EA199900353A1 - Получение 3,5-лутидина - Google Patents
Получение 3,5-лутидинаInfo
- Publication number
- EA199900353A1 EA199900353A1 EA199900353A EA199900353A EA199900353A1 EA 199900353 A1 EA199900353 A1 EA 199900353A1 EA 199900353 A EA199900353 A EA 199900353A EA 199900353 A EA199900353 A EA 199900353A EA 199900353 A1 EA199900353 A1 EA 199900353A1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- lutidina
- obtaining
- pentadiamine
- lutidine
- picoline
- Prior art date
Links
- HWWYDZCSSYKIAD-UHFFFAOYSA-N 3,5-dimethylpyridine Chemical compound CC1=CN=CC(C)=C1 HWWYDZCSSYKIAD-UHFFFAOYSA-N 0.000 abstract 2
- ITQTTZVARXURQS-UHFFFAOYSA-N 3-methylpyridine Chemical compound CC1=CC=CN=C1 ITQTTZVARXURQS-UHFFFAOYSA-N 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000012808 vapor phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/06—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
- C07D213/08—Preparation by ring-closure
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/06—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
- C07D213/08—Preparation by ring-closure
- C07D213/09—Preparation by ring-closure involving the use of ammonia, amines, amine salts, or nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
Abstract
Настоящее изобретение представляет способ получения 3,5-лутидина и 3-пиколина из 2-метил-1,5-пентадиамина парофазной реакцией с водородом при приблизительно 400-500°С над окисным катализатором.Международная заявка была опубликована вместе с отчетом о международном поиске.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/725,434 US5708176A (en) | 1996-10-03 | 1996-10-03 | Preparation of 3,5-lutidene |
PCT/US1997/017730 WO1998014428A1 (en) | 1996-10-03 | 1997-10-03 | Preparation of 3,5-lutidine |
Publications (2)
Publication Number | Publication Date |
---|---|
EA199900353A1 true EA199900353A1 (ru) | 1999-08-26 |
EA001774B1 EA001774B1 (ru) | 2001-08-27 |
Family
ID=24914539
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EA199900353A EA001774B1 (ru) | 1996-10-03 | 1997-10-03 | Способ получения 3,5-диметилпиридина (3,5-лутидина) и 3-метилпиридина (3-пиколина) |
Country Status (9)
Country | Link |
---|---|
US (1) | US5708176A (ru) |
EP (1) | EP0929523B1 (ru) |
JP (1) | JP2001501623A (ru) |
KR (1) | KR100474624B1 (ru) |
CA (1) | CA2263912A1 (ru) |
DE (1) | DE69705849T2 (ru) |
EA (1) | EA001774B1 (ru) |
TW (1) | TW426668B (ru) |
WO (1) | WO1998014428A1 (ru) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102164895A (zh) * | 2008-09-26 | 2011-08-24 | 帝斯曼知识产权资产管理有限公司 | 3-甲基吡啶的制备方法 |
RU2474473C1 (ru) * | 2011-09-16 | 2013-02-10 | Российская Федерация, От Имени Которой Выступает Министерство Промышленности И Торговли Российской Федерации | КАТАЛИЗАТОР, СПОСОБ ЕГО ПРИГОТОВЛЕНИЯ И СПОСОБ ПОЛУЧЕНИЯ β-ПИКОЛИНА |
CN103301823A (zh) * | 2012-03-15 | 2013-09-18 | 清华大学 | 催化剂及其用途 |
CN103044317B (zh) * | 2013-01-07 | 2015-07-29 | 清华大学 | 制备3-甲基吡啶的方法和系统 |
CN104492479B (zh) * | 2014-12-10 | 2017-01-11 | 中国科学院大连化学物理研究所 | 一种3-甲基吡啶制吡啶催化剂及其制备方法 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1795239B2 (de) * | 1968-08-27 | 1978-04-20 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von symmetrischen 3,5-Dialkylpyridinen |
DE2045880A1 (de) * | 1970-09-17 | 1972-03-23 | Farbenfabriken Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von 3,5-Dimethylpyridin |
US4189585A (en) * | 1970-12-04 | 1980-02-19 | Stamicarbon, B.V. | Process for the preparation of pyridine and 2,6-lutidine |
DE3104765A1 (de) * | 1981-02-11 | 1982-09-02 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von pyridinen oder pyrrolen aus (alpha),(omega)-dinitrilen |
CH656879A5 (de) * | 1981-07-09 | 1986-07-31 | Lonza Ag | Verfahren zur herstellung von 3,5-dialkylpyridinen. |
US5149816A (en) * | 1988-07-11 | 1992-09-22 | Reilly Industries | High temperature process for selective production of 3-methylpyridine |
-
1996
- 1996-10-03 US US08/725,434 patent/US5708176A/en not_active Expired - Fee Related
-
1997
- 1997-10-03 EP EP97909923A patent/EP0929523B1/en not_active Expired - Lifetime
- 1997-10-03 DE DE69705849T patent/DE69705849T2/de not_active Expired - Fee Related
- 1997-10-03 CA CA002263912A patent/CA2263912A1/en not_active Abandoned
- 1997-10-03 EA EA199900353A patent/EA001774B1/ru not_active IP Right Cessation
- 1997-10-03 WO PCT/US1997/017730 patent/WO1998014428A1/en active IP Right Grant
- 1997-10-03 KR KR10-1999-7002852A patent/KR100474624B1/ko not_active IP Right Cessation
- 1997-10-03 JP JP10516849A patent/JP2001501623A/ja not_active Withdrawn
- 1997-10-16 TW TW086115246A patent/TW426668B/zh not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
JP2001501623A (ja) | 2001-02-06 |
TW426668B (en) | 2001-03-21 |
WO1998014428A1 (en) | 1998-04-09 |
DE69705849D1 (de) | 2001-08-30 |
DE69705849T2 (de) | 2002-04-04 |
KR100474624B1 (ko) | 2005-03-08 |
CA2263912A1 (en) | 1998-04-09 |
EP0929523A1 (en) | 1999-07-21 |
US5708176A (en) | 1998-01-13 |
KR20000048850A (ko) | 2000-07-25 |
EP0929523B1 (en) | 2001-07-25 |
EA001774B1 (ru) | 2001-08-27 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
Designated state(s): AM AZ BY KZ KG MD TJ TM RU |