DE69233679D1 - Verfahren zur Trennung von optischen Isomeren in einem simulierten Wanderbettsystem - Google Patents
Verfahren zur Trennung von optischen Isomeren in einem simulierten WanderbettsystemInfo
- Publication number
- DE69233679D1 DE69233679D1 DE69233679T DE69233679T DE69233679D1 DE 69233679 D1 DE69233679 D1 DE 69233679D1 DE 69233679 T DE69233679 T DE 69233679T DE 69233679 T DE69233679 T DE 69233679T DE 69233679 D1 DE69233679 D1 DE 69233679D1
- Authority
- DE
- Germany
- Prior art keywords
- separation
- optical isomers
- moving bed
- bed system
- simulated moving
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1814—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns recycling of the fraction to be distributed
- B01D15/1821—Simulated moving beds
- B01D15/185—Simulated moving beds characterized by the components to be separated
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/38—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving specific interaction not covered by one or more of groups B01D15/265 - B01D15/36
- B01D15/3833—Chiral chromatography
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B57/00—Separation of optically-active compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP21056591 | 1991-08-22 | ||
JP3210565A JP3010816B2 (ja) | 1991-08-22 | 1991-08-22 | 光学分割における光学異性体と溶媒との回収方法、溶媒の循環使用方法、および光学異性体の再利用方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69233679D1 true DE69233679D1 (de) | 2007-03-29 |
DE69233679T2 DE69233679T2 (de) | 2007-06-14 |
Family
ID=16591429
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69233679T Expired - Lifetime DE69233679T2 (de) | 1991-08-22 | 1992-08-10 | Verfahren zur Trennung von optischen Isomeren in einem simulierten Wanderbettsystem |
DE69223037T Expired - Lifetime DE69223037T3 (de) | 1991-08-22 | 1992-08-10 | Wiedergewinnung von optischen isomeren und lösungsmittel bei einer optischen auflösung, wiederbenutzung des lösungsmittels und optischen isomers nach recycling |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69223037T Expired - Lifetime DE69223037T3 (de) | 1991-08-22 | 1992-08-10 | Wiedergewinnung von optischen isomeren und lösungsmittel bei einer optischen auflösung, wiederbenutzung des lösungsmittels und optischen isomers nach recycling |
Country Status (6)
Country | Link |
---|---|
US (2) | US5434298A (de) |
EP (2) | EP0563388B2 (de) |
JP (1) | JP3010816B2 (de) |
KR (1) | KR960009561B1 (de) |
DE (2) | DE69233679T2 (de) |
WO (1) | WO1993004022A1 (de) |
Families Citing this family (39)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5770088A (en) * | 1992-06-30 | 1998-06-23 | Daicel Chemical Industries, Ltd. | Simulated moving bed chromatographic separation process |
WO1995023125A1 (fr) * | 1994-02-25 | 1995-08-31 | Daicel Chemical Industries, Ltd. | Procede de production de compose de mevalonolactone optiquement actif |
JPH07285889A (ja) * | 1994-04-20 | 1995-10-31 | Daicel Chem Ind Ltd | 光学異性体の分離方法 |
JPH08176133A (ja) * | 1994-12-26 | 1996-07-09 | Takeda Chem Ind Ltd | L−アスコルビン酸の精製法 |
US5518625A (en) * | 1995-02-13 | 1996-05-21 | Uop | Chiral separations by simulated moving bed chromatography operating at low k' values |
US5626762A (en) * | 1995-02-13 | 1997-05-06 | Uop | Separations by simulated moving bed chromatography operating at low K' values using weakly interating adsorbents as the stationary phase |
US5645729A (en) * | 1995-02-13 | 1997-07-08 | Uop | Separations by simulated moving bed chromatography operating at low k' values using weakly interacting adsorbents as the stationary phase |
IL115941A (en) * | 1995-11-09 | 1998-10-30 | Weizmann Kiryat Membrane Prod | Multi-stage membrane system and process |
FR2754731B1 (fr) * | 1996-10-18 | 1999-07-02 | Novasep Sa | Perfectionnement aux procedes d'enrichissement d'isomeres optiques par lit mobile simule |
JPH1190106A (ja) * | 1997-09-26 | 1999-04-06 | Daicel Chem Ind Ltd | 擬似移動床式クロマト分離装置 |
EP1070076A4 (de) * | 1998-03-16 | 2002-05-29 | Chiral Technologies Inc | Chirale trennung von pyrimidinen |
DE69913332T2 (de) | 1998-05-01 | 2004-05-27 | Pfizer Products Inc., Groton | Verfahren zur herstellung von enantiomeren reinem oder optisch angereicherter sertraline-tetralon durch kontinuierliche chromatographie |
US6107492A (en) * | 1998-05-08 | 2000-08-22 | Ucb, S.A. | Process for the preparation of levetiracetam |
JP3453516B2 (ja) * | 1998-05-29 | 2003-10-06 | オルガノ株式会社 | クロマト分離方法 |
DE19858892A1 (de) * | 1998-12-19 | 2000-06-21 | Merck Patent Gmbh | Kontinuierliches Verfahren zur Trennung von Stoffen nach Molekülgröße |
DE19962543A1 (de) * | 1999-12-23 | 2001-07-05 | Degussa | Chromatographische Enantiomerentrennung von bicyclischen Lactamen |
JP4651264B2 (ja) | 2000-07-21 | 2011-03-16 | ギリアード サイエンシーズ, インコーポレイテッド | ホスホネートヌクレオチドアナログのプロドラッグならびにこれを選択および作製するための方法。 |
EP1331214A4 (de) | 2000-10-13 | 2006-08-02 | Daicel Chem | Packungsmaterial zur trennung optischer isomere und verfahren zur trennung optischer isomere unter anwendung dieses materials |
JP4873207B2 (ja) * | 2001-02-26 | 2012-02-08 | 東レ・ファインケミカル株式会社 | 光学活性カルボン酸クロリドの精製方法 |
US6977301B1 (en) | 2001-05-29 | 2005-12-20 | Ucb, S.A. | Process for preparing (S) and (R)—2-[4-(4-chlorobenzhydryl)piperazin-1-yl]-ethoxyacetamide |
US7199241B1 (en) | 2001-05-29 | 2007-04-03 | Ucb, S.A. | Process for preparing (S) and (R)-2-[4-(4-chlorobenzhydryl)piperazin-1-yl]-ethoxyacetamide |
AR034759A1 (es) * | 2001-07-13 | 2004-03-17 | Lundbeck & Co As H | Metodo para la preparacion de escitalopram |
FR2836396B1 (fr) * | 2002-02-22 | 2004-06-18 | Novasep | Procede et dispositif de chromatographie avec recuperation de solvant |
JP2004003935A (ja) * | 2002-04-12 | 2004-01-08 | Daicel Chem Ind Ltd | 擬似移動床式クロマトグラフィー用光学異性体分離用充填剤 |
FR2846252B1 (fr) * | 2002-10-29 | 2005-07-01 | Novasep | Procede et dispositif de chromatographie integrant une etape de concentration |
US20060128955A1 (en) * | 2003-05-09 | 2006-06-15 | Vela Pharmaceuticals, Inc. | Method of isolating (R)-tofisopam |
GB0325055D0 (en) * | 2003-10-27 | 2003-12-03 | Smithkline Beecham Corp | New process |
DE102004025000A1 (de) | 2004-05-21 | 2005-12-08 | Bayer Technology Services Gmbh | Verfahren zur Herstellung von chemischen und pharmazeutischen Produkten mit integrierter Mehrsäulen-Chromatographie |
EP1773793A2 (de) * | 2004-07-03 | 2007-04-18 | Merck Generics (UK) Limited | Verfahren zur herstellung von pramipexol durch chirale chromatographie |
EP1828198B1 (de) * | 2004-12-20 | 2011-02-09 | SK Holdings Co., Ltd. | Verfahren zur trennung von optisch reinen thiophenverbindungen unter anwendung von simulierter bewegtbettchromatographie |
FR2889077B1 (fr) * | 2005-07-26 | 2007-10-12 | Novasep Soc Par Actions Simpli | Procede et dispositif de separation chromatographique de fractions d'un melange |
JP2007085829A (ja) * | 2005-09-21 | 2007-04-05 | Daicel Chem Ind Ltd | 近赤外分光分析装置を校正するための装置及び方法 |
HU226863B1 (en) * | 2005-12-09 | 2009-12-28 | Chinoin Gyogyszer Es Vegyeszet | Process for separation of optical isomers of "corey-lactone" by liquid chromatography |
KR100741752B1 (ko) * | 2005-12-26 | 2007-07-23 | 삼성토탈 주식회사 | 단일 흡착 챔버를 사용하여 공급물을 전처리하는 유사 이동층 흡착 분리 방법 및 그에 사용되는 장치 |
US20080314835A1 (en) * | 2007-01-16 | 2008-12-25 | Regina Valluzzi | Chiral separating agents with active support |
US7618539B2 (en) | 2008-03-31 | 2009-11-17 | Ampac Fine Chemicals Llc | Simulated moving bed chromatography for strongly retained compounds |
WO2013156630A1 (en) | 2012-04-20 | 2013-10-24 | Alphaptose Gmbh | S-enantiomer of a tri-substituted glycerol compound |
EP2801604B1 (de) | 2013-05-07 | 2017-04-12 | Groupe Novasep | Chromatographisches Verfahren zur Herstellung von hochreinen, mehrfach ungesättigten Fettsäuren |
CN104387237B (zh) * | 2014-01-22 | 2016-01-27 | 江苏汉邦科技有限公司 | 模拟移动床色谱拆分4-氯二苯甲醇对映体的方法 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2985589A (en) * | 1957-05-22 | 1961-05-23 | Universal Oil Prod Co | Continuous sorption process employing fixed bed of sorbent and moving inlets and outlets |
JPS5820283B2 (ja) * | 1976-12-18 | 1983-04-22 | 田辺製薬株式会社 | ラセミ有機化合物の連続的光学分割方法 |
GB8429121D0 (en) * | 1984-11-17 | 1984-12-27 | Laporte Industries Ltd | Zeolites |
FR2593409B1 (fr) * | 1986-01-30 | 1990-08-24 | Centre Nat Rech Scient | Procede de separation des constituants d'un melange comprenant au moins deux composes connus pour etre difficiles a separer et faisant appel au phenomene d'adsorption |
JPS62210053A (ja) * | 1986-03-07 | 1987-09-16 | Agency Of Ind Science & Technol | 光学異性体分離用充填剤 |
JP2925753B2 (ja) * | 1990-02-23 | 1999-07-28 | ダイセル化学工業株式会社 | 光学異性体の分離方法 |
US5220053A (en) * | 1992-01-24 | 1993-06-15 | Ethyl Corporation | Preparation of optically active aliphatic carboxylic acids |
-
1991
- 1991-08-22 JP JP3210565A patent/JP3010816B2/ja not_active Expired - Lifetime
-
1992
- 1992-08-10 EP EP92916823A patent/EP0563388B2/de not_active Expired - Lifetime
- 1992-08-10 US US08/030,063 patent/US5434298A/en not_active Expired - Lifetime
- 1992-08-10 DE DE69233679T patent/DE69233679T2/de not_active Expired - Lifetime
- 1992-08-10 DE DE69223037T patent/DE69223037T3/de not_active Expired - Lifetime
- 1992-08-10 WO PCT/JP1992/001024 patent/WO1993004022A1/ja active IP Right Grant
- 1992-08-10 EP EP96101608A patent/EP0719749B1/de not_active Expired - Lifetime
-
1993
- 1993-04-15 KR KR93701126A patent/KR960009561B1/ko not_active IP Right Cessation
- 1993-11-22 US US08/156,264 patent/US5434299A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
US5434299A (en) | 1995-07-18 |
DE69223037D1 (de) | 1997-12-11 |
DE69223037T2 (de) | 1998-02-26 |
EP0719749B1 (de) | 2007-02-14 |
EP0563388B1 (de) | 1997-11-05 |
EP0563388B2 (de) | 2001-04-04 |
EP0563388A1 (de) | 1993-10-06 |
EP0563388A4 (en) | 1994-07-06 |
JP3010816B2 (ja) | 2000-02-21 |
DE69223037T3 (de) | 2001-08-02 |
DE69233679T2 (de) | 2007-06-14 |
JPH06239767A (ja) | 1994-08-30 |
EP0719749A3 (de) | 1996-07-17 |
KR930702252A (ko) | 1993-09-08 |
US5434298A (en) | 1995-07-18 |
EP0719749A2 (de) | 1996-07-03 |
KR960009561B1 (en) | 1996-07-20 |
WO1993004022A1 (en) | 1993-03-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
R071 | Expiry of right |
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