DE69512227D1 - Einstufiges kristallisationsverfahren bei konstanter temperatur zur rückgewinnung von paraxylol - Google Patents
Einstufiges kristallisationsverfahren bei konstanter temperatur zur rückgewinnung von paraxylolInfo
- Publication number
- DE69512227D1 DE69512227D1 DE69512227T DE69512227T DE69512227D1 DE 69512227 D1 DE69512227 D1 DE 69512227D1 DE 69512227 T DE69512227 T DE 69512227T DE 69512227 T DE69512227 T DE 69512227T DE 69512227 D1 DE69512227 D1 DE 69512227D1
- Authority
- DE
- Germany
- Prior art keywords
- paraxylol
- recovery
- constant temperature
- crystalization process
- crystalization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
- C07C15/02—Monocyclic hydrocarbons
- C07C15/067—C8H10 hydrocarbons
- C07C15/08—Xylenes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C6/00—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions
- C07C6/08—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond
- C07C6/12—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond of exclusively hydrocarbons containing a six-membered aromatic ring
- C07C6/123—Preparation of hydrocarbons from hydrocarbons containing a different number of carbon atoms by redistribution reactions by conversion at a saturated carbon-to-carbon bond of exclusively hydrocarbons containing a six-membered aromatic ring of only one hydrocarbon
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/14—Purification; Separation; Use of additives by crystallisation; Purification or separation of the crystals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Water Supply & Treatment (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/223,063 US5498822A (en) | 1994-04-04 | 1994-04-04 | Single temperature stage crystallization of paraxylene |
PCT/US1995/003519 WO1995026947A1 (en) | 1994-04-04 | 1995-03-20 | Single temperature stage crystalization to recover paraxylene |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69512227D1 true DE69512227D1 (de) | 1999-10-21 |
DE69512227T2 DE69512227T2 (de) | 1999-12-30 |
Family
ID=22834861
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69512227T Expired - Fee Related DE69512227T2 (de) | 1994-04-04 | 1995-03-20 | Einstufiges kristallisationsverfahren bei konstanter temperatur zur rückgewinnung von paraxylol |
Country Status (10)
Country | Link |
---|---|
US (1) | US5498822A (de) |
EP (1) | EP0754169B1 (de) |
JP (1) | JPH09511504A (de) |
KR (1) | KR100332947B1 (de) |
AU (1) | AU684976B2 (de) |
CA (1) | CA2186456C (de) |
DE (1) | DE69512227T2 (de) |
ES (1) | ES2135721T3 (de) |
TW (1) | TW323268B (de) |
WO (1) | WO1995026947A1 (de) |
Families Citing this family (32)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2728894A1 (fr) * | 1994-12-29 | 1996-07-05 | Inst Francais Du Petrole | Procede de separation de paraxylene comportant au moins deux etages de cristallisation a haute temperature |
US5811629A (en) * | 1995-09-22 | 1998-09-22 | Raytheon Engineers & Constructors, Inc. | Crystallization process for purification of paraxylene |
US5961545A (en) * | 1997-01-17 | 1999-10-05 | Meadox Medicals, Inc. | EPTFE graft-stent composite device |
US5971907A (en) * | 1998-05-19 | 1999-10-26 | Bp Amoco Corporation | Continuous centrifugal separator with tapered internal feed distributor |
US6398947B2 (en) | 1999-09-27 | 2002-06-04 | Exxon Mobil Oil Corporation | Reformate upgrading using zeolite catalyst |
US7381858B2 (en) * | 2004-01-30 | 2008-06-03 | Bp Corporation North America Inc. | Xylene process using perm-selective separations |
US7358414B2 (en) * | 2004-01-30 | 2008-04-15 | Miller Jeffrey T | Para-xylene process using perm-selective separations |
US7249469B2 (en) * | 2004-11-18 | 2007-07-31 | Exxonmobil Chemical Patents Inc. | Method for separating a multicomponent stream |
US7812206B2 (en) * | 2006-03-21 | 2010-10-12 | Bp Corporation North America Inc. | Apparatus and process for the separation of solids and liquids |
CN103288569B (zh) | 2007-04-04 | 2015-09-23 | 埃克森美孚化学专利公司 | 对二甲苯生产的方法和装置 |
US8530716B2 (en) * | 2008-08-14 | 2013-09-10 | Bp Corporation North America Inc. | Melt-crystallization separation and purification process |
WO2010059317A2 (en) | 2008-11-19 | 2010-05-27 | Exxonmobil Chemical Patents Inc. | Separation process |
CN101735001B (zh) * | 2008-11-21 | 2013-04-03 | 中国石油化工股份有限公司 | 对二甲苯结晶分离的方法 |
CN101941882B (zh) * | 2009-07-06 | 2013-07-31 | 中国石油化工股份有限公司 | 由混合二甲苯分离对二甲苯的方法 |
CN102371081B (zh) * | 2010-08-23 | 2013-12-04 | 中国石油化工股份有限公司 | 带细晶消除的结晶方法 |
CN102371080B (zh) * | 2010-08-23 | 2013-12-04 | 中国石油化工股份有限公司 | 晶浆外循环的结晶方法 |
CN102371082B (zh) * | 2010-08-23 | 2013-08-21 | 中国石油化工股份有限公司 | 带清母液溢流的结晶方法 |
CN102701899A (zh) * | 2012-06-21 | 2012-10-03 | 大连理工大学 | 甲苯甲醇烷基化生产对二甲苯节能减排工艺 |
CN103664491B (zh) * | 2012-09-05 | 2015-07-08 | 中国石油化工股份有限公司 | 对二甲苯的生产方法 |
CN103772130B (zh) * | 2012-10-25 | 2015-10-21 | 中国石油化工股份有限公司 | 分离对二甲苯的结晶方法 |
CN104230638B (zh) * | 2013-06-17 | 2016-04-13 | 中国石油化工股份有限公司 | 悬浮结晶生产对二甲苯的方法 |
CN104230639B (zh) * | 2013-06-17 | 2016-06-08 | 中国石油化工股份有限公司 | 悬浮结晶分离对二甲苯的方法 |
CN104557424B (zh) * | 2013-10-28 | 2016-09-07 | 中国石油化工股份有限公司 | 多级悬浮结晶分离对二甲苯的方法 |
CN104557433B (zh) * | 2013-10-28 | 2017-08-25 | 中国石油化工股份有限公司 | 多级悬浮结晶生产对二甲苯的方法 |
EP3077104B1 (de) | 2014-06-06 | 2018-11-07 | Northwestern University | Kohlenhydratvermittelte reinigung von petrochemikalien |
CN106831303A (zh) * | 2015-12-03 | 2017-06-13 | 中国石油化工股份有限公司 | 分离对二甲苯的多级悬浮熔融结晶方法 |
CN106831301B (zh) * | 2015-12-03 | 2020-06-09 | 中国石油化工股份有限公司 | 多级悬浮熔融结晶分离对二甲苯的方法 |
CN106831302B (zh) * | 2015-12-03 | 2019-09-06 | 中国石油化工股份有限公司 | 悬浮熔融结晶生产对二甲苯的方法 |
CN106831311A (zh) * | 2015-12-03 | 2017-06-13 | 中国石油化工股份有限公司 | 生产对二甲苯的多级悬浮熔融结晶方法 |
CN106831312A (zh) * | 2015-12-03 | 2017-06-13 | 中国石油化工股份有限公司 | 悬浮熔融结晶分离对二甲苯的方法 |
US20220274900A1 (en) | 2019-08-23 | 2022-09-01 | Exxonmobil Chemical Patents Inc. | Processes for Isomerizing C8 Aromatic Hydrocarbons |
WO2021041022A1 (en) | 2019-08-23 | 2021-03-04 | Exxonmobil Chemical Patents Inc. | Processes for isomerizing c8 aromatic hydrocarbons using serial reactors |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE499776A (de) * | 1947-08-26 | |||
US2766309A (en) * | 1952-05-23 | 1956-10-09 | Exxon Research Engineering Co | Wash technique for paraxylene process |
NL278713A (de) * | 1961-05-22 | |||
US3462509A (en) * | 1967-05-22 | 1969-08-19 | Sinclair Research Inc | Separation of p-xylene from a c8 aromatic hydrocarbon mixture by crystallization |
GB1292812A (en) * | 1969-02-10 | 1972-10-11 | Ici Ltd | Separation process |
DE1934721C3 (de) * | 1969-07-09 | 1974-01-17 | Fried. Krupp Gmbh, 4300 Essen | Verfahren zum Abtrennen von Flüssigkeitsfilmen von p-Xylol-Kristallen |
DE1949446A1 (de) * | 1969-10-01 | 1972-02-03 | Krupp Gmbh | Verfahren zur Gewinnung von reinem p-Xylol |
US3662013A (en) * | 1970-02-03 | 1972-05-09 | Mobil Oil Corp | Single stage crystallization process for separating high purity paraxylene |
US3916018A (en) * | 1973-03-26 | 1975-10-28 | Atlantic Richfield Co | Separation of paraxylene |
DE2509182A1 (de) * | 1974-03-11 | 1975-10-02 | Standard Oil Co | Einstufiges kristallisationsverfahren zur gewinnung von hochgereinigtem p-xylol |
US4851604A (en) * | 1987-09-02 | 1989-07-25 | Mobil Oil Corp. | Toluene disproportionation |
DE3839229A1 (de) * | 1988-11-19 | 1990-05-23 | Krupp Koppers Gmbh | Verfahren zur gewinnung von p-xylol mit einer reinheit von mehr als 99,8 gew.-% |
EP0451941B1 (de) * | 1990-03-21 | 1993-06-30 | Mobil Oil Corporation | Katalysator und Verfahren zur selektiven Herstellung von Paradialkyl-substituierten Benzolen |
US5173461A (en) * | 1990-03-21 | 1992-12-22 | Mobil Oil Corporation | Toluene disproportionation catalyst |
US5243117A (en) * | 1990-06-05 | 1993-09-07 | Mobil Oil Corp. | Catalyst and process for the selective production of para-dialkyl substituted benzenes |
US5321183A (en) * | 1992-03-12 | 1994-06-14 | Mobil Oil Corp. | Process for the regioselective conversion of aromatics to para-disubstituted benzenes |
US5367099A (en) * | 1993-05-28 | 1994-11-22 | Mobil Oil Corp. | Selective toluene disproportionation process (STDP) with ex situ selectivated zeolite catalyst |
US5365004A (en) * | 1993-05-28 | 1994-11-15 | Mobil Oil Corp. | Selective toluene disproportionation process (STDP) with ex situ selectivated zeolite catalysts |
US5448005A (en) * | 1994-04-04 | 1995-09-05 | Mobil Oil Corporation | Crystallization of paraxlene from high purity paraxylene feeds |
-
1994
- 1994-04-04 US US08/223,063 patent/US5498822A/en not_active Expired - Fee Related
-
1995
- 1995-03-20 ES ES95914786T patent/ES2135721T3/es not_active Expired - Lifetime
- 1995-03-20 CA CA002186456A patent/CA2186456C/en not_active Expired - Fee Related
- 1995-03-20 EP EP95914786A patent/EP0754169B1/de not_active Expired - Lifetime
- 1995-03-20 DE DE69512227T patent/DE69512227T2/de not_active Expired - Fee Related
- 1995-03-20 WO PCT/US1995/003519 patent/WO1995026947A1/en active IP Right Grant
- 1995-03-20 AU AU21891/95A patent/AU684976B2/en not_active Ceased
- 1995-03-20 JP JP7525737A patent/JPH09511504A/ja active Pending
- 1995-03-20 KR KR1019960705479A patent/KR100332947B1/ko not_active IP Right Cessation
- 1995-03-30 TW TW084103052A patent/TW323268B/zh active
Also Published As
Publication number | Publication date |
---|---|
CA2186456A1 (en) | 1995-10-12 |
EP0754169A1 (de) | 1997-01-22 |
AU2189195A (en) | 1995-10-23 |
EP0754169B1 (de) | 1999-09-15 |
TW323268B (de) | 1997-12-21 |
WO1995026947A1 (en) | 1995-10-12 |
KR100332947B1 (ko) | 2002-09-17 |
ES2135721T3 (es) | 1999-11-01 |
EP0754169A4 (de) | 1996-12-10 |
CA2186456C (en) | 2006-05-30 |
AU684976B2 (en) | 1998-01-08 |
US5498822A (en) | 1996-03-12 |
JPH09511504A (ja) | 1997-11-18 |
DE69512227T2 (de) | 1999-12-30 |
KR970702231A (ko) | 1997-05-13 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8339 | Ceased/non-payment of the annual fee |