DE69329279T2 - Verfahren zur entfernung von fremdstoffen aus einem zuführungsstrom von verbrauchtem polyethylenterephthalat - Google Patents

Verfahren zur entfernung von fremdstoffen aus einem zuführungsstrom von verbrauchtem polyethylenterephthalat

Info

Publication number
DE69329279T2
DE69329279T2 DE1993629279 DE69329279T DE69329279T2 DE 69329279 T2 DE69329279 T2 DE 69329279T2 DE 1993629279 DE1993629279 DE 1993629279 DE 69329279 T DE69329279 T DE 69329279T DE 69329279 T2 DE69329279 T2 DE 69329279T2
Authority
DE
Germany
Prior art keywords
consumed
polyethylene terephthalate
removing foreign
foreign materials
supplying flow
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE1993629279
Other languages
English (en)
Other versions
DE69329279D1 (de
Inventor
John Burkett
Sue Jenks
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
M&G Polimeri Italia SpA.
Original Assignee
Shell Internationale Research Maatschappij BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Internationale Research Maatschappij BV filed Critical Shell Internationale Research Maatschappij BV
Application granted granted Critical
Publication of DE69329279D1 publication Critical patent/DE69329279D1/de
Publication of DE69329279T2 publication Critical patent/DE69329279T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/88—Post-polymerisation treatment
    • C08G63/90—Purification; Drying
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/04—Recovery or working-up of waste materials of polymers
    • C08J11/10—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
    • C08J11/18—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material
    • C08J11/22—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material by treatment with organic oxygen-containing compounds
    • C08J11/24—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material by treatment with organic oxygen-containing compounds containing hydroxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
    • B03B5/00—Washing granular, powdered or lumpy materials; Wet separating
    • B03B5/28—Washing granular, powdered or lumpy materials; Wet separating by sink-float separation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B13/00—Conditioning or physical treatment of the material to be shaped
    • B29B13/02—Conditioning or physical treatment of the material to be shaped by heating
    • B29B13/022—Melting the material to be shaped
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/02—Separating plastics from other materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/04—Recovery or working-up of waste materials of polymers
    • C08J11/10—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00168—Controlling or regulating processes controlling the viscosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00171—Controlling or regulating processes controlling the density
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/0077—Baffles attached to the reactor wall inclined
    • B01J2219/00772—Baffles attached to the reactor wall inclined in a helix
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/02—Separating plastics from other materials
    • B29B2017/0203—Separating plastics from plastics
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/02—Separating plastics from other materials
    • B29B2017/0213—Specific separating techniques
    • B29B2017/0217—Mechanical separating techniques; devices therefor
    • B29B2017/0237—Mechanical separating techniques; devices therefor using density difference
    • B29B2017/0244—Mechanical separating techniques; devices therefor using density difference in liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/02—Separating plastics from other materials
    • B29B2017/0213—Specific separating techniques
    • B29B2017/0255—Specific separating techniques using different melting or softening temperatures of the materials to be separated
    • B29B2017/0258—Specific separating techniques using different melting or softening temperatures of the materials to be separated using heated surfaces for selective softening or melting of at least one plastic ingredient
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2023/00—Use of polyalkenes or derivatives thereof as moulding material
    • B29K2023/04—Polymers of ethylene
    • B29K2023/06—PE, i.e. polyethylene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2067/00—Use of polyesters or derivatives thereof, as moulding material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/06—Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts
    • B29K2105/065—Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts containing impurities
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29L—INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
    • B29L2031/00—Other particular articles
    • B29L2031/712—Containers; Packaging elements or accessories, Packages
    • B29L2031/7158—Bottles
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
    • C08J2367/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/52—Mechanical processing of waste for the recovery of materials, e.g. crushing, shredding, separation or disassembly
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/62—Plastics recycling; Rubber recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Sustainable Development (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Thermal Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Polyethers (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
DE1993629279 1992-03-31 1993-03-24 Verfahren zur entfernung von fremdstoffen aus einem zuführungsstrom von verbrauchtem polyethylenterephthalat Expired - Fee Related DE69329279T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/860,963 US5223544A (en) 1992-03-31 1992-03-31 Process for the removal of foreign materials from a post-consumer plyethylene terephthalate feed stream
PCT/EP1993/000737 WO1993020125A2 (en) 1992-03-31 1993-03-24 Process for the removal of foreign materials from a post-consumer polyethylene terephthalate feed stream

Publications (2)

Publication Number Publication Date
DE69329279D1 DE69329279D1 (de) 2000-09-28
DE69329279T2 true DE69329279T2 (de) 2001-04-26

Family

ID=25334501

Family Applications (1)

Application Number Title Priority Date Filing Date
DE1993629279 Expired - Fee Related DE69329279T2 (de) 1992-03-31 1993-03-24 Verfahren zur entfernung von fremdstoffen aus einem zuführungsstrom von verbrauchtem polyethylenterephthalat

Country Status (11)

Country Link
US (1) US5223544A (de)
EP (1) EP0637326B1 (de)
JP (1) JP3459919B2 (de)
KR (1) KR100245206B1 (de)
AU (1) AU671109B2 (de)
BR (1) BR9306156A (de)
CA (1) CA2133214C (de)
DE (1) DE69329279T2 (de)
ES (1) ES2149810T3 (de)
TW (1) TW237463B (de)
WO (1) WO1993020125A2 (de)

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US5602187A (en) * 1992-05-18 1997-02-11 Swig Pty Ltd. Polyethylene terephthalate decontamination
US5504121A (en) * 1992-05-18 1996-04-02 Swig Pty Ltd. Polyethylene terephthalate decontamination
US5886057A (en) * 1993-07-05 1999-03-23 E. I. Du Pont De Nemours And Company Production of dicarboxylic acids
DE4410672C2 (de) * 1994-03-26 1996-04-04 Christian O Schoen Verfahren zur Wiederverwertung von Kunststoff
DE4417721A1 (de) * 1994-05-20 1995-11-23 Veba Oel Ag Vorrichtung zur Depolymerisation von Alt- und Abfallkunststoffen
DE4428355A1 (de) * 1994-05-20 1996-02-15 Veba Oel Ag Vorrichtung zur Depolymerisation von Alt- und Abfallkunststoffen
US5468780A (en) * 1994-06-21 1995-11-21 Miyaso Chemical Co. Method of recycling unsaturated polyester resin waste
US5559159A (en) * 1995-12-07 1996-09-24 Eastman Chemical Company Process including depolymerization in polyester reactor for recycling polyester materials
US6284808B1 (en) * 1997-02-03 2001-09-04 Illinois Tool Works Inc. Inline solid state polymerization of PET flakes for manufacturing plastic strap by removing non-crystalline materials from recycled PET
US5945460A (en) * 1997-03-20 1999-08-31 Eastman Chemical Company Process for continuously producing polyester articles with scrap recycle in a continuous melt-to-preform process
JP3715812B2 (ja) * 1998-12-10 2005-11-16 株式会社アイエス ポリエチレンテレフタレート廃棄物のケミカルリサイクル方法
US6410607B1 (en) * 1999-02-10 2002-06-25 Eastman Chemical Company Glycolysis process for recycling of post-consumer pet
WO2004029113A1 (ja) * 2002-09-27 2004-04-08 Meishin Kogyo Kabushikigaisha 減容化ゲル状ポリスチレン樹脂分離回収装置
US7666368B2 (en) * 2002-09-27 2010-02-23 Meishin Kogyo Kabushikigaisha Apparatus for treating volume-reduced polystyrene resin in gel state for material separation and recovery
US7297721B2 (en) * 2003-06-20 2007-11-20 Futura Polyesters Limited Process for controlled polymerization of a mixed polymer
ITTP20030002A1 (it) * 2003-10-09 2005-04-10 Giovanni Maurizio Di Processo ossidoriduzione per riciclare qualsiasi frazione rifiuto:fanghi, scarti industriali, agroalimentari, macellazione, ittici, ecc. in biostabilizzato sterile e/o polixano espanso isolante termoacustico, in innovativo impianto mobile o fisso con
JP2005131856A (ja) * 2003-10-29 2005-05-26 Teijin Fibers Ltd 脂肪族ポリエステルから異素材を除去する方法
JP2005132901A (ja) * 2003-10-29 2005-05-26 Teijin Fibers Ltd 脂肪族ポリエステルから異素材を除去する方法
WO2010137756A1 (en) * 2009-05-28 2010-12-02 Byung Kyoo Park Method and apparatus for recycling thermoplastic resin from a resin mixture
WO2012115984A2 (en) 2011-02-21 2012-08-30 Felice Kristopher M Polyurethane dispersions and methods of making and using same
US20120279023A1 (en) * 2011-05-06 2012-11-08 Avery Dennison Corporation Plastic Fastening Device Comprising a Recycled Thermoplastic Resin
KR101507696B1 (ko) 2011-06-10 2015-04-07 크리스토퍼 엠. 펠리체 투명 코팅, 아크릴 코팅
JP6244915B2 (ja) * 2012-08-29 2017-12-13 東洋紡株式会社 熱収縮性ポリエステル系フィルム
US9732026B2 (en) 2012-12-14 2017-08-15 Resinate Technologies, Inc. Reaction products containing hydroxyalkylterephthalates and methods of making and using same
KR102090218B1 (ko) * 2018-05-23 2020-03-17 주식회사 포스코 탕도
EP4041797A1 (de) 2019-10-08 2022-08-17 Eastman Chemical Company Katalysatorsysteme für kristallisierbare reaktionsharze mit recyceltem inhalt
MX2022004815A (es) 2019-10-25 2022-05-16 Eastman Chem Co Copoliesteres producidos a partir de copoliesteres reciclados.
NL2024181B1 (en) * 2019-11-07 2021-07-20 Ioniqa Tech B V Reactor system and method of separating a first contaminant from a feed stream
US12013191B2 (en) * 2020-10-20 2024-06-18 Katz Water Tech, Llc Coiled spring
CN113351140B (zh) * 2021-06-23 2022-10-18 山东佳星环保科技有限公司 高分散全混流反应釜

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US3701741A (en) * 1971-02-01 1972-10-31 Eastman Kodak Co Purification of impure scrap poly(ethylene terephthalate)
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US4542239A (en) * 1981-11-18 1985-09-17 Board Of Control Of Michigan Technological University Process for recovering terephthalic acid from waste polyethylene terephthalate
US4605762A (en) * 1982-04-23 1986-08-12 Celanese Mexicana S.A. Depolymerization of condensation polymers
US4439550A (en) * 1982-11-22 1984-03-27 Texaco Inc. Aromatic polyols made from recycled polyethylene terephthalate waste streams, alkylene glycol and dibasic acid waste streams
JPS60248646A (ja) * 1984-05-25 1985-12-09 Toray Ind Inc ポリエステル屑の解重合方法
US4746422A (en) * 1985-07-26 1988-05-24 Rutgers University Method for the separation of a mixture of plastic and contaminant
DE3843068A1 (de) * 1988-12-21 1990-06-28 Esselte Meto Int Gmbh Vorrichtung zum zufuehren eines etikettenbandes
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WO1992007025A1 (en) * 1990-10-22 1992-04-30 Mobil Oil Corporation Decontamination of polystyrene
US5120768A (en) * 1991-05-09 1992-06-09 The Goodyear Tire & Rubber Company Process for separating polyethylene terephthalate from polyvinyl chloride

Also Published As

Publication number Publication date
EP0637326A1 (de) 1995-02-08
JP3459919B2 (ja) 2003-10-27
JPH07505424A (ja) 1995-06-15
WO1993020125A2 (en) 1993-10-14
EP0637326B1 (de) 2000-08-23
KR950700954A (ko) 1995-02-20
TW237463B (de) 1995-01-01
CA2133214A1 (en) 1993-10-14
WO1993020125A3 (en) 1994-04-14
DE69329279D1 (de) 2000-09-28
CA2133214C (en) 2003-10-14
AU671109B2 (en) 1996-08-15
US5223544A (en) 1993-06-29
KR100245206B1 (ko) 2000-02-15
ES2149810T3 (es) 2000-11-16
BR9306156A (pt) 1998-06-23
AU3752493A (en) 1993-11-08

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