DE69507957D1 - Integriertes verfahren zur herstellung von lactid - Google Patents
Integriertes verfahren zur herstellung von lactidInfo
- Publication number
- DE69507957D1 DE69507957D1 DE69507957T DE69507957T DE69507957D1 DE 69507957 D1 DE69507957 D1 DE 69507957D1 DE 69507957 T DE69507957 T DE 69507957T DE 69507957 T DE69507957 T DE 69507957T DE 69507957 D1 DE69507957 D1 DE 69507957D1
- Authority
- DE
- Germany
- Prior art keywords
- lactid
- producing
- integrated method
- integrated
- producing lactid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D319/10—1,4-Dioxanes; Hydrogenated 1,4-dioxanes
- C07D319/12—1,4-Dioxanes; Hydrogenated 1,4-dioxanes not condensed with other rings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/06—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from hydroxycarboxylic acids
- C08G63/08—Lactones or lactides
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Polyesters Or Polycarbonates (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/292,756 US5521278A (en) | 1994-08-18 | 1994-08-18 | Integrated process for the manufacture of lactide |
PCT/US1995/009643 WO1996006092A1 (en) | 1994-08-18 | 1995-08-14 | Integrated process for the manufacture of lactide |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69507957D1 true DE69507957D1 (de) | 1999-04-01 |
DE69507957T2 DE69507957T2 (de) | 1999-10-21 |
Family
ID=23126047
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69507957T Expired - Lifetime DE69507957T2 (de) | 1994-08-18 | 1995-08-14 | Integriertes verfahren zur herstellung von lactid |
Country Status (8)
Country | Link |
---|---|
US (1) | US5521278A (de) |
EP (1) | EP0777664B1 (de) |
JP (1) | JPH10504563A (de) |
AU (1) | AU3235395A (de) |
BR (1) | BR9508618A (de) |
CA (1) | CA2197644A1 (de) |
DE (1) | DE69507957T2 (de) |
WO (1) | WO1996006092A1 (de) |
Families Citing this family (49)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3301311B2 (ja) * | 1996-05-24 | 2002-07-15 | 株式会社神戸製鋼所 | 2−ヒドロキシカルボン酸オリゴマーの連続製造方法 |
US6475759B1 (en) | 1997-10-14 | 2002-11-05 | Cargill, Inc. | Low PH lactic acid fermentation |
US6229046B1 (en) * | 1997-10-14 | 2001-05-08 | Cargill, Incorported | Lactic acid processing methods arrangements and products |
JP4565208B2 (ja) * | 2000-03-31 | 2010-10-20 | 株式会社クレハ | グリコリドの精製方法 |
DE10020898B4 (de) * | 2000-04-20 | 2004-02-05 | Inventa-Fischer Gmbh | Verfahren zur Herstellung von Polymilchsäure und Vorrichtung hierzu |
US6984293B2 (en) * | 2001-03-15 | 2006-01-10 | Tate & Lyle Ingredients | Azeotropic distillation of cyclic esters of hydroxy organic acids |
BE1015060A3 (fr) * | 2002-08-06 | 2004-09-07 | Brussels Biotech Nv Sa | Procede de production de polylactide au depart d'une solution d'acide lactique ou d'un de ses derives. |
US8053584B2 (en) * | 2003-12-10 | 2011-11-08 | Tate & Lyle Public Limited Company | Purification process for lactide |
JP4565278B2 (ja) * | 2004-03-10 | 2010-10-20 | 株式会社日立プラントテクノロジー | ラクチド合成方法及びラクチド合成装置 |
CN100417651C (zh) * | 2005-06-22 | 2008-09-10 | 西北师范大学 | 催化乳酸合成丙交酯的方法 |
CN100417652C (zh) * | 2005-08-25 | 2008-09-10 | 西北师范大学 | 一种蒙脱土催化乳酸合成丙交酯的方法 |
JP4696824B2 (ja) * | 2005-10-07 | 2011-06-08 | 株式会社日立プラントテクノロジー | ポリエステルの製造方法及びポリエステルの製造装置 |
WO2008008068A1 (en) | 2006-07-14 | 2008-01-17 | Kimberly-Clark Worldwide, Inc. | Biodegradable aliphatic-aromatic copolyester for use in nonwoven webs |
US9091004B2 (en) * | 2006-07-14 | 2015-07-28 | Kimberly-Clark Worldwide, Inc. | Biodegradable polylactic acid for use in nonwoven webs |
EP2044251B1 (de) | 2006-07-14 | 2019-10-02 | NatureWorks LLC | Biologisch abbaubarer aliphatischer polyester zur verwendung in vliesstoffen |
US20100048082A1 (en) * | 2006-12-15 | 2010-02-25 | Topolkaraev Vasily A | Biodegradable polylactic acids for use in forming fibers |
US20100048081A1 (en) * | 2006-12-15 | 2010-02-25 | Topolkaraev Vasily A | Biodegradable polyesters for use in forming fibers |
WO2008119518A1 (en) * | 2007-03-30 | 2008-10-09 | Laccure Ab | Use of oligomers of lactic acid in the treatment of gynaecological disorders |
ATE506472T1 (de) * | 2007-08-22 | 2011-05-15 | Kimberly Clark Co | Mehrkomponentige biologisch abbaubare filamente und daraus gebildete vliesstoffe |
EP2031009A1 (de) | 2007-09-03 | 2009-03-04 | Uhde Inventa-Fischer GmbH | Reinigungsvorrichtung zur Abtrennung von Dilactid aus Stoffgemischen, Polymerisationsvorrichtung, Verfahren zur Abtrennung von Dilactid aus Stoffgemischen sowie Verwendung |
CN101896649B (zh) * | 2007-12-13 | 2012-07-18 | 金伯利-克拉克环球有限公司 | 由包含聚乳酸和聚醚共聚物的热塑性组合物形成的生物可降解纤维 |
JP5459974B2 (ja) * | 2008-04-11 | 2014-04-02 | 株式会社日立製作所 | 精製乳酸環状二量体の製造方法及び製造装置、並びに、ポリ乳酸の製造方法及び製造装置 |
KR101526636B1 (ko) * | 2008-05-30 | 2015-06-05 | 킴벌리-클라크 월드와이드, 인크. | 폴리락트산 섬유 |
AT507580B1 (de) * | 2008-11-19 | 2011-10-15 | Jungbunzlauer Austria Ag | Verfahren zur reinigung zyklischer diester der milchsäure |
JP5229268B2 (ja) * | 2010-05-10 | 2013-07-03 | 株式会社日立プラントテクノロジー | ポリ乳酸の合成装置及び方法 |
US8501875B2 (en) | 2010-10-28 | 2013-08-06 | Covidien Lp | Surface induced ring-opening polymerization and medical devices formed therefrom |
US8461262B2 (en) | 2010-12-07 | 2013-06-11 | Kimberly-Clark Worldwide, Inc. | Polylactic acid fibers |
BR112013018066B1 (pt) | 2011-02-18 | 2021-09-08 | Sulzer Management Ag | Método para preparar um ácido poliláctico |
US20120245322A1 (en) * | 2011-03-25 | 2012-09-27 | Hyundai Motor Company | Manufacturing lactide from lactic acid |
KR101326521B1 (ko) * | 2011-05-26 | 2013-11-07 | 현대자동차주식회사 | 유산으로부터 락타이드의 제조 방법 |
EP2853552B1 (de) | 2011-11-04 | 2017-12-06 | Uhde Inventa Fischer GmbH | Verfahren zur Herstellung einer polymerisationsfähigen Milchsäure |
KR101395357B1 (ko) | 2011-12-29 | 2014-05-15 | 주식회사 삼양사 | 폴리락트산-폴리실록산 공중합체 및 그 제조 방법 |
KR101376485B1 (ko) * | 2012-08-17 | 2014-04-01 | 한국화학연구원 | 다발관 강하막 반응기를 이용한 락타이드 제조 방법 |
EP2777791A1 (de) * | 2013-03-11 | 2014-09-17 | Sulzer Chemtech AG | Verfahren und Vorrichtung zum Reinigen eines Stromes mit einem zyklischen Ester einer Alpha-Hydroxycarboxylsäure |
US9573925B2 (en) | 2013-05-06 | 2017-02-21 | Futerro S.A. | Process for recovering and improving production of meso-lactide from a crude lactide containing stream |
WO2015112098A1 (en) * | 2014-01-23 | 2015-07-30 | Ptt Public Company Limited | Process for manufacturing lactide from plastics having polylactic acid |
KR102277898B1 (ko) | 2014-07-03 | 2021-07-15 | 삼성전자주식회사 | 산물 생산능이 향상된 효모 및 그를 이용한 산물을 생산하는 방법 |
KR20160046615A (ko) | 2014-10-21 | 2016-04-29 | 삼성전자주식회사 | 폴리우레탄 엘라스토머, 이를 포함하는 열가소성 수지 조성물, 열가소성 수지조성물로 이루어진 성형품 및 폴리우레탄 엘라스토머 제조방법 |
CN107531663B (zh) * | 2015-04-30 | 2022-02-08 | 荷兰普拉克公司 | 制造丙交酯的方法和装置 |
CN110382591A (zh) | 2017-05-31 | 2019-10-25 | Sk化学株式会社 | 聚酯树脂、其制备方法以及由其形成的树脂模制产品 |
CN110573551B (zh) | 2017-06-22 | 2022-02-15 | Sk化学株式会社 | 聚酯容器及其制造方法 |
KR20190001551A (ko) | 2017-06-26 | 2019-01-04 | 에스케이케미칼 주식회사 | 폴리에스테르 필름 및 이의 제조 방법 |
CN110204527B (zh) * | 2019-06-20 | 2021-12-17 | 南京大学 | 一种基于催化剂配制成浆料的丙交酯制备工艺 |
CN112851628A (zh) * | 2019-11-26 | 2021-05-28 | 南京华基塔业有限公司 | 一种由乳酸制备丙交酯的反应系统及方法 |
CN112898266B (zh) * | 2021-01-29 | 2021-11-19 | 安徽丰原生物技术股份有限公司 | 工业化制备l-丙交酯的装置及方法 |
CN113582964B (zh) * | 2021-08-23 | 2022-04-12 | 扬州惠通科技股份有限公司 | 一种丙交酯连续化生产系统及生产方法 |
CN116063271B (zh) * | 2021-10-31 | 2024-05-31 | 中国石油化工股份有限公司 | 一种高分子量乳酸低聚物制备丙交酯的方法 |
WO2023139207A1 (en) | 2022-01-21 | 2023-07-27 | Purac Biochem B.V. | Method for processing lactides |
CN116283889A (zh) * | 2023-03-29 | 2023-06-23 | 中国科学院长春应用化学研究所 | 一种乙交酯的制备方法和制备装置 |
Family Cites Families (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AT279547B (de) * | 1967-04-14 | 1970-03-10 | Buchs Metallwerk Ag | Verfahren und Vorrichtung zur Trennung oder Reinigung schmelzflüssiger, flüssiger oder gelöster Stoffe durch fraktioniertes Kristallisieren |
EP0261572A1 (de) * | 1986-09-20 | 1988-03-30 | Boehringer Ingelheim Kg | Verfahren zur Herstellung von Lactid |
ES2052551T3 (es) * | 1986-12-19 | 1994-07-16 | Akzo Nv | Metodo para preparar poli(acido lactico) o copolimeros de poli(acido lactico) por polimeracion de la lactida. |
US4835293A (en) * | 1987-02-24 | 1989-05-30 | E. I. Du Pont De Nemours And Company | Atmospheric pressure process for preparing pure cyclic esters |
US5223630A (en) * | 1989-10-10 | 1993-06-29 | E. I. Du Pont De Nemours And Company | Glycolide purification process |
US5023349A (en) * | 1990-05-08 | 1991-06-11 | E. I. Du Pont De Nemours And Company | Continuous process for rapid conversion of oligomers to cyclic esters |
US5091544A (en) * | 1990-05-08 | 1992-02-25 | E. I. Du Pont De Nemours And Company | Process for rapid conversion of oligomers to cyclic esters |
US5043458A (en) * | 1990-05-03 | 1991-08-27 | E. I. Du Pont De Nemours And Company | One-step continuous process for preparing cyclic esters |
US5023350A (en) * | 1990-05-24 | 1991-06-11 | E. I. Du Pont De Nemours And Company | Process for the purification of cyclic esters |
US5138074A (en) * | 1990-06-28 | 1992-08-11 | E. I. Du Pont De Nemours And Company | Continuous catalyzed vapor phase dimeric cyclic ester process |
EP0591188A1 (de) * | 1990-07-13 | 1994-04-13 | E.I. Du Pont De Nemours And Company | Rezyklierungsverfahren mit hoher lactid-ausbeute |
US5089632A (en) * | 1991-01-30 | 1992-02-18 | E. I. Du Pont De Nemours And Company | Process for preparing cyclic esters using a fluorocarbon |
US5326887A (en) * | 1991-02-27 | 1994-07-05 | E. I. Du Pont De Nemours And Company | Process for the preparation of 1,4-dioxane-2,5-diones |
US5196581A (en) * | 1991-05-01 | 1993-03-23 | Utah State University Foundation | Alkylcarbamoylborane cyclic dimers |
US5229528A (en) * | 1991-11-22 | 1993-07-20 | E. I. Du Pont De Nemours And Company | Rapid depolymerization of polyhydroxy acids |
US5264626A (en) * | 1991-11-22 | 1993-11-23 | E. I. Du Pont De Nemours And Company | Rapid depolymerization of polyhydroxy acids |
US5264614A (en) * | 1991-11-22 | 1993-11-23 | E. I. Du Pont De Nemours And Company | Recovery of polyhydroxy acids |
US5208297A (en) * | 1991-12-30 | 1993-05-04 | E. I. Du Pont De Nemours And Company | Rare earth metal coordination compounds as lactone polymerization catalysts |
US6326458B1 (en) * | 1992-01-24 | 2001-12-04 | Cargill, Inc. | Continuous process for the manufacture of lactide and lactide polymers |
US5247059A (en) * | 1992-01-24 | 1993-09-21 | Cargill, Incorporated | Continuous process for the manufacture of a purified lactide from esters of lactic acid |
US5258488A (en) * | 1992-01-24 | 1993-11-02 | Cargill, Incorporated | Continuous process for manufacture of lactide polymers with controlled optical purity |
US5142023A (en) * | 1992-01-24 | 1992-08-25 | Cargill, Incorporated | Continuous process for manufacture of lactide polymers with controlled optical purity |
ES2345307T3 (es) * | 1992-01-24 | 2010-09-20 | Cargill, Incorporated | Proceso continuo para la fabricacion de lactida y polimeros de lactida. |
US5247058A (en) * | 1992-01-24 | 1993-09-21 | Cargill, Incorporated | Continuous process for manufacture of lactide polymers with controlled optical purity |
US5288881A (en) * | 1992-03-12 | 1994-02-22 | E. I. Du Pont De Nemours And Company | Continuous reduced pressure dimeric cyclic ester production |
US5236560A (en) * | 1992-03-13 | 1993-08-17 | E. I. Du Pont De Nemours And Company | Solventless dimeric cyclic ester distillation process |
JPH0665230A (ja) * | 1992-08-19 | 1994-03-08 | Showa Denko Kk | ラクチドの製造方法 |
US5310599A (en) * | 1993-05-06 | 1994-05-10 | E. I. Du Pont De Nemours And Company | Method for making polymers of alpha-hydroxy acids |
-
1994
- 1994-08-18 US US08/292,756 patent/US5521278A/en not_active Expired - Lifetime
-
1995
- 1995-08-14 BR BR9508618A patent/BR9508618A/pt not_active Application Discontinuation
- 1995-08-14 DE DE69507957T patent/DE69507957T2/de not_active Expired - Lifetime
- 1995-08-14 CA CA002197644A patent/CA2197644A1/en not_active Abandoned
- 1995-08-14 AU AU32353/95A patent/AU3235395A/en not_active Abandoned
- 1995-08-14 WO PCT/US1995/009643 patent/WO1996006092A1/en active IP Right Grant
- 1995-08-14 JP JP8508081A patent/JPH10504563A/ja active Pending
- 1995-08-14 EP EP95928694A patent/EP0777664B1/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
WO1996006092A1 (en) | 1996-02-29 |
JPH10504563A (ja) | 1998-05-06 |
DE69507957T2 (de) | 1999-10-21 |
BR9508618A (pt) | 1997-09-30 |
AU3235395A (en) | 1996-03-14 |
CA2197644A1 (en) | 1996-02-29 |
EP0777664A1 (de) | 1997-06-11 |
EP0777664B1 (de) | 1999-02-24 |
US5521278A (en) | 1996-05-28 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition |