EA201690318A1 - Способ извлечения воды, металлов и органических веществ при производстве поликарбоновой кислоты - Google Patents

Способ извлечения воды, металлов и органических веществ при производстве поликарбоновой кислоты

Info

Publication number
EA201690318A1
EA201690318A1 EA201690318A EA201690318A EA201690318A1 EA 201690318 A1 EA201690318 A1 EA 201690318A1 EA 201690318 A EA201690318 A EA 201690318A EA 201690318 A EA201690318 A EA 201690318A EA 201690318 A1 EA201690318 A1 EA 201690318A1
Authority
EA
Eurasian Patent Office
Prior art keywords
organic substances
metals
organic matter
polycarboxylic acid
water
Prior art date
Application number
EA201690318A
Other languages
English (en)
Other versions
EA030560B1 (ru
Inventor
Саймон Робертс
Джулиан Стюарт Грей
Original Assignee
Джонсон Мэтти Дэйви Текнолоджис Лимитед
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Джонсон Мэтти Дэйви Текнолоджис Лимитед filed Critical Джонсон Мэтти Дэйви Текнолоджис Лимитед
Publication of EA201690318A1 publication Critical patent/EA201690318A1/ru
Publication of EA030560B1 publication Critical patent/EA030560B1/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/24—Dialysis ; Membrane extraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/58—Multistep processes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/26—Further operations combined with membrane separation processes
    • B01D2311/263—Chemical reaction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/26—Further operations combined with membrane separation processes
    • B01D2311/2673—Evaporation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Supply & Treatment (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Urology & Nephrology (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

Способ извлечения воды, металлов, растворимых органических веществ и нерастворимых органических веществ в потоке маточного раствора со стадии разделения процесса производства поликарбоновой кислоты, в котором способ включает охлаждение потока до температуры, при которой растворенные органические вещества осаждаются; отделение осажденных органических веществ из потока жидкости и рециркулирование указанных органических веществ в процесс получения поликарбоновой кислоты; жидкий поток со стадии (b) затем обрабатывают щелочью для преобразования оставшихся органических веществ в форме щелочной соли и присутствующие металлы преобразовывают в нерастворимую форму; извлекают нерастворимые металлы из жидкого потока; пропускают поток жидкости со стадии (d), содержащий щелочные соли органических веществ, через блок мембранного разделения, где он разделяется на пермеат, содержащий воду, и ретентат, содержащий воду и щелочные соли органических веществ; извлекают пермеат и рециркулируют его в процесс получения поликарбоновой кислоты; и извлекают ретентат.
EA201690318A 2013-08-14 2014-07-31 Способ извлечения воды, металлов и органических веществ при производстве поликарбоновой кислоты EA030560B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GBGB1314561.0A GB201314561D0 (en) 2013-08-14 2013-08-14 Process
PCT/GB2014/052361 WO2015022493A1 (en) 2013-08-14 2014-07-31 Process for recovering water, metal and organics from the production of polycarboxylic acid

Publications (2)

Publication Number Publication Date
EA201690318A1 true EA201690318A1 (ru) 2016-10-31
EA030560B1 EA030560B1 (ru) 2018-08-31

Family

ID=49262166

Family Applications (1)

Application Number Title Priority Date Filing Date
EA201690318A EA030560B1 (ru) 2013-08-14 2014-07-31 Способ извлечения воды, металлов и органических веществ при производстве поликарбоновой кислоты

Country Status (14)

Country Link
US (1) US9505698B2 (ru)
EP (1) EP3033323B1 (ru)
JP (1) JP2016528243A (ru)
KR (1) KR20160042428A (ru)
CN (1) CN105517987B (ru)
BR (1) BR112016002764A2 (ru)
EA (1) EA030560B1 (ru)
ES (1) ES2641852T3 (ru)
GB (2) GB201314561D0 (ru)
MX (1) MX361189B (ru)
PL (1) PL3033323T3 (ru)
PT (1) PT3033323T (ru)
TW (1) TW201522244A (ru)
WO (1) WO2015022493A1 (ru)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110393958A (zh) * 2019-08-16 2019-11-01 南通百川新材料有限公司 一种隔膜压滤机滤饼洗涤装置及方法
CN114478232B (zh) * 2022-02-09 2023-03-17 河北海力香料股份有限公司 一种3,3′,4,4′-二苯醚四甲酸精制母液的回收处理方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3919306A (en) * 1970-05-18 1975-11-11 Atlantic Richfield Co Purification of recirculated stream for isophthalic acid production
BR9815459A (pt) * 1997-03-14 2001-10-16 Du Pont Processo para o tratamento de uma corrente efluente, processo para a produção de um ácido carboxìlico aromático e planta para a produção de um ácido carboxìlico aromático
US5980750A (en) * 1998-07-06 1999-11-09 Mobile Process Technology, Co. Process for the purification of waste wash water
EP1212278B1 (en) * 1999-08-30 2005-01-19 Mossi & Ghisolfi International S.A. A process for separation of crude naphthalene dicarboxylic acid using reverse osmosis
CN102137707B (zh) * 2008-08-26 2013-08-21 瑞来斯实业公司 用于从对苯二甲酸生产中回收有价值的物质的方法和设备
CN101391952B (zh) * 2008-11-12 2012-02-22 中国石油化工股份有限公司 对苯二甲酸/间苯二甲酸精制母液回收方法
BRPI1006621A2 (pt) * 2009-04-24 2016-04-19 INVISTA Technologies S à r l "método de resfriar uma corrente de água-mãe"

Also Published As

Publication number Publication date
CN105517987A (zh) 2016-04-20
TW201522244A (zh) 2015-06-16
JP2016528243A (ja) 2016-09-15
PT3033323T (pt) 2017-12-06
MX361189B (es) 2018-11-29
PL3033323T3 (pl) 2018-01-31
US9505698B2 (en) 2016-11-29
KR20160042428A (ko) 2016-04-19
MX2016001994A (es) 2016-05-18
US20160200658A1 (en) 2016-07-14
EP3033323B1 (en) 2017-08-30
BR112016002764A2 (pt) 2017-08-01
ES2641852T3 (es) 2017-11-14
EP3033323A1 (en) 2016-06-22
GB201413623D0 (en) 2014-09-17
EA030560B1 (ru) 2018-08-31
GB2520796B (en) 2018-04-04
GB2520796A (en) 2015-06-03
GB201314561D0 (en) 2013-09-25
CN105517987B (zh) 2017-09-19
WO2015022493A1 (en) 2015-02-19

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MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): AM AZ BY KZ KG TJ TM