosphere. It is it is advantageous if the hydrogen atmosphere during the Heat treatment of the die-cast magnetic body continuously or is discontinuously renewed by rinsing.
  • the die-cast magnetic body initially in damp hydrogen a temperature between 850 and 1000 ° C and then in dry hydrogen at a temperature between 1000 and 1250 ° C heat treated.
  • the die-cast magnetic body at a temperature in the range of 870 to 950 ° C for a period of 2 to 16 hours in moist Hydrogen and finally at a temperature in the range from 1050 to 1120 ° C for a minimum of Heat treated in dry hydrogen for 1.5 hours.
  • the conditions are created to high quality soft magnetic alloys effective in Die casting process to process massive magnetic bodies.
  • At the Casting does not create any disruptive pores in the material. It can reusable molds are used and the The temperature of the casting melt can be lowered to such an extent that the Die casting tools have a sufficiently long service life.
  • the invention is based on exemplary embodiments explained in more detail.
  • Boron is added to a soft magnetic Fe 85 Si 15 alloy, which has a melting point of 1420 ° C., in such an amount that an Fe 77.5 Si 13.5 B 9 alloy is formed, the melting point of which is only 1160 ° C lies.
  • Rings with an outer ring diameter of 20 mm and a material thickness of 2 x 2 mm are cast from this alloy.
  • a measurement of the coercive field strength results in an H C value of> 1200 A / m.
  • These rings are then subjected to heat treatment in moist hydrogen at 1000 ° C. for 8 hours and then to heat treatment in dry hydrogen at 1100 ° C. for 8 hours.
  • the heat treatment reduces the boron content in the rings to ⁇ 0.1% and approximately the original Fe 85 Si 15 alloy with a coercive field strength H C of ⁇ 100 A / m is formed.
  • the rings thus produced can be used as ring cores for transformers be used.
  • the rods thus produced can be used as cores for relays be used.

Landscapes

  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Soft Magnetic Materials (AREA)
  • Hard Magnetic Materials (AREA)
  • Manufacturing Cores, Coils, And Magnets (AREA)
  • Magnetic Ceramics (AREA)
  • Manufacturing Of Steel Electrode Plates (AREA)
EP97117634A 1996-10-22 1997-10-11 Verfahren zur Herstellung massiver Magnetkörper Expired - Lifetime EP0838289B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19643602 1996-10-22
DE19643602A DE19643602A1 (de) 1996-10-22 1996-10-22 Verfahren zur Herstellung massiver Magnetkörper

Publications (2)

Publication Number Publication Date
EP0838289A1 EP0838289A1 (de) 1998-04-29
EP0838289B1 true EP0838289B1 (de) 2002-12-18

Family

ID=7809469

Family Applications (1)

Application Number Title Priority Date Filing Date
EP97117634A Expired - Lifetime EP0838289B1 (de) 1996-10-22 1997-10-11 Verfahren zur Herstellung massiver Magnetkörper

Country Status (5)

Country Link
US (1) US5932032A (ja)
EP (1) EP0838289B1 (ja)
JP (1) JPH10154625A (ja)
AT (1) ATE229859T1 (ja)
DE (2) DE19643602A1 (ja)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6722887B2 (ja) * 2016-06-08 2020-07-15 パナソニックIpマネジメント株式会社 鉄基磁性体の圧粉磁心

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB450841A (en) * 1935-01-21 1936-07-21 Birmingham Electr Furnaces Ltd Methods or processes for the heat-treatment of iron, steel and alloy steels
DE1182276B (de) * 1958-11-12 1964-11-26 Armco Steel Corp Verfahren zur Herstellung von nichtalterndem Siliziumstahlblech
DD108628A1 (ja) * 1973-09-20 1974-09-20
DD126155A1 (ja) * 1976-06-22 1977-06-22
JPS54104427A (en) * 1978-02-06 1979-08-16 Hitachi Metals Ltd Low temperature fusion magnetic alloy

Also Published As

Publication number Publication date
DE19643602A1 (de) 1998-04-23
ATE229859T1 (de) 2003-01-15
JPH10154625A (ja) 1998-06-09
EP0838289A1 (de) 1998-04-29
DE59708998D1 (de) 2003-01-30
US5932032A (en) 1999-08-03

Similar Documents

Publication Publication Date Title
DE1936153B2 (de) Verfahren und giessform zum herstellen von gusstuecken mit kugelgraphit
DE69015035T2 (de) Verfahren zur Herstellung gesinterter Formkörper einer Fe-P-Legierung mit weichmagnetischen Eigenschaften.
DE3004209A1 (de) Verfahren zur herstellung eines metallischen sinterformteils und fuer die durchfuehrung des verfahrens geeignete maschine
DE3685656T2 (de) Verfahren zur herstellung eines voellig dichten gegenstandes.
EP0838289B1 (de) Verfahren zur Herstellung massiver Magnetkörper
DE3841748C2 (ja)
DE69428236T2 (de) Metallisches Pulver zum Herstellen von Teilen durch Pressformen und Sinterung, und Verfahren zur Herstellung von dem Pulver
DE656966C (de) Permanenter Magnet und Verfahren zu seiner Herstellung
EP1259341B1 (de) Verfahren zur herstellung einer oxidationshemmenden titangussform
DE877318C (de) Verfahren zur Verbesserung der magnetischen Guetewerte bei der Herstellung gesinterter Dauermagnete
DE2529231A1 (de) Verfahren zur behandlung von gussstuecken aus superlegierungen
EP0354389B1 (de) Verfahren zum Herstellen eines Formteiles aus Sinterstahl und daraus hergestelltes Formteil
EP0590186B1 (de) Kern nach dem Wachsausschmelzverfahren
DE3135661C2 (ja)
DE2807930C2 (de) Verfahren und Gießform zur Herstellung von Schleudergießkokillen aus stickstoffhaltigem Gußeisen
DE764867C (de) Dauermagnete und Verfahren zur Erhoehung ihrer Festigkeit
DE864616C (de) Verfahren zur Herstellung von Gussstuecken mit kohlenstoffarmen Aussenschichten aus Gusseisen
EP0020819A1 (de) Verfahren zur Herstellung von Gussstücken aus Gusseisen mit Vermicular-Grafit
DE3330231A1 (de) Hochverschleissfester magnetischer werkstoff
DE737371C (de) Verfahren zur Beeinflussung der magnetischen Eigenschaften von mechanisch durch Walzen, Ziehen usw. verarbeiteten Eisennickelsinterlegierungen
DE2164698A1 (de) Verfahren zur herstellung fussandfreier schmiedebloecke
DE2521422C3 (de) Verfahren zur Herstellung magnetischer Alnico-Werkstoffe und Verwendung dieser Werkstoffe
DE10209183A1 (de) Formstoff für die Herstellung von Gießformteilen
AT165056B (de) Verfahren zur Herstellung eines Verbundwerkstoffes und Formkörpers daraus
AT165531B (de) Verfahren zur Herstellung von mehrgliedrigen FormkÖrpern in einem kombiniert pulvermetallurgischen und Einseigerungsverfahren

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AT DE FR GB NL SE

AX Request for extension of the european patent

Free format text: AL;LT;LV;RO;SI

17P Request for examination filed

Effective date: 19981007

AKX Designation fees paid

Free format text: AT DE FR GB NL SE

RBV Designated contracting states (corrected)

Designated state(s): AT DE FR GB NL SE

17Q First examination report despatched

Effective date: 20010208

GRAG Despatch of communication of intention to grant

Free format text: ORIGINAL CODE: EPIDOS AGRA

GRAG Despatch of communication of intention to grant

Free format text: ORIGINAL CODE: EPIDOS AGRA

GRAH Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOS IGRA

GRAH Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOS IGRA

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT DE FR GB NL SE

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: NL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20021218

REF Corresponds to:

Ref document number: 229859

Country of ref document: AT

Date of ref document: 20030115

Kind code of ref document: T

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

Free format text: NOT ENGLISH

REF Corresponds to:

Ref document number: 59708998

Country of ref document: DE

Date of ref document: 20030130

Kind code of ref document: P

Ref document number: 59708998

Country of ref document: DE

Date of ref document: 20030130

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20030318

GBT Gb: translation of ep patent filed (gb section 77(6)(a)/1977)

Effective date: 20030326

ET Fr: translation filed
PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: GB

Payment date: 20030917

Year of fee payment: 7

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: FR

Payment date: 20031021

Year of fee payment: 7

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: AT

Payment date: 20031024

Year of fee payment: 7

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed

Effective date: 20030919

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20031215

Year of fee payment: 7

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20041011

Ref country code: AT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20041011

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: DE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20050503

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20041011

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20050630

REG Reference to a national code

Ref country code: FR

Ref legal event code: ST