DE69511109D1 - Kristallisation der adipinsäure - Google Patents
Kristallisation der adipinsäureInfo
- Publication number
- DE69511109D1 DE69511109D1 DE69511109T DE69511109T DE69511109D1 DE 69511109 D1 DE69511109 D1 DE 69511109D1 DE 69511109 T DE69511109 T DE 69511109T DE 69511109 T DE69511109 T DE 69511109T DE 69511109 D1 DE69511109 D1 DE 69511109D1
- Authority
- DE
- Germany
- Prior art keywords
- crystallization
- adipic acid
- adipic
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1875—Stationary reactors having moving elements inside resulting in a loop-type movement internally, i.e. the mixture circulating inside the vessel such that the upwards stream is separated physically from the downwards stream(s)
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/80—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
- B01F31/85—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations with a vibrating element inside the receptacle
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/10—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/356,758 US5471001A (en) | 1994-12-15 | 1994-12-15 | Crystallization of adipic acid |
PCT/US1995/015553 WO1996018597A1 (en) | 1994-12-15 | 1995-12-04 | Crystallization of adipic acid |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69511109D1 true DE69511109D1 (de) | 1999-09-02 |
DE69511109T2 DE69511109T2 (de) | 2000-02-24 |
Family
ID=23402834
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69511109T Expired - Lifetime DE69511109T2 (de) | 1994-12-15 | 1995-12-04 | Kristallisation der adipinsäure |
Country Status (8)
Country | Link |
---|---|
US (1) | US5471001A (de) |
EP (1) | EP0797562B1 (de) |
JP (1) | JPH10510808A (de) |
KR (1) | KR987000253A (de) |
CN (1) | CN1169711A (de) |
DE (1) | DE69511109T2 (de) |
TW (1) | TW314514B (de) |
WO (1) | WO1996018597A1 (de) |
Families Citing this family (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB9624615D0 (en) * | 1996-11-26 | 1997-01-15 | Zeneca Ltd | Chrystallisation process |
US5966966A (en) * | 1997-05-21 | 1999-10-19 | Trustees Of Tufts College | Process and system for freeze concentration using ultrasonic nucleation useful in effluent processing |
GB9810859D0 (en) | 1998-05-20 | 1998-07-22 | Zeneca Ltd | Crystallisation process |
JP2002533926A (ja) * | 1998-12-21 | 2002-10-08 | インテル・コーポレーション | 埋込みフレームを有する窓付き非セラミック・パッケージ |
GB9828721D0 (en) * | 1998-12-24 | 1999-02-17 | Glaxo Group Ltd | Novel apparatus and process |
IL128001A (en) * | 1999-01-11 | 2005-09-25 | Rafael Armament Dev Authority | Method and apparatus for shaping particles, particularly of explosives, by ultrasonic cavitation |
US6458339B1 (en) * | 2000-02-11 | 2002-10-01 | Charles F. Cox | Acid resistant film forming dental composition and method of use |
US6423301B1 (en) * | 1999-02-16 | 2002-07-23 | Jeffrey S. Cox | Acid resistant film forming dental composition and method of use |
EP1033357A1 (de) * | 1999-03-02 | 2000-09-06 | Aerospace Propulsion Products B.V. | Verfahren zur Herstellung von kristallinen energetischen Materialen |
FR2795721B1 (fr) * | 1999-06-29 | 2003-04-18 | Rhone Poulenc Fibres | Procede de fabrication d'acide adipique |
DE19946671A1 (de) | 1999-09-29 | 2001-04-05 | Basf Ag | Verminderung der Krustenbildung bei Kristallisationsprozessen |
FR2803292B1 (fr) * | 1999-12-30 | 2002-02-15 | Rhodia Polyamide Intermediates | Procede de fabrication de sel de diamine et diacide carboxylique |
DE10123073A1 (de) * | 2001-05-11 | 2003-03-27 | Fraunhofer Ges Forschung | Verfahren zur Herstellung von Kristallen aus in einem Lösungsmittel gelösten Feststoffen |
DE10137017A1 (de) | 2001-07-30 | 2003-02-20 | Basf Ag | Kristallisationsverfahren zur Einstellung kleiner Partikel |
FR2829761B1 (fr) * | 2001-09-18 | 2004-02-20 | Rhodia Polyamide Intermediates | Procede de fabrication de cristaux d'acide adipique et cristaux ainsi obtenus |
GB0201400D0 (en) * | 2002-01-22 | 2002-03-13 | Glaxo Group Ltd | Novel apparatus and process |
US6946571B2 (en) * | 2003-09-30 | 2005-09-20 | Invista North America S.A.R.L. | Drying of adipic acid |
TW201029738A (en) * | 2009-02-11 | 2010-08-16 | Univ Nat Central | Method of lowering the sublimation points of small-molecular organic semiconductors |
FR2946646B1 (fr) * | 2009-06-16 | 2012-09-21 | Rhodia Operations | Procede de production de cristaux d'acide adipique |
CN102210940A (zh) * | 2010-04-07 | 2011-10-12 | 中川工程顾问(上海)有限公司 | 结晶装置和结晶方法 |
ES2715599T3 (es) * | 2012-01-20 | 2019-06-05 | Lianyungang Jinkang Hexin Pharmaceutical Co Ltd | Forma de cristal de sal de (6S)-5-metiltetrahidrofolato y método para preparar esta |
CN102872612B (zh) * | 2012-10-15 | 2013-11-27 | 中国工程物理研究院化工材料研究所 | 超声结晶器 |
US9855538B2 (en) | 2013-03-08 | 2018-01-02 | The Board Of Trustees Of The University Of Illinois | Ultrasonic method and apparatus for producing particles having a controlled size distribution |
AU2014284224B2 (en) * | 2013-06-21 | 2019-08-01 | Intra-Cellular Therapies, Inc. | Free base crystals |
DE102016008296B4 (de) * | 2016-07-05 | 2020-02-20 | Technische Universität Bergakademie Freiberg | Verfahren und Vorrichtung zur Sonokristallisation |
JP2021506914A (ja) * | 2017-12-22 | 2021-02-22 | ビーエイエスエフ・ソシエタス・エウロパエアBasf Se | アジピン酸から硝酸塩化合物を除去する方法 |
CN110433523A (zh) * | 2019-09-02 | 2019-11-12 | 齐鲁师范学院 | 基于声波干预的硫酸铜结晶方法 |
CN113754530B (zh) * | 2020-06-02 | 2023-09-29 | 中国石油化工股份有限公司 | 提纯己二酸的方法 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3123635A (en) * | 1964-03-03 | Agitation of adipic acid crystals to | ||
AT332362B (de) * | 1974-10-10 | 1976-09-27 | Erz & Stahl Ges M B H | Verfahren zur gewinnung von monocarbonsaureestern und dicarbonsauren oder deren estern aus den abfallsalzlosungen der cyclohexanonherstellung |
US4254283A (en) * | 1979-06-07 | 1981-03-03 | Monsanto Company | Process for preparing adipic acid with recovery of glutaric and succinic acids |
NL8006766A (nl) * | 1980-12-12 | 1982-07-01 | Tno | Kristallisatieinrichting en werkwijze voor het vormen van kristallen in een dergelijke inrichting. |
US4650507A (en) * | 1982-06-24 | 1987-03-17 | Cheng Chen Yen | Wet and dry distillative freezing process for separating mixtures and apparatuses for use therein |
IE852919L (en) * | 1985-11-21 | 1987-05-21 | Loctite Ireland Ltd | Activation of adhesive compositions |
-
1994
- 1994-12-15 US US08/356,758 patent/US5471001A/en not_active Expired - Lifetime
-
1995
- 1995-10-09 TW TW84110617A patent/TW314514B/zh active
- 1995-12-04 DE DE69511109T patent/DE69511109T2/de not_active Expired - Lifetime
- 1995-12-04 EP EP95941500A patent/EP0797562B1/de not_active Expired - Lifetime
- 1995-12-04 CN CN95196793A patent/CN1169711A/zh active Pending
- 1995-12-04 WO PCT/US1995/015553 patent/WO1996018597A1/en not_active Application Discontinuation
- 1995-12-04 JP JP8519048A patent/JPH10510808A/ja active Pending
-
1997
- 1997-06-13 KR KR19977003974A patent/KR987000253A/ko unknown
Also Published As
Publication number | Publication date |
---|---|
WO1996018597A1 (en) | 1996-06-20 |
JPH10510808A (ja) | 1998-10-20 |
EP0797562B1 (de) | 1999-07-28 |
EP0797562A1 (de) | 1997-10-01 |
TW314514B (en) | 1997-09-01 |
US5471001A (en) | 1995-11-28 |
KR987000253A (en) | 1998-03-30 |
CN1169711A (zh) | 1998-01-07 |
DE69511109T2 (de) | 2000-02-24 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8363 | Opposition against the patent | ||
8327 | Change in the person/name/address of the patent owner |
Owner name: INVISTA TECHNOLOGIES S.A.R.L., WILMINGTON, DEL, US |
|
8328 | Change in the person/name/address of the agent |
Representative=s name: MARKS & CLERK, LUXEMBOURG, LU |