EP0663599B1 - Magnetic sensor and magnetic detector - Google Patents

Magnetic sensor and magnetic detector Download PDF

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Publication number
EP0663599B1
EP0663599B1 EP93916252A EP93916252A EP0663599B1 EP 0663599 B1 EP0663599 B1 EP 0663599B1 EP 93916252 A EP93916252 A EP 93916252A EP 93916252 A EP93916252 A EP 93916252A EP 0663599 B1 EP0663599 B1 EP 0663599B1
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EP
European Patent Office
Prior art keywords
bobbin
squid
magnetic
wires
pick
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EP93916252A
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German (de)
English (en)
French (fr)
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EP0663599A4 (en
EP0663599A1 (en
Inventor
Kenichi Sata
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Daikin Industries Ltd
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Daikin Industries Ltd
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/02—Measuring direction or magnitude of magnetic fields or magnetic flux
    • G01R33/035—Measuring direction or magnitude of magnetic fields or magnetic flux using superconductive devices
    • G01R33/0354—SQUIDS
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/02—Measuring direction or magnitude of magnetic fields or magnetic flux
    • G01R33/035—Measuring direction or magnitude of magnetic fields or magnetic flux using superconductive devices
    • G01R33/0354—SQUIDS
    • G01R33/0358—SQUIDS coupling the flux to the SQUID
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F5/00—Coils
    • H01F5/02—Coils wound on non-magnetic supports, e.g. formers
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S505/00—Superconductor technology: apparatus, material, process
    • Y10S505/825—Apparatus per se, device per se, or process of making or operating same
    • Y10S505/842—Measuring and testing
    • Y10S505/843—Electrical
    • Y10S505/845—Magnetometer
    • Y10S505/846—Magnetometer using superconductive quantum interference device, i.e. squid

Definitions

  • This invention relates to a magnetic sensor having a superconducting quantum interference device (SQUID) which is in the superconducting state on a level of cryogenic temperature, and relates to a magnetic detecting device in which the magnetic sensor is combined with a cryogenic refrigerator.
  • this invention pertains to thermal conduction structure of a superconducting pick-up coil in a magnetic-flux input circuit which is connected to the SQUID.
  • a SQUID using Josephson effect As one of superconducting devices, a SQUID using Josephson effect.
  • a SQUID magnetometer as a kind of magnetic sensor for measuring an extremely faint magnetic field, i.e., a magnetic field generated from faint current in a living body such as a magnetocardiogram, a magnetic field generated from a microscopic magnetic substance in a living body.
  • cryogenic temperature that is, to a temperature level on which the SQUID and the superconducting coil turn to the superconducting state
  • a method of cooling the SQUID magnetometer in such a manner that liquid helium on the level of cryogenic temperature is stored in a cryogenic container (cryostat) and the SQUID magnetometer is steeped in the liquid helium so as to be cooled.
  • a cooling head of a refrigerator for generating cool condition is entered in the cryogenic container and helium gas evaporated in the container is recondensed into liquid by the refrigerator.
  • the SQUID magnetometer since the SQUID magnetometer is steeped in liquid helium, the SQUID magnetometer can be cooled at a short time.
  • the container in which the liquid helium is stored is not filled to the uppermost end thereof with the liquid helium, the temperature at the inside of the container increases toward the upper part of the container. As a result, a thermal gradient occurs at the inside of the container. This thermal gradient disadvantageously limits an angle capable of inclination of the container. Due to this disadvantage, when a biomagnetic field is measured, it becomes difficult to optionally set the SQUID, the pick-up coil and such in accordance with the condition (posture) of a subject. This is a problem which cannot be disregard.
  • the SQUID magnetometer, the pick-up coil and such are attached and thermally connected to a final cooling stage to be cooled below a transition temperature of superconductivity by the cryogenic refrigerator. Accordingly, if only the operation of the cryogenic refrigerator is controlled, selection makes possible between the superconducting state and the normal conducting state. This does not require to move the SQUID, the pick-up coil and such for the above selection.
  • the pick-up coil of the magnetic-flux input circuit is generally wound into loops around a tubular bobbin made of resin.
  • the thermal conductivity of the resin forming the bobbin is low, it is very difficult to cool the pick-up coil around the bobbin to its transition temperature of superconductivity when the SQUID magnetometer is directly cooled by the refrigerator as above-mentioned.
  • the bobbin by metal such as copper and aluminium with high thermal conductivity even in a range of cryogenic temperature.
  • metal such as copper and aluminium
  • a normal conducting current loop generates at the bobbin in close vicinity to the magnetic-flux input circuit.
  • mutual inductance generates between the current loop and the pick-up coil. This invites another problem that out-put-to-input characteristic of the SQUID magnetometer varies with frequency.
  • a second problem is described next.
  • the SQUID is connected to the cryogenic refrigerator so as to be thermally conductable.
  • a superconducting shield member containing the SQUID is placed on the center of the top surface of a stage which is cooled below the transition temperature of superconductivity (for example, a 4K stage cooled to about 4K) by the cryogenic refrigerator, a thermally-conductive block member is arranged in such a manner as to interpose and cross over the superconducting shield member, and a bobbin around which a pick-up coil is wound is stood on the center of the top surface of the thermally-conductive block.
  • the thermally-conductive block member in such a manner as to cross over the superconducting shield member. Therefore, the plane form of the SQUID magnetometer can be little lessened and it is difficult to make the SQUID magnetometer multichannelized for high-precise measurement of a biomagnetic field.
  • the superconducting shield member, the thermally-conductive block and the bobbin may be lessened in size.
  • the bobbin cannot be minimized because its sensitivity of detecting magnetic flux is lowered when the bobbin is lessened in diameter.
  • the superconducting shield member is limited in its minimization. Consequently, the thermally conductive block arranged in such a manner as to cross over the superconducting shield member is limited in its minimization.
  • the pick-up coil is wound around the bobbin so as to form first-order or second-order differential type coil. This requires the following producing steps. From this, minimization of the SQUID magnetometer is also limited.
  • the producing steps are as follows: The pick-up coil is wound in such a manner as to be provided together with the thermally-conductive block and the bobbin; a lead wire from the pick-up coil is conducted to the SQUID with the pick-up coil thermally connected to the bobbin and the thermally-conductive block; and then the lead wire is electrically connected to the SQUID by superconductive soldering or the like.
  • an inner space of the thermally-conductive block has an area allowing the above work of electrical connection, in detail, an area allowing insertion of a soldering iron and fingers. Since the size of the inner space of the thermally-conductive block is limited as mentioned above, the SQUID magnetometer can be little lessened in its form projected on the plane. Since it is a matter of course that a complicated producing process for the SQUID magnetometer is required, it costs long time to assemble the SQUID magnetometer. As for this point, even in case of the above electric connection between the SQUID and the pick-up coil, the above-mentioned complicated process is required.
  • the SQUID magnetometer is relatively lessened in size.
  • the 4K stage is cooled in a way of thermal conduction by the cryogenic refrigerator, the 4K stage cannot be increased in size above the cooling capability of the cryogenic refrigerator. This also prevents the SQUID magnetometer from being multi-channelized.
  • the thermally-conductive block is generally so composed that plural blocks are fixed in order by screws or the like, the heat resistance of the thermally-conductive block is different between portions thereof depending on the contacting state between the plural blocks. This may make the temperature of the pick-up coil different between one SQUID magnetometer and another SQUID magnetometer, and, in the worst case, a pick-up coil of at least one SQUID magnetometer cannot be cooled below the transition temperature of superconductivity.
  • a sensor according to the preamble of claims 1 and 3 is known from JP-A-2/302682.
  • This document relates to a superconducted quantum inference element becoming a superconductive state at an extremely low temperature level and the magnetic-flux input circuit connected thereto and composed of superconducted coils are mounted.
  • a plurality of coil units wherein the coils are wound by bobbins are provided and combined to constitute the circuit as a whole.
  • a first object of this invention is to improve the structure of a bobbin around which a pick-up coil is wound in a SQUID magnetometer, that is, to enhance the cooling efficiency of the SQUID magnetometer to the pick-up coil without affecting input/output characteristic of the SQUID magnetometer, thereby effectively carrying out the cooling of the SQUID magnetometer by a refrigerator.
  • a second object of this invention is to readily multichannelize the SQUID magnetometer which is cooled in a way of thermal conduction by a cryogenic refrigerator, to simplify an assembling work of the SQUID magnetometer, and to extremely enhance the operation performance in maintenance, check and repair of the SQUID magnetometer.
  • wires each coated with a resinous film and made of non-magnetic material with high thermal conductivity, such as copper, aluminium, are arranged in a body of a resinous bobbin.
  • this invention premises a magnetic sensor having a SQUID which is in the superconducting state on a level of cryogenic temperature and having a magnetic-flux input circuit which is connected to the SQUID.
  • the magnetic-flux input circuit comprises: a pick-up coil wound around a tubular resinous bobbin; and plural wires each coated with a resinous film and made of non-magnetic material with high thermal conductivity, such as copper, and aluminium, the plural wires being arranged in the body of the resinous bobbin and netted in a grid pattern so as to extend substantially in an axial direction of the bobbin and a circumferential direction of the bobbin.
  • the thermal-conduction characteristic of the bobbin is improved with respect to the direction of the center axis of the bobbin and the circumferential direction thereof, that is, with respect to the entire bobbin. Accordingly, when the magnetic sensor is cooled by a cryogenic refrigerator, a thermally-conductable connection of the bobbin to a cooling stage of the refrigerator results in smooth thermal conduction between the cooling stage and the bobbin, thereby readily cooling the bobbin. This enables the pick-up coil wound around the bobbin to be cooled to the transition temperature of superconductivity at a short time.
  • each of the wires as components of the bobbin is coated with a resinous film, even if the wires are made of metal such as copper and aluminium, the wires do not contact directly one another though they intersect one another. In addition, it is avoided that ends of the wires extending substantially in the circumferential direction of the bobbin contact one another. Accordingly, a loop of normal conducting current generates only at an inner section of each wire and is extremely little. As a result, variation of input/output characteristic of the magnetic sensor due to the loop of normal conducting current can be restricted.
  • the wires extending substantially in the axial direction of the bobbin may be larger in diameter than the wires extending substantially in the circumferential direction of the bobbin.
  • the thermal-conduction characteristic of the bobbin is enhanced with respect to the axial direction thereof. Accordingly, even if the end of the bobbin is connected to the cooling stage of the refrigerator so as to be thermally conductable, cooling to the bobbin by the cooling stage is smoothly conducted, thereby cooling the bobbin and the pick-up coil wounded therearound to the transition temperature of superconductivity at a short time.
  • plural wires each coated with a resinous film and made of non-magnetic material with high thermal conductivity, such as copper, aluminium, and plural wires each made of non-conductive material, such as glass fiber, may be arranged at the internal part of a tubular resinous bobbin around which a pick-up coil of the magnetic-flux input circuit is wound, and netted in a grid pattern in such a manner that the wires made of non-magnetic material with high thermal conductivity extend substantially in an axial direction of the bobbin.
  • the thermal-conduction characteristic of the bobbin is enhanced with respect to the axial direction of the bobbin, thereby cooling the bobbin and the pick-up coil to the transition temperature of superconductivity at a short time through the cooling stage of the refrigerator.
  • each of the above-mentioned magnetic sensors is combined with a cryogenic refrigerator for cooling a cold receiving member to a level of cryogenic temperature and the resinous bobbin of the magnetic sensor is connected to the cold receiving member so as to be thermally conductive.
  • each of the magnetic sensors of the above magnetic detecting devices composes a high thermally-conductive member an end of which is connected to the bobbin and another end of which is removably attached to a set position of a cold receiving member to be cooled on a level of cryogenic temperature by the cryogenic refrigerator, and a superconducting shield member which is removably attached to a set position of the side of the high thermally-conductive member and contains a SQUID at the attached state.
  • the magnetic sensor can be readily disposed. Since it is a matter of fact that the superconducting shield member containing the SQUID is attached removably to the set position of the side of the high thermally-conductive member, this has very little influence on the disposition of the magnetic sensor.
  • the electric connection between the SQUID and the pick-up coil can be accomplished before the high thermally-conductive member is attached to the cold receiving member. This dispenses with wiring and soldering at a narrow space. Accordingly, there can be simplified assembly, maintenance, check and repair of the magnetic sensor.
  • the magnetic sensor can be readily multi-channelized without increasing the cold receiving member in size.
  • plural SQUIDs and its corresponding superconducting shield members are attached, thereby enhancing utilization efficiency of space.
  • the multi-channelization of the magnetic sensor can be readily accomplished at a relatively narrow area.
  • the pick-up coil can be securely cooled below the transition temperature of superconductivity.
  • the high thermally-conductive member may have a concavity at the set position of the side thereof and the superconducting shield member may be attached to the concavity.
  • the required projective form on the plane of the magnetic sensor for preventing interference with other magnetic sensors resulting from the attachment can be lessened, thereby further enhancing utilization efficiency of space.
  • the number of magnetic sensors attachable to a relatively narrow area is further increased.
  • the high thermally-conductive member may have, at an end thereof which is removably attached to the set position of the cold receiving member, a through hole for being inserted by a wire toward a room temperature's side.
  • the high thermally-conductive member has, at its end which is removably attached to the set position of the cold receiving member, a through hole for being inserted by a wire toward the room temperature's side, the wire toward the room temperature's side is connected to the SQUID before the magnetic sensor is attached to the cold receiving member. Accordingly, after the attachment of the magnetic sensor to the cold receiving member, the wire can be arranged only on a back side of the cold receiving member without arranging the wire on a front side thereof. This simplifies wire arrangement.
  • Fig.1 is an enlarged perspective view of a main part of a bobbin in an example 1 of this invention.
  • Fig.2 is an enlarged section of a main part of a cryogenic refrigerator in the example 1.
  • Fig.3 is a schematic section of the cryogenic refrigerator and a SQUID magnetometer in the example 1.
  • Fig.4 is a corresponding diagram to Fig.1 in an example 2 of this invention.
  • Fig.5 is a corresponding diagram to Fig.1 in an example 3 of this invention.
  • Fig.6 is an elevation showing a magnetometer unit in a further example of this invention.
  • Fig.7 is a longitudinal section cut in the middle of the magnetometer unit of the further example.
  • Fig.8 is a longitudinal section cut in the middle schematically showing a structure of multi-channelized measuring system in which the thirty-two magnetometer units of the further example are disposed.
  • Fig.9 is a section taken on line XI-XI of Fig.8.
  • Fig.10 is a plan view of a printed wiring substrate in the further example.
  • Fig.11 is a bottom view of a cold receiving member in the further example.
  • Fig.3 is a total structure of an example 1 of this invention.
  • a SQUID magnetometer as a magnetic sensor is used for measuring magnetic waves from a human heart.
  • (1) indicates a stand for laying thereon a subject (M) whose magnetic waves from the human heart are measured and the stand (1) is disposed in an electromagnetic shield room or a magnetic shield room.
  • a tubular supporting stand (2) is disposed below the stand (1).
  • a sealed vacuum chamber (3) is fixedly supported by the supporting stand (2) in such a manner that the bottom end thereof is sunk in the supporting stand (2). An inner space of the vacuum chamber (3) is maintained in a vacuous condition.
  • a SQUID magnetometer (B) as a magnetic sensor is contained.
  • (A) indicates a helium refrigerator having a binary circuit for cooling the SQUID magnetometer (B) to a level of cryogenic temperature on which the SQUID magnetometer (B) is operable.
  • the precooling refrigerating circuit (4) is composed of a refrigerator of G-M (Gifford-McMahon) cycle for compressing and expanding helium gas to precool helium gas in the J-T circuit (10), and is connected in a closed circuit with an un-shown compressor of the precooling refrigerating circuit and the expander (5).
  • the expander (5) is attached to a bottom wall of the vacuum chamber (3) so as to insulate its vibration.
  • the expander (5) has a casing (6) fixedly disposed at an under surface of the bottom wall of the vacuum chamber (3), and a cylinder (7) of a two-stage structure which is connected to an upper part of the casing (6).
  • the casing (6) has a high-pressure gas inlet (6a) which is connected to a discharge side of the compressor of precooling refrigerating circuit, and a low-pressure gas outlet (6b) which is connected to an intake side of the compressor.
  • the cylinder (7) passes through the bottom wall of the vacuum chamber (3) so as to make the bottom wall gastight and extends upward at the inside of the vacuum chamber (3).
  • the cylinder (7) has a first heat station (8) which is formed at an upper end of a larger diameter part thereof and maintained on a temperature level of 55-60 K, and a second heat station (9) which is formed at an upper end of a smaller diameter part thereof and maintained on a temperature level of 15-20 K lower than that of the first heat station (8).
  • a displacer which is un-shown in the figure, is inserted reciprocatably in the cylinder (7) so as to section an expansion chamber at corresponding positions to the heat stations (8), (9).
  • Inserted in the casing (6) are a rotary valve which opens at respective rotations to change over a gas flow so as to supply helium gas flowing into the casing from the high-pressure gas inlet (6a) to the expansion chamber in the cylinder (7) or so as to discharge helium gas expanded in the expansion chamber from the low-pressure gas outlet (6b), and a valve motor for driving the rotary valve.
  • High-pressure helium gas is expanded by Simon expansion in the expansion chamber of the cylinder (7) by the opening of the rotary valve of the expander (5).
  • the precooling refrigerating circuit (4) of closed circuit type is so arranged that: high-pressure helium gas discharged from the refrigerator for precooling is supplied to the expander (5); the temperature of the heat stations (8), (9) is lowered by adiabatic expansion in the expander (5) thereby precooling the below-mentioned precoolers (15), (16) of the J-T circuit (10); and then the expanded helium gas is returned to the compressor for re-compression.
  • the J-T circuit (10) is a refrigerating circuit for compressing helium gas thereby leading the helium gas to Joule-Thomson expansion in order to generate cool condition on a level of cryogenic temperature of about 4K, and has a compressor (no-shown) for compressing helium gas and the expansion unit (11) for leading the compressed helium gas to Joule-Thomson expansion.
  • the expansion unit (11) has a first J-T heat exchanger (12) which passes through the bottom wall of the vacuum chamber (3) so as to make the bottom wall gastight.
  • the first J-T heat exchanger (12) is connected to second and third J-T heat exchangers (13), (14) which are arranged inside the vacuum chamber (3).
  • Each of the J-T heat exchangers (12)-(14) exchanges heat between helium gasses passing on its primary side and its secondary side.
  • the primary side of the first J-T heat exchanger (12) is connected to the discharge side of the compressor of the J-T circuit.
  • Both the primary sides of the first and second J-T heat exchangers (12), (13) are connected to each other via a first precooler (15) composed of a heat exchanger which is disposed around an outer periphery of the first heat station (8) of the expander (5).
  • both the primary sides of the second and third J-T heat exchangers (13), (14) are connected to each other via a secondary precooler (16) composed of a heat exchanger which is disposed around an outer periphery of the second heat station (9) of the expander (5).
  • the primary side of the third J-T heat exchanger (14) is connected to a cooler (18) via a J-T valve (17) for leading high-pressure helium gas to Joule-Thomson expansion.
  • An opening of the J-T valve (17) is regulated by an operating rod (no-shown) from the outside of the vacuum chamber (3).
  • the cooler (18) is formed of a coiled pipe wound around an outer periphery of a cool reception part (19a) located on a under surface of a disk-shaped cold receiving member (cold receiving plate) (19). According to this structure, the cold receiving member (19) contacts the cooler (18) so as to be thermally conductable, thereby maintaining about 4K of the same temperature as in the cooler (18). Further, the SQUID magnetometer (B) is integrally mounted, so as to be thermally conductable, on a top surface of the cold receiving member (19).
  • the cooler (18) is connected to the secondary side of the first J-T heat exchanger (12) via respective secondary sides of the third and second J-T heat exchangers (14), (13).
  • the secondary side of the first J-T heat exchanger (12) is connected to the intake side of the compressor of the J-T circuit (10).
  • the J-T circuit (10) is so arranged that: helium gas is compressed into high pressure to be supplied toward the vacuum chamber (3); heat exchange is conducted, by the first to third J-T heat exchangers (12)-(14) in the vacuum chamber (3), between the high-pressure helium gas and low-temperature low-pressure helium gas which returns to the compressor; heat exchange is conducted, by the first and second precoolers (15), (16), between the high-pressure helium gas and the first and second heat stations (8), (9) of the expander (5); Joule-Thomson expansion is conducted to the high-pressure helium gas by the J-T valve (17) so that the helium gas is made into helium of a gas-liquid mixing state with 1 atm and about 4K by the cooler (18); the cold receiving member (19) and the SQUID magnetometer (B) contacting it are cooled and held on a level of cryogenic temperature of about 4K by latent heat of vaporization of the helium; and then the helium gas of low pressure
  • the SQUID magnetometer (B) has a SQUID (no-shown) which is in the superconducting state on a level of cryogenic temperature, and a magnetic-flux input circuit (32) connected to the SQUID.
  • the SQUID is fixed, so as to be thermally conductable, to the upper surface of the cold receiving member (19) in such a manner as to be contained in the superconducting shield member (31).
  • the magnetic-flux input circuit (32) has a pick-up coil (33) which is formed of a superconducting wire wound in loops to a tubular bobbin (34).
  • the pick-up coil (33) has four loops and is a second-order differential type one that the four loops are connected in series with set spaces left respectively in order that the current of each of upper and lower loops (33a), (33d) flows in an opposite direction to the current of two middle loops (33b), (33c) in an alternative way. That is, the SQUID magnetometer (B) forms a gradiometer for measuring a second order gradient of the magnetic field by the pick-up coil (33) which is wound into the four loops (33a)-(33d).
  • a thermally-conductive bracket (20) is attached over the superconducting shield member (31) for containing the SQUID.
  • the bobbin (34) is disposed in such a manner as to stand on the top surface of the bracket (20).
  • the bobbin (34) has a length of about 200-300mm and extends upward in an upper swelling (3a) formed at a center of an upper wall of the vacuum chamber (3).
  • the pick-up coil (33) is wound around an upper part of the bobbin (34) and cooled below the transition temperature of superconductivity thereof through the bobbin (34).
  • the upper end of the swelling (3a) of the vacuum chamber (3) faces an opening (1a) at the center of the stand (1). Magnetic waves of a heart of a subject (M) on the top surface of the stand (1) is measured through the opening (1a).
  • This invention has a feature thereof in a structure of the bobbin (34) around which the pick-up coil (33) is wound.
  • plural wires (35), (35), ... in which copper wires of about 0.5mm diameter as non-magnetic material with high thermal conductivity are each coated with a resinous film are arranged at the internal part of the resinous bobbin (34) and netted in a grid pattern so as to extend substantially in an axial direction of the bobbin (34) and a circumferential direction of the bobbin (34).
  • the copper wire may be substituted by an aluminium wire.
  • (21) indicates a radiant-heat shield disposed at the upper part of the vacuum chamber (3) so as to cover the cold receiving member (19), the superconducting shield member (31) for containing the SQUID, the bracket (20), and the lower part of the bobbin (34).
  • the radiant-heat shield contacts the first heat station (8) of the expander of the precooling refrigerating circuit (4) thereby maintaining its temperature at about 80K.
  • (22) indicates a super insulation disposed concentrically around the bobbin (34).
  • the SQUID magnetometer (B) In accordance with the operation of the helium refrigerator (A), the SQUID magnetometer (B) is cooled. When the SQUID magnetometer (B) decreases its temperature to the level of cryogenic temperature of about 4K, the SQUID magnetometer starts operating.
  • high-pressure helium gas discharged from the compressor is supplied toward the vacuum chamber (3).
  • the high-pressure helium gas supplied toward the vacuum chamber (3) enters the primary side of the first J-T heat exchanger (12) and heat exchange is conducted therein between the high-pressure helium gas and low-pressure helium gas of secondary side which returns to the compressor so that the high-pressure helium gas is cooled from its room temperature of 300K to about 70K.
  • the helium gas enters the first precooler (15) located at the outer periphery of the first heat station (8) which is cooled at 55-60K in the expander (5) thereby decreasing its temperature to about 55K.
  • the cooled gas enters the primary side of the second J-T heat exchanger (13) and heat exchange is conducted therein between the high-pressure helium gas and low-pressure helium gas of secondary side so that the high-pressure helium gas is cooled to about 20K. Then, the gas enters the second precooler (16) located at the outer periphery of the second heat station (9) which is cooled at 15-20K in the expander (5) thereby decreasing its temperature to about 15K. Next, the gas enters the primary side of the third J-T heat exchanger (14) and heat exchange is conducted therein between the high-pressure helium gas and low-pressure helium gas of secondary side so that the high-pressure helium gas is cooled to about 5K.
  • the gas reaches to the J-T valve (17).
  • the high-pressure helium gas is squeezed to make a Joule-Thomson expansion, thereby being helium of 1 atm and about 4K in a gas-liquid mixing condition.
  • the helium is supplied to the cooler (18) located downstream the J-T valve (17).
  • the cooler (18) the cold receiving member (19) is cooled by latent heat of vaporization by liquid part of the helium in a gas-liquid mixing condition.
  • the cold receiving member (19) When the cold receiving member (19) is cooled, there are cooled the SQUID of the SQUID magnetometer (B) contacting the cold receiving member (19) so as to be thermally conductable, a superconducting shield member (31) containing the SQUID magnetometer, the bobbin (34), and the pick-up coil (33) of the magnetic-flux input circuit (32).
  • the evaporated low-pressure helium gas returns from the cooler (18) to the secondary side of the third J-T heat exchanger (14) and becomes saturated gas of about 4K during the return.
  • the helium gas passes respective secondary sides of the second and first J-T heat exchanger (13), (12) to cool the high-pressure helium gases of respective primary sides, and finally increases its temperature to about 300K (room temperature). Successively, the gas returns to the intake side of the compressor.
  • one cycle of the precooling refrigerating circuit (4) and the J-T circuit (10) completes.
  • refrigerating operation of the refrigerator (A) is carried out so as to repeat the above manner.
  • the temperature of the SQUID magnetometer (B) falls toward the level of cryogenic temperature (operation temperature level). When the temperature reaches to the level of cryogenic temperature, the SQUID magnetometer starts operating.
  • the wires (35), (35), ... that is the copper wires with high thermal conductivity, are each coated with a resinous film are arranged longitudinally and laterally in the body of the resinous bobbin (34) around which the pick-up coil (33) made of the superconducting wire is wound, thermal-conduction characteristic of the bobbin (34) is enhanced with respect to an axial direction and a circumferential direction of the bobbin (34), as compared with the case where the entire bobbin is formed of only resinous material. Accordingly, the cooling from the cold receiving member (19) which is cooled on a 4K level by the refrigerator (A) is smoothly conducted to the bobbin (34), thereby readily cooling the bobbin (34).
  • the pick-up coil (33) wound around the bobbin (34) can be cooled to the level of cryogenic temperature at a short time.
  • the wires (35) arranged in the body of the resinous bobbin (34), which are copper wires, is each coated at the surface with the resinous film of insulation material, the wires (35) do not contact one another directly at the intersecting part and the circumferential end.
  • the bobbin (34) does not generate, at a wide area, a normal conducting current loop, that is, the loop generates only at the inner of each wire (35) to be extremely small. Accordingly, it is prevented that the input/output characteristic of the SQUID magnetometer (B) varies due to the current loop.
  • both the wires (35), (35) respectively arranged in the axial direction and the circumferential direction of the resinous bobbin (34) have same diameter as each other.
  • the wires (35) in the axial direction may be larger in diameter than the wires (35) in the circumferential direction.
  • thermal-conduction characteristic in the axial direction of the bobbin (34) further enhances as compared with that in the circumferential direction, and the cooling from the cold receiving member (19) is conducted smoothly by the bobbin (34), even if the bobbin (34) is so arranged that the lower end thereof contacts, so as to be thermally conductable, the cold receiving member (19) of the refrigerator (A) as in the above-mentioned construction. This enhances efficiency of cooling the bobbin (34) and the pick-up coil (33) wound around the bobbin (34).
  • Fig.5 shows an example 3 of this invention, wherein the wire in a circumferential direction in the body of the resinous bobbin (34) is changed in material.
  • wires are arranged in a body of a tubular resinous bobbin (34) around which a pick-up coil (33) of a magnetic-flux input circuit (32) is wound, and netted so as to form a grid pattern in an axial direction and a circumferential direction of the bobbin (34).
  • the wires (35) in the axial direction are each made of a copper wire (or an aluminium wire) coated with a resinous film while the wires (36) in the circumferential direction are made of non-conductive material such as glass fiber.
  • the wires (35) in the axial direction arranged in the body of the bobbin (34) is each made of a copper wire or an aluminium wire which is coated with a resinous film, similar to the example 1, thermal-conduction characteristic of the bobbin (34) is enhanced with respect to the axial direction of the bobbin. Accordingly, the bobbin (34) and the pick-up coil (33) are cooled to the transition temperature of superconductivity at a short time by the cold receiving member (19) of the refrigerator (A).
  • the wires (36) in the circumferential direction arranged in the body of the bobbin (34) are made of non-conductive material such as glass fiber, it can be securely restrained that current loops in a circumferential direction of the bobbin (34) generate at the bobbin (34). This prevents further effectively variation of the input/output characteristic of the SQUID magnetometer (B).
  • Figs.6 to 11 show a further example of this invention.
  • Fig.6 is an elevation of a SQUID magnetometer of the example 6
  • Fig.7 is a longitudinal section cut in the middle of the SQUID magnetometer.
  • (51) indicates a high thermally-conductive member having at its both ends male screw parts (51a), (51b), respectively.
  • a pair of concavities (51c), (51c) are formed.
  • a removable superconducting shield member (52) for containing the SQUID.
  • the upper male screw part (51b) is engaged and fastened to a female screw part (41) located at the lower end of the bobbin (34) around which a pair of pick-up coils (33), (33) are wound.
  • the high thermally-conductive member (51) is made of such as copper and has a wire insert hole (51d) which is penetrated so as to open at the center of the end surface of the lower male screw part (51a) and at respective set positions of the concavities (51c).
  • the superconducting shield member (52) is composed of a base member (52a) attached so as to be embedded in the concavity (51c) of the high thermally-conductive member (51) and a cover member (52b) attached removably by a screw or the like. Grooves (52c) for inserting lead wires are formed at set positions of the cover member (52b). To each of set positions of the base member (52a), a substrate (52e) on which a SQUID (no-shown) is mounted is attached through a spacer member (52d).
  • a large-diameter flange part (51e) is integrally formed at an upper side of the lower male screw part (51a), thereby increasing a contact area between the high thermally-conductive member (51) and the cold receiving member (19).
  • the bobbin (34) is the same as in the example 5.
  • Each of the pick-up coils (33) is wound around the outer periphery of the bobbin (34), for example, so as to be a first-order differential type. Loops of the pick-up coils (33) are wound so as to be set in respective annular grooves (40), (40), ... formed at set positions of the bobbin (34). As shown in Figs.6 and 7, the pair of pick-up coils (33), (33) are wound around the bobbin (34), and the pair of substrates (52e), (52e) respectively corresponding to the pick-up coils (33), (33) are contained in the superconducting shield members (52), (52), respectively.
  • a magnetometer unit (B) in which two SQUID magnetometers are integrated.
  • a lead wire (33e) of the pick-up coil (33) passes one of the grooves (52c) and is connected to the SQUID of the substrate (52e), while a lead wire (52f) from the SQUID passes through the wire insert hole (51d) and is led out it.
  • a connecter (52g) is provided at an end of the lead wire (52f).
  • Fig.8 is a longitudinal section cut in the middle schematically showing the construction of a multi-channelized measuring system in which thirty-two magnetometer units shown in Fig.7 are arranged.
  • Fig.9 is a section taken on line XI-XI of Fig.8.
  • the thirty-two magnetometer units (B), (B), ... are arranged with set spaces left respectively in such a manner as to be screwed into the cold receiving member (19).
  • the cold receiving member (19) is cooled up to below the transition temperature of superconductivity (for example, to about 4K) by the no-shown cryogenic refrigerator.
  • (21a) and (21b) indicate radiant heat shield members.
  • a printed wiring board (53) in which connecters (53d) are previously attached.
  • connecters (53d) are previously attached.
  • pins (53a) of the connecters (53d) are exposed and a wiring pattern (53b) for electrically connecting between corresponding pins (53a), (53a), ... is formed.
  • through holes (53c) for respectively passing through the male screw parts (51a) of the magnetometer units (B).
  • a large-diameter hole (53e) for allowing a direct contact between the cold receiving member (19) and the cooler (18) as a final cooling part of the cryogenic refrigerator.
  • Fig.11 shows a bottom surface of the cold receiving member (19).
  • female screw holes (54) for respectively engaging with the lower male screw part (53c) of the high thermally-conductive member (51) are formed at corresponding positions to the through holes (53c), and concavities (55) for respectively containing the pin (53a) are formed at corresponding positions to the connecters (53d).
  • the high thermally- conductive member (51) is integrally connected to the bobbin (34).
  • the base members (52a) of the superconducting shield member (52) are attached to the concavities (51c) on the side of the high thermally-conductive member (51), respectively.
  • the substrate (52e) on which the SQUID is mounted is attached to the base member (52a) through the spacer member (52d).
  • the pick-up coil (33) is wound around the bobbin (34).
  • the lead wire (33e) of the pick-up coil (33) is connected at a set position of the substrate (52e) so as to be electrically connected to the SQUID.
  • the lead wire (52f) for supplying a bias power source to the SQUIDs and for leading out electric signals from the SQUID is drawn out from the center of the end surface of the male screw part (51a) through the wire insert hole (51d).
  • the connecter (52g) is connected to a free end of the lead wire (52f).
  • each of the cover members (52b) of the superconducting shield members (52) is fixed to the high thermally-conductive member (51) by a screw or the like and the lead wires (33e), (52f) are set in the grooves (52c) of the cover members (52b).
  • the printed wiring board (53) is disposed at the back (bottom surface) of the cold receiving member (19), and the cold receiving member (19) and the printed wiring board (53) are positioned and fixed in such a manner that the cooler (18) of the cryogenic refrigerator directly contacts the center of the bottom surface of the cold receiving member (19). At this time, the wiring of the printed wiring board also serves as a thermal anchor. Under this construction, since respective pins (53a) of the connecters (53d) are set in the concavities (55) of the cold receiving member (19), the pins do not short-circuit to one another.
  • the radiant heat shield members (21a), (21b) and the vacuum chamber (3) are attached. Requisite wiring to the printed wiring board (53) is also conducted. In general, the above processes are previously conducted. Accordingly, when the magnetometer unit (B) is attached to the cold receiving member (19), the vacuum chamber (3) and the radiant heat shield members (21a), (21b) are removed so that the cold receiving member (19) is exposed to the outside. In such a condition, the magnetometer units (B) are attached to the cold receiving member (19) in such a manner that the male screw part (51a) is screwed into the female screw hole (54).
  • each magnetometer unit (B) is only a screwing and the superconducting shield member (52) is attached to the concavity (51c) of the high thermally-conductive member (51). This minimizes the space between the adjacent magnetometer units (B), (B).
  • the lead wire (52f) in which the connecter (52g) is attached to the free end thereof hangs downward from the printed wiring board (53). Accordingly, if merely the connecter (52g) is connected to the corresponding connecter (53g) of the printed wiring board (53), requisite wiring can be readily accomplished.
  • the radiant heat shield member (21a), (21b) are attached and then the vacuum chamber (3) is attached.
  • the inner space of the vacuum chamber (3) is made vacuous and the cryogenic refrigerator is operated to cool all the SQUID magnetometers below the transition temperature of superconductivity. In this condition, a biomagnetic field is measured by the SQUID magnetometers.
  • Each of the magnetometer units (B) has two SQUID magnetometers. Accordingly, when the magnetometers are used for signal detection and for reference respectively in the above measuring, noise component resulting from, for example, the cryogenic refrigerator is removed thereby obtaining magnetic-field measuring signals with high precision.
  • each SQUID magnetometer has a pick-up coil (33) of first-order differential type
  • a set factor is multiplied to an output of one of the SQUID magnetometers and the multiplied value is subtracted from an output of another SQUID magnetometer, thereby obtaining a measuring signal equivalent to a SQUID magnetometer having a pick-up coil of second-order differential type which is well-balanced at 100%.
  • the present invention is applicable to a magnetic sensor composed of a SQUID magnetometer other than that for measuring magnetic waves from a human heart.
  • a SQUID which operates on a level of cryogenic temperature and a pick-up coil wound around a bobbin can be cooled below a transition temperature of superconductivity by the cryogenic refrigerator, without using liquid helium which requires much skill in operation.
  • cooling from a cooling stage is smoothly conducted to the bobbin, thereby readily cooling the bobbin. This allows the pick-up coil to be cooled below the transition temperature of superconductivity at a short time.

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  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Measuring Magnetic Variables (AREA)
  • Superconductor Devices And Manufacturing Methods Thereof (AREA)
  • Measurement And Recording Of Electrical Phenomena And Electrical Characteristics Of The Living Body (AREA)
  • Containers, Films, And Cooling For Superconductive Devices (AREA)
EP93916252A 1992-03-06 1993-08-02 Magnetic sensor and magnetic detector Expired - Lifetime EP0663599B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP4049397A JP2882167B2 (ja) 1992-03-06 1992-03-06 Ｓｑｕｉｄ磁束計
PCT/JP1993/001081 WO1995004287A1 (en) 1992-03-06 1993-08-02 Magnetic sensor and magnetic detector

Publications (3)

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EP0663599A1 EP0663599A1 (en) 1995-07-19
EP0663599A4 EP0663599A4 (en) 1996-03-06
EP0663599B1 true EP0663599B1 (en) 1997-05-14

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US (1) US5666052A (fi)
EP (1) EP0663599B1 (fi)
JP (1) JP2882167B2 (fi)
DE (1) DE69310755T2 (fi)
FI (1) FI943868A (fi)
WO (1) WO1995004287A1 (fi)

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US9239314B2 (en) 2013-03-13 2016-01-19 Endomagnetics Ltd. Magnetic detector
US9427186B2 (en) 2009-12-04 2016-08-30 Endomagnetics Ltd. Magnetic probe apparatus

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US5880583A (en) * 1996-12-27 1999-03-09 The United States Of America As Represented By The Secretary Of Commerce Cryogenic current comparator based on liquid nitrogen temperature superconductors
US6181530B1 (en) * 1998-07-31 2001-01-30 Seagate Technology Llc Heat sink for a voice coil motor
JP2001255358A (ja) * 2000-03-10 2001-09-21 Sumitomo Electric Ind Ltd 磁気センサ
JP4132720B2 (ja) * 2001-05-07 2008-08-13 独立行政法人科学技術振興機構 量子干渉型磁束計の製造方法
US6600633B2 (en) 2001-05-10 2003-07-29 Seagate Technology Llc Thermally conductive overmold for a disc drive actuator assembly
GB2425610A (en) * 2005-04-29 2006-11-01 Univ London Magnetic properties sensing system
JP5022660B2 (ja) * 2006-10-06 2012-09-12 株式会社日立ハイテクノロジーズ 磁場計測装置
JP5134447B2 (ja) * 2008-06-10 2013-01-30 国立大学法人九州工業大学 ピストンシリンダー型の高圧力発生装置
US10634741B2 (en) 2009-12-04 2020-04-28 Endomagnetics Ltd. Magnetic probe apparatus
WO2013053498A2 (en) * 2011-10-14 2013-04-18 Fluid Automation Systems S.A. Solenoid valve with a metallic tube bobbin
KR101403318B1 (ko) 2012-10-29 2014-06-05 한국표준과학연구원 초전도 양자 간섭 소자의 간접 냉각 장치 및 그 방법
WO2014140543A1 (en) 2013-03-11 2014-09-18 Endomagnetics Ltd. Hypoosmotic solutions for lymph node detection
KR101520801B1 (ko) * 2013-10-24 2015-05-18 한국표준과학연구원 Squid 센서 모듈 및 뇌자도 측정 장치
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US9427186B2 (en) 2009-12-04 2016-08-30 Endomagnetics Ltd. Magnetic probe apparatus
US9234877B2 (en) 2013-03-13 2016-01-12 Endomagnetics Ltd. Magnetic detector
US9239314B2 (en) 2013-03-13 2016-01-19 Endomagnetics Ltd. Magnetic detector
US9523748B2 (en) 2013-03-13 2016-12-20 Endomagnetics Ltd Magnetic detector

Also Published As

Publication number Publication date
JPH05251774A (ja) 1993-09-28
DE69310755D1 (de) 1997-06-19
US5666052A (en) 1997-09-09
JP2882167B2 (ja) 1999-04-12
FI943868A0 (fi) 1994-08-23
WO1995004287A1 (en) 1995-02-09
EP0663599A4 (en) 1996-03-06
EP0663599A1 (en) 1995-07-19
DE69310755T2 (de) 1997-08-28
FI943868A (fi) 1994-08-23

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