EP0484542B1 - Composition lubrifiante pour la transformation des metaux - Google Patents
Composition lubrifiante pour la transformation des metaux Download PDFInfo
- Publication number
- EP0484542B1 EP0484542B1 EP91908465A EP91908465A EP0484542B1 EP 0484542 B1 EP0484542 B1 EP 0484542B1 EP 91908465 A EP91908465 A EP 91908465A EP 91908465 A EP91908465 A EP 91908465A EP 0484542 B1 EP0484542 B1 EP 0484542B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- carbon atoms
- weight
- denotes
- alkyl group
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- 0 C1CC*CC1 Chemical compound C1CC*CC1 0.000 description 2
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- C—CHEMISTRY; METALLURGY
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M127/00—Lubricating compositions characterised by the additive being a non- macromolecular hydrocarbon
- C10M127/02—Lubricating compositions characterised by the additive being a non- macromolecular hydrocarbon well-defined aliphatic
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- C10M101/00—Lubricating compositions characterised by the base-material being a mineral or fatty oil
- C10M101/02—Petroleum fractions
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- C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
- C10M105/02—Well-defined hydrocarbons
- C10M105/04—Well-defined hydrocarbons aliphatic
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- C10M129/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
- C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/01—Emulsions, colloids, or micelles
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2080/00—Special pretreatment of the material to be lubricated, e.g. phosphatising or chromatising of a metal
Definitions
- the present invention relates to a lubricating oil composition for metal working, particularly to a lubricating oil composition which comprises a specific type of straight chain olefin, alcohol and the like, and which has excellent detergency (removability) of abrasion dust produced in metal working of aluminum and aluminum alloy.
- the present inventors have earnestly pursued the studies in order to develop a lubricating oil for metal working which has excellent removability (detergency) of abrasion dust produced in metal working such as plastic working, cutting, and grinding performed on various kinds of metal such as aluminum, steel and brass, and alloys thereof, which is excellent in workability and capable of finishing the surface of a worked material in an excellent condition.
- the straight chain olefin constituting the base oil of the component (a) has 6 to 40 carbon atoms as described above.
- the straight chain olefin with the carbon atoms of less than 6 is undesirable because of a low flash point. If the number of carbon atoms is more than 40, the practical use is difficult because of a solid state. Furthermore, there become difficult the mixing with and the dissolving in mineral oil, synthetic oil, and other additives.
- the straight chain olefin having more than 40 carbon atoms is not popular and is difficult to be available.
- the composition having one double bond in a molecule and 6 to 30 carbon atoms is preferable.
- ⁇ -olefin namely, n- ⁇ -olefin having 12 to 30 carbon atoms are most preferable.
- examples for the straight chain olefin may include 1-octene, 1-decene, 1-dodecene, 1-tetradecene, 1-hexadecene, 1-octadecene, 1-eicocene, or mixtures thereof.
- the straight chain olefin can be produced by various methods. For example, there may be used ethylene oligomer obtained by polymerization of ethylene in an ordinary method.
- mineral oil and/or synthetic oil is used together with the straight chain olefin. Water is excluded.
- Mineral oil and synthetic oil to be added have usually a kinematic viscosity of 0.5 to 500 cSt at a temperature of 40 °C, preferably, 0.5 to 30 cSt.
- Various kinds of mineral oil can be used, for example, distillate oil obtained through atmospheric distillation of paraffinic crude oil, intermediate crude oil, or naphthenic crude oil, or through vacuum distillation of residual oil in atmospheric distillation.
- synthetic oil there may be used various types of olefin other than the above-mentioned straight chain olefin (for example, branched chain olefin such as polybutene and polypropylene), and hydrogenated product of such olefin.
- olefin other than the above-mentioned straight chain olefin (for example, branched chain olefin such as polybutene and polypropylene), and hydrogenated product of such olefin.
- polybutene having low molecular weight, polypropylene having low molecular weight, and ⁇ -olefin oligomer having 8 to 14 carbon atoms are preferable.
- the resultant lubricating oil emits less odor during its use so as to improve working environment. Further, degreasing ability on the surface of a worked product is improved.
- the mineral oil or the synthetic oil is mixed with the above-mentioned straight chain olefin to constitute the base oil of the component (a), the amount of the straight chain olefin is at least 3% by weight, preferably 5 to 60% by weight, while the amount of the mineral oil and/or the synthetic oil is at most 97% by weight, preferably, 95 to 40% by weight.
- component (b) in the composition according to the present invention there is used one member selected from the group consisting of alcohol and fatty acid, or a combination of both members.
- alcohol various alcohols may be used, and among them, aliphatic alcohol is preferable. Branched chain saturated or unsaturated aliphatic alcohol having 6 to 40 carbon atoms (especially 8 to 30 carbon atoms), or straight chain saturated or unsaturated aliphatic alcohol having 6 to 20 carbon atoms (especially 8 to 18 carbon atoms) is more preferable. The alcohol having less than 6 carbon atoms is rapidly consumed due to evaporation or splashing during its use and thus is economically disadvantageous. Branched chain alcohol having more than 40 carbon atoms or straight chain alcohol having more than 20 carbon atoms is sometimes undesirable since it may be insoluble in the base oil of the component (a).
- Examples for such alcohol may include octyl (2-ethylhexyl) alcohol, decyl alcohol, lauryl alcohol, myristyl alcohol, cetyl alcohol, stearyl alcohol, eicosyl alcohol, oleyl alcohol, isostearyl alcohol, oxoalcohol, and the like.
- the amount of the alcohol is not limited, but it is suitable to use 0.05 to 50% by weight, preferably, 0.1 to 20% by weight, based on total amount of the composition.
- fatty acid there are used straight/branched chain saturated/unsaturated fatty acid having 6 to 40 carbon atoms (preferably 8 to 20 carbon atoms). There is a risk that fatty acid having less than 6 carbon atoms are rapidly consumed due to evaporation or splashing during its use, while fatty acid having more than 40 carbon atoms is sometimes insoluble in the base oil of the component (a).
- fatty acid examples include caprylic acid, capric acid, lauric acid, myristic acid, palmitic acid, stearic acid, arachic acid, behenic acid, isostearic acid, undecylenic acid, oleic acid, linoleic acid, linolenic acid, arachidonic acid, and the like.
- the amount of fatty acid is 0.05 to 1.0% by weight, based on the total amount of the composition. If the amount of fatty acid exceeds 1.0% by weight, the anti-stain ability in annealing is unfavorably deteriorated.
- composition according to the present invention comprises the above-mentioned components (a), (b) and (c) comprising at least one compound selected from the group consisting of phenolic compounds and amine compounds.
- each of R4 and R5 denotes an alkyl group having 1 to 8 carbon atoms
- each of R6 and R7 denotes a hydrogen atom or an alkyl group having 1 to 6 carbon atoms.
- DBPC 2,6-di-tert-butyl-4-metylphenol
- 2,6-di-tert-butyl-4-ethylphenol 2,2'-methylenebis (4-methyl-6-tert-butylphenol), 2,2'-methylenebis (4-ethyl-6-tert-butylphenol), and the like are preferable.
- each of R8 and R11 denotes a hydrogen atom or an alkyl group having 1 to 10 carbon atoms
- each of R9 and R10 denotes an alkyl group having 1 to 20 carbon atoms
- each of R12 to R14 denotes a hydrogen atom or an alkyl group having 1 to 20 carbon atoms.
- di-p-octyldiphenylamine, di-p-butyldiphenylamine, di-p-nonyldiphenylamine, phenyl- ⁇ -naphthylamine, phenyl- ⁇ -naphtylamine, and the like are preferable.
- the amount of the component (c) is preferably not less than 0.1% by weight, more preferably 0.1 to 2.0% by weight, based on the total amount of the composition.
- an oiliness agent an extreme-pressure agent, a rust inhibitor, a corrosion inhibitor, a defoaming agent, or the like may be blended with the composition according to the present invention.
- a JIS A 5052 H16 aluminum plate (a coiled plate having a thickness of 1.2 mm and a width of 60 mm) was prepared as a material to be rolled.
- the plate was rolled by a four-stage rolling mill having a work roll diameter of 135 mm at a rolling speed of 100 m/min. under forward tensions of 170 kgf and 400 kgf.
- the rolling process was carried out in such a manner that the reduction was stepwise increased per 20 m length during one pass as 50.0 ⁇ 54.2 ⁇ 58.3 ⁇ 60.8 ⁇ 63.3 ⁇ 65.8 ⁇ 68.3 (%).
- the plate having a thickness of 0.38 mm (a draft of 68.3 %) after the rolling process (after seven passes), the rolling load was measured.
- Abrasion dust detergency and anti-stain ability were evaluated by the following methods.
- a cellophane tape was stuck onto the surface of the aluminum plate after rolling so as to pick up abrasion dust adhering thereto. Then, the tape was applied on a white paper sheet to visually determine a degree of contamination by abrasion dust. Thus, the detergency for abrasion dust adhering to the surface of the aluminum plate was evaluated. The results thus obtained are shown in Table 1.
- the aluminum plate after rolling was cut into piece having a short length of 10 cm.
- the stack of several tens of the cut pieces were fixed by a thick steel plate and annealed in a small-size annealing furnace.
- the heating process in the annealing furnace comprises the step of: heating in an air atmosphere with a temperature rising rate of 5 °C/min. until the temperature reaches 330 °C; holding for 30 minutes; and cooling. After completion of the heating process, a degree of occurrence of annealing stains on the annealed plate was visually determined. Thus, the anti-stain ability was evaluated. The results are shown in Table 1.
- a cylindrical aluminum alloy material (AC-4A-T6) having a diameter of 80 mm was prepared as a material to be cut.
- the aluminum alloy material was cut to form an end face by the use of a cutting tool (cemented carbide P20) under the cutting condition that a cutting depth (t) is 1 mm and a feed rate (f) is 0.1 mm/revolution.
- abrasion dust detergency is improved in metal working (plastic working such as rolling, drawing, blanking, cold forging; cutting; and grinding) for various kinds of metals and alloys thereof while anti-stain ability in annealing of a worked material is improved.
- a lubricating oil composition according to the present invention is widely and effectively used as a metal working oil in plastic working, cutting, or grinding of various kinds of metals and alloys such as aluminum, aluminum alloy, aluminum foil.
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Lubricants (AREA)
Abstract
Claims (2)
- Une composition d'huile lubrifiante pour le travail des métaux constituée essentiellement de(a) une huile de base qui contient comme constituant essentiel au moins 3 % en poids d'une oléfine à chaîne droite ayant de 6 à 40 atomes de carbone en mélange avec au maximum 97 % en poids d'une huile minérale et/ou d'une huile synthétique ; les pourcentages en poids étant basés sur le poids de l'huile de base ;(b) au moins un constituant choisi parmi 0,05 à 50 % en poids d'un alcool aliphatique saturé ou insaturé à chaîne ramifiée ayant 6 à 40 atomes de carbone ou d'un alcool aliphatique saturé ou insaturé à chaîne droite ayant 6 à 20 atomes de carbone et 0,05 à 1,0 % en poids d'un acide gras saturé ou insaturé à chaîne droite ou ramifiée ayant 6 à 40 atomes de carbone, par rapport à la quantité totale de la composition ; et(c) pas moins de 0,1 % en poids, par rapport à la quantité totale de la composition, d'au moins un composé choisi dans le groupe constitué par un composé phénolique représenté par la formule générale (II) ou (III) suivante
l'eau étant exclue. - Une composition d'huile lubrifiante pour le travail des métaux selon la revendication 1, qui contient en outre (d) au moins un composé choisi dans le groupe constitué par les agents d'onctuosité, les agents extrême-pression, les agents antirouille, les inhibiteurs de corrosion et les agents antimousse.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12136190 | 1990-05-14 | ||
JP121361/90 | 1990-05-14 | ||
PCT/JP1991/000534 WO1991018074A1 (fr) | 1990-05-14 | 1991-04-23 | Composition lubrifiante pour la transformation des metaux |
Publications (3)
Publication Number | Publication Date |
---|---|
EP0484542A1 EP0484542A1 (fr) | 1992-05-13 |
EP0484542A4 EP0484542A4 (en) | 1992-10-21 |
EP0484542B1 true EP0484542B1 (fr) | 1995-11-15 |
Family
ID=14809351
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP91908465A Expired - Lifetime EP0484542B1 (fr) | 1990-05-14 | 1991-04-23 | Composition lubrifiante pour la transformation des metaux |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP0484542B1 (fr) |
KR (1) | KR970010855B1 (fr) |
DE (1) | DE69114672T2 (fr) |
WO (1) | WO1991018074A1 (fr) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2927644B2 (ja) * | 1993-07-02 | 1999-07-28 | 出光興産株式会社 | 金属加工油組成物 |
CA2099526C (fr) * | 1993-07-02 | 2005-06-21 | Hydro-Quebec | Additifs pour lubrifiants utilises dans le laminage de feuillards de lithium en films minces |
EP0690121A3 (fr) * | 1994-06-27 | 1996-07-31 | Carrier Corp | Subrifiant pour le formage de métaux |
EP1000674B1 (fr) * | 1994-07-12 | 2005-05-11 | Hydro-Quebec | Procédé d'élaboration d'un film mince de métal alcalin ou d'alliage de métal alcalin, par laminage d'un feuillard en présence d'une composition lubrifiante |
JP3490148B2 (ja) * | 1994-08-10 | 2004-01-26 | 出光興産株式会社 | 金属加工用潤滑油組成物 |
JP3354024B2 (ja) * | 1994-12-22 | 2002-12-09 | 株式会社神戸製鋼所 | アルミニウム及びアルミニウム合金板の低温成形用潤滑剤 |
JP3529069B2 (ja) * | 1995-11-29 | 2004-05-24 | 出光興産株式会社 | 金属加工油組成物 |
KR20020039565A (ko) * | 2000-11-22 | 2002-05-27 | 이구택 | 미스트 발생이 억제되는 강판 연마용 연삭유 |
JP2002322487A (ja) * | 2001-04-26 | 2002-11-08 | Idemitsu Kosan Co Ltd | 金属加工用潤滑油組成物 |
JP2003096481A (ja) * | 2001-09-21 | 2003-04-03 | Nippon Oil Corp | アルミニウム加工用潤滑油組成物 |
JP2003096482A (ja) * | 2001-09-21 | 2003-04-03 | Nippon Oil Corp | アルミニウム加工用潤滑油組成物 |
JP4741816B2 (ja) * | 2004-07-09 | 2011-08-10 | 住友軽金属工業株式会社 | 冷間圧延潤滑油 |
EP3957708A1 (fr) | 2020-08-17 | 2022-02-23 | Speira GmbH | Lubrifiant de refroidissement pour laminage à froid de l'aluminium |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB964268A (en) * | 1961-12-05 | 1964-07-22 | Aluminium Lab Ltd | Improvements in or relating to lubricants |
US3288715A (en) * | 1963-10-24 | 1966-11-29 | Gen Electric | Fabricating aluminum products with olefin lubricants |
US3536622A (en) * | 1967-12-11 | 1970-10-27 | Sinclair Research Inc | Biodegradable emulsifiable lubricant compositions |
DE3035016C2 (de) * | 1980-09-12 | 1985-02-21 | Schweizerische Aluminium Ag, Chippis | Oel-in-Wasser-Emulsion zum Kaltwalzen von Leichtmetallen |
JPS63202697A (ja) * | 1987-02-18 | 1988-08-22 | Nippon Guriisu Kk | 鏡面加工用金属加工油剤 |
JPH01153794A (ja) * | 1987-12-10 | 1989-06-15 | Hakutou Kagaku Kk | アルミニウム冷間加工用潤滑油 |
JP2551459B2 (ja) * | 1988-05-10 | 1996-11-06 | 株式会社日立製作所 | 伸線加工用潤滑油 |
JPH0726110B2 (ja) * | 1988-09-20 | 1995-03-22 | 株式会社日立製作所 | 導電線の製造方法 |
US5072067A (en) * | 1988-11-15 | 1991-12-10 | Idemitsu Kosan Company Limited | Lubricating oil composition |
-
1991
- 1991-04-23 EP EP91908465A patent/EP0484542B1/fr not_active Expired - Lifetime
- 1991-04-23 WO PCT/JP1991/000534 patent/WO1991018074A1/fr active IP Right Grant
- 1991-04-23 KR KR1019920700066A patent/KR970010855B1/ko not_active IP Right Cessation
- 1991-04-23 DE DE69114672T patent/DE69114672T2/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
KR970010855B1 (ko) | 1997-07-01 |
EP0484542A4 (en) | 1992-10-21 |
EP0484542A1 (fr) | 1992-05-13 |
DE69114672D1 (de) | 1995-12-21 |
WO1991018074A1 (fr) | 1991-11-28 |
DE69114672T2 (de) | 1996-04-18 |
KR927003454A (ko) | 1992-12-18 |
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