EP0710055A1 - Réacteurs à plasma pour le traitement de plaquettes semi-conductrices - Google Patents

Réacteurs à plasma pour le traitement de plaquettes semi-conductrices Download PDF

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Publication number
EP0710055A1
EP0710055A1 EP95307268A EP95307268A EP0710055A1 EP 0710055 A1 EP0710055 A1 EP 0710055A1 EP 95307268 A EP95307268 A EP 95307268A EP 95307268 A EP95307268 A EP 95307268A EP 0710055 A1 EP0710055 A1 EP 0710055A1
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EP
European Patent Office
Prior art keywords
plasma reactor
ceiling
reactor
antenna
windings
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP95307268A
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German (de)
English (en)
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EP0710055B1 (fr
Inventor
Xue-Yu Qian
Arthur H. Sato
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Applied Materials Inc
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Applied Materials Inc
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32009Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
    • H01J37/32082Radio frequency generated discharge
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32009Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
    • H01J37/32082Radio frequency generated discharge
    • H01J37/321Radio frequency generated discharge the radio frequency energy being inductively coupled to the plasma
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05HPLASMA TECHNIQUE; PRODUCTION OF ACCELERATED ELECTRICALLY-CHARGED PARTICLES OR OF NEUTRONS; PRODUCTION OR ACCELERATION OF NEUTRAL MOLECULAR OR ATOMIC BEAMS
    • H05H1/00Generating plasma; Handling plasma
    • H05H1/24Generating plasma
    • H05H1/46Generating plasma using applied electromagnetic fields, e.g. high frequency or microwave energy

Definitions

  • the invention is related to fabrication of microelectronic integrated circuits with a inductively coupled RF plasma reactor and particularly to such reactors having coiled RF antennas providing a highly uniform plasma distribution.
  • Inductively coupled plasma reactors are employed where high density inductively coupled plasmas are desired for processing semiconductor wafers. Such processing may be etching, chemical vapor deposition and so forth.
  • Inductively coupled reactors typically employ a coiled antenna wound around or near a portion of the reactor chamber and connected to an RF power source.
  • the plasma density provided by the coiled antenna must be *uniform across the surface of the semiconductor wafer.
  • One attempt to provide such a uniform field is to wind the coiled antenna in a flat disk parallel to overlying the wafer, as disclosed in U.S. Patent No. 4,948,458 to Ogle. This concept is depicted in FIG. 1.
  • One problem with the flat coiled antenna of FIG. 1 is that there is a large potential difference between the center of the antenna and the circumferential edge thereof, with the result that the plasma can have a high ion density or "hot spot" over the center of the wafer and a lower ion density at the wafer periphery. This in turn causes the etch rate --or deposition rate-- to be nonuniform across the wafer surface.
  • One way of ameliorating this problem is to limit the power applied to the antenna coil to a few hundred watts so as to minimize the plasma non-uniformity. This approach is not completely satisfactory because it limits the etch rate (or deposition rate), thereby reducing throughput or productivity of the reactor, and moreover does not solve the problem of process non-uniformity across the wafer surface.
  • a coil antenna for radiating RF power supplied by an RF source into a vacuum chamber of an inductively coupled plasma reactor which processes a semiconductor wafer in the vacuum chamber, the reactor having a gas supply inlet for supplying processing gases into the vacuum chamber, the coil antenna including plural concentric spiral conductive windings, each of the windings having an interior end near an apex of a spiral of the winding and an outer end at a periphery of the spiral of the winding, and a common terminal connected to the interior ends of the plural concentric spiral windings, the RF power source being connected across the terminal and the outer end of each one of the windings.
  • the RF power source includes two terminals, one of the two terminals being an RF power terminal and the other of the two terminals being an RF return terminal which is connected to ground, the common terminal of the plural concentric spiral conductive windings being connected to one of the RF source terminals and the outer ends of the plural concentric spiral conductive windings being connected to the other RF source terminal.
  • the reactor chamber includes a planar ceiling and the antenna coil has a planar disk shape and lies on an exterior surface of the ceiling.
  • the reactor chamber includes a cylindrical side wall and the antenna coil has a cylindrical shape and is helically wound around a portion of the cylindrical wall.
  • the reactor includes a dome-shaped ceiling and the antenna coil has a dome shape and is helically wound around, lies on and is congruent with at least a portion of the dome-shaped ceiling.
  • the reactor includes a truncated dome-shaped ceiling and the antenna coil has a truncated dome shape and is helically wound around, lies on and is congruent with at least a portion of the truncated dome-shaped ceiling.
  • the reactor chamber includes a planar ceiling and a cylindrical side wall and one portion of the antenna coil is planar and overlies the planar ceiling while another portion of the antenna coil is cylindrical and is helically wound around at least a portion of the cylindrical side wall.
  • the reactor includes a dome-shaped ceiling and a cylindrical side wall and one portion of the antenna coil is dome-shaped and overlies and is congruent with the dome-shaped ceiling and another portion of the coil antenna is cylindrical and is wound around at least a portion of the cylindrical side wall.
  • the reactor includes a truncated dome-shaped ceiling and a cylindrical side wall and one portion of the antenna coil is truncated dome-shaped and overlies and is congruent with the truncated dome-shaped ceiling and another portion of the coil antenna is cylindrical and is wound around at least a portion of the cylindrical side wall.
  • the plural windings are of about the same length.
  • the coil antenna includes three of the windings.
  • the inner ends are circumferentially spaced from one another at equal intervals and wherein the outer ends are circumferentially spaced from one another at equal intervals.
  • a bias RF source may be connected to the wafer pedestal.
  • FIG. 1 is a simplified diagram of a coiled antenna for an inductively coupled plasma reactor of the prior art.
  • FIG. 2 is a simplified diagram of a coil antenna having its windings connected in parallel across an RF source.
  • FIG. 3A is a top view of a flat disk coil antenna for a plasma reactor in accordance with a first embodiment of the invention.
  • FIG. 3B is a top view of a flat disk coil antenna corresponding to FIG. 3A but having a greater number of windings.
  • FIG. 4 is a side view corresponding to FIG. 3A.
  • FIG. 5 is a perspective cut-away view of an inductively coupled plasma reactor employing the coiled antenna of the embodiment of FIG. 3A.
  • FIG. 6 is a perspective view of a cylindrical coil antenna in accordance with a second embodiment of the invention.
  • FIG. 7 is a perspective view of a coil antenna in accordance with a third embodiment of the invention which is a variant of the cylindrical coil antenna of FIG. 6 in that the cylindrical coil is continued over the ceiling of the reactor.
  • FIG. 8 is a perspective view of a coil antenna in accordance with a fourth embodiment of the invention having a dome shape.
  • FIG. 9 is a perspective view of a coil antenna in accordance with a fifth embodiment which is a variant of the cylindrical coil antenna of FIG. 6 and the dome antenna of FIG. 8.
  • FIG. 10 is a perspective view of a coil antenna in accordance with a sixth embodiment having a truncated dome shape overlying a truncated dome-shaped ceiling of a plasma reactor.
  • FIG. 11 is a perspective view of a coil antenna in accordance with a seventh embodiment having a truncated dome-shaped portion overlying a truncated dome-shaped reactor ceiling and a cylindrical portion surrounding the reactor side wall.
  • FIG. 12 is a perspective view of an embodiment of the invention having a truncated dome ceiling forming a chamfered corner along the circumference of the ceiling.
  • FIG. 13 is a perspective view of a variation of the embodiment of FIG. 12 including a cylindrical winding.
  • FIG. 14 is a perspective view of an embodiment of the invention having a shallow or partial dome-shaped ceiling.
  • FIG. 15 is a perspective view of a variation of the embodiment of FIG. 14 including a cylindrical winding.
  • FIG. 16 is a perspective view of an embodiment of the invention having a shallow dome-shaped ceiling with a chamfered corner along its circumference.
  • FIG. 17 is a perspective view of a variation of the embodiment of FIG. 16 including a cylindrical winding.
  • FIG. 18 contains superimposed graphs of ion current measured at the wafer surface as a function of radial position from the wafer center for various types of reactors of the prior art and corresponding graphs for a reactor incorporating the present invention.
  • FIG. 19 contains superimposed graphs of ion current measured at the wafer surface as a function of reactor chamber pressure for different reactors of the prior art.
  • FIG. 20 contains superimposed graphs of ion current measured at the wafer surface as a function of reactor chamber pressure for different reactors of the prior art and corresponding graphs for a reactor incorporating the present invention.
  • FIG. 21 contains superimposed graphs of ion current measured at the wafer surface as a function of reactor chamber pressure for different reactors of the prior art.
  • FIG. 2 illustrates one way of accomplishing this by connecting all of the coil windings 10, 12, 14 in parallel across the RF power source 16, 18 via conductors 20, 22.
  • One end 10a, 12a, 14a of each winding is connected to the conductor 20 while the other end 10b, 12b, 14b is connected to the other conductor 22.
  • the problem is that the gap 24 between the conductors 20, 22 gives rise to a discontinuity in the RF field.
  • the discontinuity of the coil can often cause azimuthal asymmetry in the plasma density across the wafer surface. Accordingly, the coil antenna of FIG. 2 does not provide a uniform plasma density and therefore does not fulfill the need.
  • a coil antenna 30 overlies the ceiling of a reactor chamber 31, the coil antenna 30 having plural concentric spiral windings 32, 34, 36 connected in parallel across a capacitor 62 and an RF source 64.
  • the windings 32, 34, 36 have inner ends 32a, 34a, 36a near the center of the spirals and outer ends 32b, 34b, 36b at the peripheries of the spirals.
  • the inner ends 32a, 34a, 36a are connected together at a common apex terminal 38.
  • the common apex terminal 38 is connected to ground while the outer winding ends 32b, 34b, 36b are connected to the RF source 64. As shown in FIG.
  • FIG. 3B illustrates a 5-winding version of the coil antenna of FIG. 3A, including concentric windings 32, 33, 34, 35, 36 with inner endings 32a, 33a, 34, 35a, 36a and outer endings 32b, 33b, 34b, 35b, 36b.
  • FIG. 5 illustrates an inductively coupled plasma reactor including a cylindrical vacuum chamber 50 having a flat disk insulating ceiling 52, a grounded conductive cylindrical side wall 54, a gas supply inlet 56 and a wafer pedestal 58.
  • a vacuum pump 60 pumps gas out of the vacuum chamber.
  • the coil antenna 30 of FIG. 3A rests on the ceiling 52.
  • An RF power source 64 applies power through the capacitor 62 to the outer winding ends 32, 34, 36 while the common terminal 38 is grounded.
  • a bias RF power source 66, 68 is connected to the wafer pedestal 58 to control ion kinetic energy.
  • the circular windings become straight radial arms terminating in the apex terminal 38, the arms extending along a radius r (FIG. 5) of about 2.5 cm.
  • the outermost one of the windings 32, 34, 36 has a radius R (FIG. 5) of about 35 cm in those cases in which the wafer diameter d (FIG. 5) is about 20 cm.
  • the height h (FIG. 5) of the coil antenna above the wafer is preferably about 5.0 cm to 7.5 cm.
  • each one of the coil windings 32, 34, 36 makes 1.5 turns.
  • the number of windings per length of radius which in the embodiment of FIG. 5 is 1.5/26 cm ⁇ 1, may be changed so as to desirably adjust the plasma density distribution across the wafer surface.
  • FIG. 6 illustrates a cylindrical version 60 of the coil antenna 30 of FIG. 3A, which also has plural concentric spiral windings 32', 34', 36' each wrapped around an insulating portion of the cylindrical side wall 54 of the reactor of FIG. 5.
  • the plural concentric windings 32', 34', 36' have respective inner ends 32a', 34', 36a' terminating in a common apex terminal 38a, as well as outer ends 32b', 34b', 36b' terminating equidistantly from each other at locations about the lower sidewall of the reactor chamber.
  • each winding 32', 34', 36' makes a smooth transition at the corner between the ceiling and the cylindrical sidewall, in the manner illustrated in the drawing.
  • FIG. 8 illustrates a dome-shaped version 80 of the coil antenna 30 of FIG. 3A for use with a version of the reactor of FIG. 5 in which the ceiling 52 is dome-shaped.
  • FIG. 9 illustrates how the dome-shaped coil antenna 80 may be integrated with the cylindrical shaped coil antenna 60 to form a single antenna 90 covering both the dome-shaped ceiling and cylindrical side wall of the reactor of the embodiment of FIG. 8. The windings make a smooth transition from the dome-shaped ceiling to the cylindrical sidewall in the manner illustrated in the drawing.
  • FIG. 10 illustrates a modification of the coil 80 of FIG. 8 in which the dome-shaped ceiling is truncated so as to have a flattened apex.
  • FIG. 11 illustrates a modification of the coil of FIG. 9 in which the dome-shaped ceiling is truncated so as to have a flattened apex.
  • windings 32, 34, 36 are spaced from one another by a sufficient spacing to prevent arcing therebetween.
  • all windings 32, 34, 36 preferably are of the same length.
  • the spacings between windings are equal and are uniform throughout the antenna coil.
  • the invention may be modified by varying the winding-to-winding spacings so as to be different at different locations or to differ as between different pairs of windings.
  • FIG. 12 illustrates a variation of the embodiment of FIG. 10 in which the ceiling 52 has a central flat region 52a surrounded by an annular chamfer 52b which provides a smooth transition from the horizontal flat region 52a to the vertical side wall 54. This in turn helps the windings 32, 33, 34, 35, 36 make a smooth transition as well.
  • An annular portion of the coil antenna overlies and conforms with the corner chamfer.
  • the embodiment of FIG. 12 has five concentric windings 32, 33, 34, 35, 36 with outer ends 32b, 33b, 34b, 35b, 36.
  • FIG. 13 illustrates a variation of the embodiment of FIG.
  • each of these windings including a first portion overlying the flattened central part 52a of the ceiling 52, a second portion overlying the corner chamfer 52b of the ceiling 52 and a third portion wrapped around the cylindrical side wall 54.
  • the winding outer ends 32b', 33b', 34b', 35b', 36b' defining the bottom of the coil antenna are disposed at about the same height as the top of the wafer pedestal 58 and are connected to the output terminal of the RF source through the capacitor 62.
  • the pitch of the windings may vary with location so that, as one example, the windings on the top may be at one pitch while the winding along the cylindrical side wall may be at a different pitch, thus providing greater control over the plasma formation.
  • FIG. 14 illustrates a variation of the embodiment of FIG. 12 having flattened dome-shaped ceiling, whose arc subtends an angle substantially less than 180 degrees, for example about 90 degrees.
  • the dome-shaped ceiling of FIG. 10 subtends approximately 180 degrees of arc.
  • FIG. 15 illustrates a variation of the embodiment of FIG. 13 also having flattened dome-shaped ceiling, whose arc subtends an angle substantially less than 180 degrees, for example about 90 degrees.
  • FIG. 16 illustrates an embodiment combining a flattened central dome 52a' like that of FIG. 14 with an outer corner chamfer 52b' like that of FIG. 12.
  • FIG. 17 illustrates a variation of the embodiment of FIG. 16 in which the windings make a smooth transition at the corner chamfer 52b from the ceiling 52 to the cylindrical side wall 54.
  • the embodiments of FIGS. 12-17 are illustrated as having 5 concentric windings each, in contrast with the 3 concentric windings of the embodiments of FIGS. 3-11.
  • the invention can be implemented with any suitable number of concentric windings.
  • the parallel arrangement of the windings 32, 34, 36 of the coil antenna 30 of FIG. 3A reduces the potential across each winding, as compared to, for example, using only one winding, and therefore reduces the capacitive coupling (as explained above with reference to the example of FIG. 2).
  • the coil antenna of FIG. 3A provides uniform plasma density over the wafer, as compared previous techniques for example, as there are no discontinuities of the type discussed above with reference to the example of FIG. 2 (e.g., in the RF field).
  • Such improved uniformity is not limited to etch applications, but is also realized when the invention is used in other plasma-assisted processes, such as chemical and physical vapor deposition of coatings.
  • the invention is used in other plasma-assisted processes, such as chemical and physical vapor deposition of coatings.
  • each of the windings 32, 34, 36 have the same length and their outer ends 32b, 34b, 36b terminate at points equidistant from each other about a circularly symmetric reaction chamber, further enhancing uniformity.
  • the winding inner ends 32a, 34a, 36a terminate at the geometric center of the coil antenna because the apex is located at the geometric center of the coil, which preferably has geometric circular symmetry.
  • this geometric antenna center is made to coincide with the axis of symmetry of a circularly symmetric reactor chamber.
  • the winding inner ends 32, 34a, 36a are preferably spaced equidistantly away from each other for a limited radial distance as they approach the apex terminal 38a.
  • windings are spaced from each other as uniformly as possible at least in flat configurations of the invention such as the embodiment of FIG. 3A; while in non-flat configurations such as the embodiment of FIG. 8, smoother variations and spacings with radius from the geometrical center may be made to compensate for chamber geometry.
  • the RF power applied to the coil antenna of FIG. 3A need not be limited as in the case of the coil antenna of FIG. 1.
  • the coil antenna of FIG. 3A can operate with 3000 Watts of RF power at 13.56 MHz, while the coil antenna of FIG. 1 must be limited to about 300 watts to prevent failures due to the nonuniform field coverage.
  • the increase in RF power afforded by the coil antenna of FIG. 3A provides higher etch rates in a plasma etch reactor, higher deposition rates in a chemical vapor deposition reactor.
  • the invention not only provides greater processing uniformity across the wafer surface but also provides greater throughput or productivity.
  • the invention provides a greater uniformity of ion density across the wafer surface, a significant advantage. This is illustrated in the superimposed graphs of FIG. 18.
  • the curves in FIG. 18 labelled Al, A2, A3 and A4 represent measurements of ion current at the wafer surface in milliAmperes per square centimeter as a function of distance from the wafer center in centimeters for a reactor employing the coil antenna of the invention depicted in FIG. 3A with a reactor chamber supplied with chlorine gas at an applied RF power level of 2000 Watts on the antenna coil, no RF bias power applied and the chamber maintained at a pressure of 2 milliTorr, 6.2 milliTorr, 10 milliTorr and 4 milliTorr, respectively.
  • the uniformity percentage represents the change in current density (vertical axis) across the wafer divided by two times the average current density in that range.
  • a reactor sold by manufacturer #1 whose performance is depicted by the curve labelled B in FIG. 18, had a deviation in plasma ion density of 4.5% across the wafer surface at the same applied RF power level and no RF bias power applied and a mixture of 50 parts of chlorine and 20 parts helium.
  • the invention provides a greater stability of ion density over a large range of chamber pressures, a significant advantage.
  • the performance of two plasma reactors of the prior art sold by manufacturers #2 and #3 are depicted by the superimposed curves labelled C and D, respectively, in FIG. 19.
  • the vertical axis is a normalized measured ion current at the wafer surface while the horizontal axis is the chamber pressure in milliTorr.
  • the manufacturer #2 plasma reactor (curve C) has a deviation of 23% in ion current over a pressure range from 2 to 5 milliTorr.
  • the manufacturer #3 reactor (curve D) has a deviation of 40% in ion current over the same pressure range.

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  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Plasma & Fusion (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Electromagnetism (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Plasma Technology (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Drying Of Semiconductors (AREA)
  • Chemical Vapour Deposition (AREA)
  • ing And Chemical Polishing (AREA)
EP95307268A 1994-10-31 1995-10-13 Réacteurs à plasma pour le traitement de plaquettes semi-conductrices Expired - Lifetime EP0710055B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US33256994A 1994-10-31 1994-10-31
US332569 1994-10-31

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EP0710055A1 true EP0710055A1 (fr) 1996-05-01
EP0710055B1 EP0710055B1 (fr) 1999-06-23

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US (2) US6297468B1 (fr)
EP (1) EP0710055B1 (fr)
JP (1) JPH08227878A (fr)
KR (1) KR100362455B1 (fr)
AT (1) ATE181637T1 (fr)
DE (1) DE69510427T2 (fr)

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US6297468B1 (en) 2001-10-02
DE69510427D1 (de) 1999-07-29
KR100362455B1 (ko) 2003-02-19
US6291793B1 (en) 2001-09-18
DE69510427T2 (de) 1999-12-30
EP0710055B1 (fr) 1999-06-23
JPH08227878A (ja) 1996-09-03

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