DE69318722D1 - Biologisch abbaubare zusammensetzungen, die stärke enthalten - Google Patents
Biologisch abbaubare zusammensetzungen, die stärke enthaltenInfo
- Publication number
- DE69318722D1 DE69318722D1 DE69318722T DE69318722T DE69318722D1 DE 69318722 D1 DE69318722 D1 DE 69318722D1 DE 69318722 T DE69318722 T DE 69318722T DE 69318722 T DE69318722 T DE 69318722T DE 69318722 D1 DE69318722 D1 DE 69318722D1
- Authority
- DE
- Germany
- Prior art keywords
- composition
- compositions containing
- biodegradable compositions
- converted starch
- alkenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
- C08J9/12—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a physical blowing agent
- C08J9/125—Water, e.g. hydrated salts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L29/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers
- C08L29/02—Homopolymers or copolymers of unsaturated alcohols
- C08L29/04—Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L3/00—Compositions of starch, amylose or amylopectin or of their derivatives or degradation products
- C08L3/02—Starch; Degradation products thereof, e.g. dextrin
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2303/00—Characterised by the use of starch, amylose or amylopectin or of their derivatives or degradation products
- C08J2303/02—Starch; Degradation products thereof, e.g. dextrin
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/06—Biodegradable
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US98086292A | 1992-11-24 | 1992-11-24 | |
US08/071,429 US5393804A (en) | 1992-11-24 | 1993-06-01 | Biodegradable compositions comprising starch and alkenol polymers |
PCT/US1993/011447 WO1994012567A1 (en) | 1992-11-24 | 1993-11-23 | Biodegradable compositions comprising starch |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69318722D1 true DE69318722D1 (de) | 1998-06-25 |
DE69318722T2 DE69318722T2 (de) | 1999-01-28 |
Family
ID=26752213
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69318722T Expired - Lifetime DE69318722T2 (de) | 1992-11-24 | 1993-11-23 | Biologisch abbaubare zusammensetzungen, die stärke enthalten |
Country Status (14)
Country | Link |
---|---|
US (1) | US5393804A (de) |
EP (1) | EP0670863B1 (de) |
JP (1) | JPH08503985A (de) |
KR (1) | KR100286794B1 (de) |
CN (1) | CN1040880C (de) |
AT (1) | ATE166372T1 (de) |
AU (1) | AU5678094A (de) |
CA (1) | CA2149139C (de) |
DE (1) | DE69318722T2 (de) |
DK (1) | DK0670863T3 (de) |
ES (1) | ES2119154T3 (de) |
GR (1) | GR3027639T3 (de) |
IL (1) | IL107590A0 (de) |
WO (1) | WO1994012567A1 (de) |
Families Citing this family (63)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6284359B1 (en) | 1991-11-25 | 2001-09-04 | National Starch And Chemical Company Investment Holding Corporation | Starch-based core products for use in rolled paper goods |
US5662731A (en) | 1992-08-11 | 1997-09-02 | E. Khashoggi Industries | Compositions for manufacturing fiber-reinforced, starch-bound articles having a foamed cellular matrix |
US5810961A (en) | 1993-11-19 | 1998-09-22 | E. Khashoggi Industries, Llc | Methods for manufacturing molded sheets having a high starch content |
US5709827A (en) | 1992-08-11 | 1998-01-20 | E. Khashoggi Industries | Methods for manufacturing articles having a starch-bound cellular matrix |
US5679145A (en) | 1992-08-11 | 1997-10-21 | E. Khashoggi Industries | Starch-based compositions having uniformly dispersed fibers used to manufacture high strength articles having a fiber-reinforced, starch-bound cellular matrix |
US5783126A (en) | 1992-08-11 | 1998-07-21 | E. Khashoggi Industries | Method for manufacturing articles having inorganically filled, starch-bound cellular matrix |
US5844023A (en) | 1992-11-06 | 1998-12-01 | Bio-Tec Biologische Naturverpackungen Gmbh | Biologically degradable polymer mixture |
US5716675A (en) | 1992-11-25 | 1998-02-10 | E. Khashoggi Industries | Methods for treating the surface of starch-based articles with glycerin |
US5362778A (en) * | 1993-02-16 | 1994-11-08 | Air Products And Chemicals, Inc. | Extrudable polyvinyl alcohol compositions containing modified starches |
DE4326118A1 (de) * | 1993-08-04 | 1995-02-09 | Buna Gmbh | Bioabbaubare, thermoplastisch verformbare Materialien aus Stärkeestern |
GB2281709B (en) * | 1993-09-14 | 1998-04-08 | Fujitsu Ltd | Biodegradable resin moulded article |
US5736209A (en) | 1993-11-19 | 1998-04-07 | E. Kashoggi, Industries, Llc | Compositions having a high ungelatinized starch content and sheets molded therefrom |
US6083586A (en) | 1993-11-19 | 2000-07-04 | E. Khashoggi Industries, Llc | Sheets having a starch-based binding matrix |
US5705203A (en) | 1994-02-07 | 1998-01-06 | E. Khashoggi Industries | Systems for molding articles which include a hinged starch-bound cellular matrix |
US5843544A (en) | 1994-02-07 | 1998-12-01 | E. Khashoggi Industries | Articles which include a hinged starch-bound cellular matrix |
US5776388A (en) | 1994-02-07 | 1998-07-07 | E. Khashoggi Industries, Llc | Methods for molding articles which include a hinged starch-bound cellular matrix |
PT819147E (pt) | 1995-04-07 | 2003-10-31 | Biotec Biolog Naturverpack | Mistura de polimeros biodegradaveis |
US6176915B1 (en) | 1995-04-14 | 2001-01-23 | Standard Starch, L.L.C. | Sorghum meal-based biodegradable formulations, shaped products made therefrom, and methods of making said shaped products |
US20010048176A1 (en) | 1995-04-14 | 2001-12-06 | Hans G. Franke | Resilient biodegradable packaging materials |
US6168857B1 (en) | 1996-04-09 | 2001-01-02 | E. Khashoggi Industries, Llc | Compositions and methods for manufacturing starch-based compositions |
DE19624641A1 (de) | 1996-06-20 | 1998-01-08 | Biotec Biolog Naturverpack | Biologisch abbaubarer Werkstoff, bestehend im wesentlichen aus oder auf Basis thermoplastischer Stärke |
US5922379A (en) * | 1998-05-05 | 1999-07-13 | Natural Polymer International Corporation | Biodegradable protein/starch-based thermoplastic composition |
US6107371A (en) * | 1998-06-16 | 2000-08-22 | National Starch And Chemical Investment Holding Corporation | Biodegradable expanded starch products and the method of preparation |
CN1218991C (zh) * | 1998-12-14 | 2005-09-14 | 普兰蒂克有限公司 | 可生物降解的聚合物以及由其制备聚合物产品的方法 |
US7326743B2 (en) * | 1998-12-14 | 2008-02-05 | Plantic Technologies Ltd. | Biodegradable polymer |
US6686405B1 (en) * | 1999-07-23 | 2004-02-03 | Kuraray Co., Ltd. | Process for producing ethylene-vinyl alcohol copolymer resin, process for producing pellets and resin pellets |
US7384993B2 (en) * | 1999-12-13 | 2008-06-10 | Plantic Technologies Ltd | Biodegradable polymer |
US6231970B1 (en) | 2000-01-11 | 2001-05-15 | E. Khashoggi Industries, Llc | Thermoplastic starch compositions incorporating a particulate filler component |
GB0001940D0 (en) * | 2000-01-27 | 2000-03-22 | Green Light Packaging Limited | Biodegradable packaging material |
KR20030020565A (ko) * | 2001-09-01 | 2003-03-10 | 드림라이프테크(주) | 생분해성 플라스틱 조성물, 그를 사용한 플라스틱 용기 및그의 제조방법 |
US20060175587A1 (en) * | 2003-03-05 | 2006-08-10 | Kasowski Maya M | Reaction product of a phosphorous acid with ethyleneamines for flame resistance |
GB0410388D0 (en) * | 2004-05-11 | 2004-06-16 | Adept Polymers Ltd | An extrusion process |
KR100559377B1 (ko) | 2004-05-28 | 2006-03-10 | 율촌화학 주식회사 | 생분해성 전분 용기용 조성물 및 이를 이용한 생분해성전분 용기 |
CN100381491C (zh) * | 2004-07-08 | 2008-04-16 | 胡靖� | 一种完全生物降解塑料餐饮具的发泡成型方法 |
KR100548949B1 (ko) * | 2004-07-09 | 2006-02-02 | 율촌화학 주식회사 | 생분해성 전분 용기 및 그 제조 방법 |
NZ554681A (en) * | 2004-10-05 | 2010-05-28 | Plantic Technologies Ltd | Mouldable biodegradable polymer |
JP2006206801A (ja) * | 2005-01-31 | 2006-08-10 | Toyo Ink Mfg Co Ltd | 微生物崩壊樹脂用着色樹脂組成物 |
CN100497458C (zh) * | 2005-02-06 | 2009-06-10 | 北京金宝帝生物环保科技有限公司 | 一种可生物降解的淀粉基高分子组合物、由其制得的薄膜,及其制备方法 |
AR055888A1 (es) * | 2005-03-24 | 2007-09-12 | Basf Ag | Tratamiento de textiles |
US7989524B2 (en) * | 2005-07-19 | 2011-08-02 | The United States Of America, As Represented By The Secretary Of Agriculture | Fiber-reinforced starch-based compositions and methods of manufacture and use |
US20070021515A1 (en) * | 2005-07-19 | 2007-01-25 | United States (as represented by the Secretary of Agriculture) | Expandable starch-based beads and method of manufacturing molded articles therefrom |
US20070082982A1 (en) * | 2005-10-11 | 2007-04-12 | The Procter & Gamble Company | Water stable compositions and articles comprising starch and methods of making the same |
CN104945683A (zh) * | 2006-04-18 | 2015-09-30 | 普朗蒂克科技有限公司 | 聚合物膜 |
CN101506291B (zh) | 2006-08-04 | 2013-12-04 | 普朗蒂克科技有限公司 | 成型性的生物降解性聚合物 |
US7713614B2 (en) * | 2006-09-19 | 2010-05-11 | Kuraray Co., Ltd. | Resin composition and multilayer structure |
ITMI20062374A1 (it) * | 2006-12-12 | 2008-06-13 | Novamont Spa | Materiale biodegradabile per stampaggio a iniezione ed articoli da esso ottenuti |
DE102007056433B4 (de) * | 2007-11-23 | 2009-08-20 | Siemens Ag | Kompressionsmulde für Mammographiegeräte, Verfahren zu ihrer Herstellung und Halterung für eine Kompressionsmulde |
US20090192245A1 (en) * | 2008-01-30 | 2009-07-30 | Satish Kumar Gaggar | Flame retardant resinous compositions and process |
US7939585B2 (en) * | 2008-01-30 | 2011-05-10 | Sabic Innovative Plastics Ip B.V. | Flame retardant resinous compositions and process |
CA2725222A1 (en) * | 2008-05-05 | 2009-11-12 | Wei Li | Thermoformed article made from bio-based biodegradable polymer composition |
US7915328B2 (en) * | 2008-12-30 | 2011-03-29 | Sabic Innovative Plastics Ip B.V. | Flame retardant resinous compositions and process |
US7915329B2 (en) * | 2008-12-30 | 2011-03-29 | Sabic Innovative Plastics Ip B.V. | Flame retardant resinous compositions and process |
CA2781963C (en) * | 2009-12-08 | 2014-01-07 | International Paper Company | Thermoformed articles made from reactive extrusion products of biobased materials |
US8889945B2 (en) * | 2010-12-08 | 2014-11-18 | Kimberly-Clark Worldwide, Inc. | Elastic film containing a renewable starch polymer |
CN102161797B (zh) * | 2011-05-31 | 2012-07-11 | 刘立文 | 一种改性线性低密度聚乙烯复合材料及其制备方法 |
CN102161796B (zh) * | 2011-06-01 | 2012-07-04 | 刘立文 | 一种改性高密度聚乙烯复合材料及其制备方法 |
US8875658B2 (en) | 2011-11-30 | 2014-11-04 | A.J. Boggs & Company | Projectile pet food |
CN103627037B (zh) * | 2013-11-07 | 2016-03-02 | 青岛文创科技有限公司 | 一种海草多酚-菊粉基复合薄膜及其制备方法 |
CN103627036B (zh) * | 2013-11-07 | 2016-06-01 | 青岛文创科技有限公司 | 一种海草多酚-菊粉基可降解复合薄膜及其制备方法 |
DE102016201498B4 (de) * | 2016-02-01 | 2017-08-17 | Norbert Kuhl | Sauerstoffdichter lebensmittelbehälter |
US10975213B2 (en) | 2018-08-13 | 2021-04-13 | Erthos Inc. | Composition and method of making biodegradable pellets |
CN113493591B (zh) * | 2020-03-19 | 2023-01-03 | 中国石油化工股份有限公司 | 聚乙烯醇母料及其制备方法 |
CN117580905A (zh) * | 2021-06-29 | 2024-02-20 | 株式会社可乐丽 | 淀粉组合物及成型体 |
Family Cites Families (36)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE501889C (de) * | 1926-05-23 | 1930-07-05 | Holzverkohlungs Ind Akt Ges | Loesungs- und Erweichungsmittel fuer Celluloseester und aehnliche Celluloseabkoemmlinge |
US2412213A (en) * | 1938-12-12 | 1946-12-10 | Groen Martinus Gerardus | Method of producing starch esters |
US2654736A (en) * | 1949-02-02 | 1953-10-06 | Nat Starch Products Inc | Stabilized starch derivatives |
US2660577A (en) * | 1950-05-27 | 1953-11-24 | Corn Prod Refining Co | Derivatization of starch witch lactones |
US3038895A (en) * | 1957-12-06 | 1962-06-12 | Nat Starch Chem Corp | Water-dispersible, partially substituted derivatives of amylose |
NL263573A (de) * | 1960-04-13 | 1900-01-01 | ||
US3184335A (en) * | 1960-12-29 | 1965-05-18 | American Mach & Foundry | Activation of amylose |
GB1077351A (en) * | 1963-09-21 | 1967-07-26 | Kurashiki Rayon Kk | Composition for films,sheets and other shaped articles of softened polyvinyl alcohol |
US4125495A (en) * | 1974-11-25 | 1978-11-14 | Coloroll Limited | Synthetic/resin based compositions |
US4061610A (en) * | 1976-05-19 | 1977-12-06 | The Sherwin-Williams Company | Coating compositions containing starch half-esters and process for preparing same |
US4207355A (en) * | 1979-01-08 | 1980-06-10 | National Starch And Chemical Corporation | Cold-water dispersible, gelling starches |
US4379138A (en) * | 1981-12-28 | 1983-04-05 | Research Triangle Institute | Biodegradable polymers of lactones |
US4738724A (en) * | 1983-11-04 | 1988-04-19 | Warner-Lambert Company | Method for forming pharmaceutical capsules from starch compositions |
US4673438A (en) * | 1984-02-13 | 1987-06-16 | Warner-Lambert Company | Polymer composition for injection molding |
US4726809A (en) * | 1986-05-19 | 1988-02-23 | American Maize-Products Company | Textile size |
US4726957A (en) * | 1987-02-26 | 1988-02-23 | National Starch And Chemical Corporation | Starch-based jelly gum confections |
CH671961A5 (de) * | 1987-02-27 | 1989-10-13 | Amrotex Ag | |
GB2206888B (en) * | 1987-07-07 | 1991-02-06 | Warner Lambert Co | A destructurized starch and a process for making same |
US5095054A (en) * | 1988-02-03 | 1992-03-10 | Warner-Lambert Company | Polymer compositions containing destructurized starch |
DE3939721C2 (de) * | 1988-12-05 | 2002-08-01 | Nippon Synthetic Chem Ind | Polyvinylalkohol-Stärke-Film |
BE1002635A6 (nl) * | 1988-12-09 | 1991-04-16 | Amylum Nv | Werkwijze voor het vervaardigen van een mengsel van zetmeel en polyvinylalcohol en aldus vervaardigd mengsel. |
DE3914022A1 (de) * | 1989-04-28 | 1990-10-31 | Aeterna Lichte Gmbh & Co Kg | Biologisch abbaubare kunststoffmaterialien |
PL285925A1 (en) * | 1989-07-11 | 1991-03-11 | Warner Lambert Co | Polymer mixture, method for manufacturing a thermoplastic product and a method for manufacturing a thermoplastic alloy |
NZ234921A (en) * | 1989-09-01 | 1993-02-25 | Air Prod & Chem | Polyvinyl alcohol pellet prepared by melt extrusion |
US5051222A (en) * | 1989-09-01 | 1991-09-24 | Air Products And Chemicals, Inc. | Method for making extrudable polyvinyl alcohol compositions |
US5137969A (en) * | 1989-09-01 | 1992-08-11 | Air Products And Chemicals, Inc. | Melt extrudable polyvinyl alcohol pellets having reduced maximum melt temperature and reduced gel content |
JP2905542B2 (ja) * | 1990-03-12 | 1999-06-14 | 株式会社クラレ | 農業用マルチフィルム |
IT1240503B (it) * | 1990-07-25 | 1993-12-17 | Butterfly Srl | Miscela polimerica amidacea particolarmente per la produzione di film e simili e procedimento per la sua produzione. |
EP0474173B1 (de) * | 1990-09-04 | 1996-04-10 | Nippon Gohsei Kagaku Kogyo Kabushiki Kaisha | Biologisch abbaubare, schmelzgeformte Gegenstände, Laminate daraus und ihre Verwendung |
JP3059200B2 (ja) * | 1990-09-27 | 2000-07-04 | 株式会社クラレ | 易崩壊性樹脂組成物 |
US5087650A (en) * | 1990-12-05 | 1992-02-11 | Fully Compounded Plastics, Inc. | Biodegradable plastics |
AU656586B2 (en) * | 1991-03-19 | 1995-02-09 | Parke, Davis & Company | Biodegradable compositions comprising starch derivatives |
WO1992018325A1 (en) * | 1991-04-12 | 1992-10-29 | Enviropack, Inc. | Biodegradable packaging material |
RU2095379C1 (ru) * | 1991-05-03 | 1997-11-10 | НОВАМОНТ С.п.А. | Полимерная композиция для получения биодеградируемых формованных изделий и биодеградируемые формованные изделия |
EP0539604B1 (de) * | 1991-05-15 | 1997-07-16 | Nippon Gohsei Kagaku Kogyo Kabushiki Kaisha | Verbundstoff hergestellt aus einer biologisch abbaubaren harzzusammensetzung |
US5205863A (en) * | 1991-11-14 | 1993-04-27 | International Communications & Energy | Agricultural biodegradable plastics |
-
1993
- 1993-06-01 US US08/071,429 patent/US5393804A/en not_active Expired - Lifetime
- 1993-11-12 IL IL10759093A patent/IL107590A0/xx unknown
- 1993-11-23 KR KR1019950702073A patent/KR100286794B1/ko not_active IP Right Cessation
- 1993-11-23 CA CA002149139A patent/CA2149139C/en not_active Expired - Fee Related
- 1993-11-23 WO PCT/US1993/011447 patent/WO1994012567A1/en active IP Right Grant
- 1993-11-23 AT AT94902392T patent/ATE166372T1/de not_active IP Right Cessation
- 1993-11-23 JP JP6513371A patent/JPH08503985A/ja active Pending
- 1993-11-23 AU AU56780/94A patent/AU5678094A/en not_active Abandoned
- 1993-11-23 ES ES94902392T patent/ES2119154T3/es not_active Expired - Lifetime
- 1993-11-23 DE DE69318722T patent/DE69318722T2/de not_active Expired - Lifetime
- 1993-11-23 EP EP94902392A patent/EP0670863B1/de not_active Expired - Lifetime
- 1993-11-23 DK DK94902392T patent/DK0670863T3/da active
- 1993-11-24 CN CN93120685A patent/CN1040880C/zh not_active Expired - Fee Related
-
1998
- 1998-08-12 GR GR980401817T patent/GR3027639T3/el unknown
Also Published As
Publication number | Publication date |
---|---|
CN1040880C (zh) | 1998-11-25 |
JPH08503985A (ja) | 1996-04-30 |
ES2119154T3 (es) | 1998-10-01 |
IL107590A0 (en) | 1994-02-27 |
CN1089279A (zh) | 1994-07-13 |
AU5678094A (en) | 1994-06-22 |
EP0670863B1 (de) | 1998-05-20 |
DE69318722T2 (de) | 1999-01-28 |
DK0670863T3 (da) | 1999-03-08 |
GR3027639T3 (en) | 1998-11-30 |
KR960700302A (ko) | 1996-01-19 |
WO1994012567A1 (en) | 1994-06-09 |
ATE166372T1 (de) | 1998-06-15 |
CA2149139A1 (en) | 1994-06-09 |
CA2149139C (en) | 2005-12-27 |
US5393804A (en) | 1995-02-28 |
KR100286794B1 (ko) | 2001-04-16 |
EP0670863A1 (de) | 1995-09-13 |
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