DE69227733D1 - Verfahren für die chromatographie - Google Patents
Verfahren für die chromatographieInfo
- Publication number
- DE69227733D1 DE69227733D1 DE69227733T DE69227733T DE69227733D1 DE 69227733 D1 DE69227733 D1 DE 69227733D1 DE 69227733 T DE69227733 T DE 69227733T DE 69227733 T DE69227733 T DE 69227733T DE 69227733 D1 DE69227733 D1 DE 69227733D1
- Authority
- DE
- Germany
- Prior art keywords
- chromatography
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004587 chromatography analysis Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/2226—Sampling from a closed space, e.g. food package, head space
- G01N2001/2229—Headspace sampling, i.e. vapour over liquid
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
- G01N2030/121—Preparation by evaporation cooling; cold traps
- G01N2030/122—Preparation by evaporation cooling; cold traps cryogenic focusing
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
- G01N2030/121—Preparation by evaporation cooling; cold traps
- G01N2030/123—Preparation by evaporation cooling; cold traps using more than one trap
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
- G01N2030/303—Control of physical parameters of the fluid carrier of temperature using peltier elements
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
- G01N2030/3076—Control of physical parameters of the fluid carrier of temperature using specially adapted T(t) profile
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/50—Conditioning of the sorbent material or stationary liquid
- G01N30/56—Packing methods or coating methods
- G01N2030/567—Packing methods or coating methods coating
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N2030/621—Detectors specially adapted therefor signal-to-noise ratio
- G01N2030/623—Detectors specially adapted therefor signal-to-noise ratio by modulation of sample feed or detector response
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
- G01N30/463—Flow patterns using more than one column with serial coupling of separation columns for multidimensional chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/60—Construction of the column
- G01N30/6047—Construction of the column with supporting means; Holders
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/86—Signal analysis
- G01N30/8658—Optimising operation parameters
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/647,790 US5135549A (en) | 1991-01-30 | 1991-01-30 | Chromatographic technique and apparatus |
PCT/US1992/000747 WO1992013622A1 (en) | 1991-01-30 | 1992-01-30 | Chromatographic technique and apparatus |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69227733D1 true DE69227733D1 (de) | 1999-01-14 |
DE69227733T2 DE69227733T2 (de) | 1999-07-22 |
Family
ID=24598280
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69227733T Expired - Lifetime DE69227733T2 (de) | 1991-01-30 | 1992-01-30 | Verfahren für die chromatographie |
Country Status (5)
Country | Link |
---|---|
US (1) | US5135549A (de) |
EP (1) | EP0522150B1 (de) |
JP (1) | JP3320065B2 (de) |
DE (1) | DE69227733T2 (de) |
WO (1) | WO1992013622A1 (de) |
Families Citing this family (108)
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US5305232A (en) * | 1992-05-13 | 1994-04-19 | The University Of Rochester | Chromatography system |
CA2110343C (en) * | 1992-12-14 | 1999-08-24 | Christopher Huk-Shi Cheh | Gas chromatographic method |
US5492555A (en) * | 1994-06-09 | 1996-02-20 | Lovelace Biomedical & Environmental Research Institute, Inc. | Automated two-dimensional interface for capillary gas chromatography |
AU2781995A (en) * | 1994-06-24 | 1996-01-19 | Universite De Montreal | Selective removal of volatile substances injected into a chromatographic packing filled column |
US5508204A (en) * | 1995-01-12 | 1996-04-16 | Norman Clinical Laboratories, Inc. | Multiple sample sequential chemical analysis |
IT1275526B (it) * | 1995-07-14 | 1997-08-07 | Fisons Instr Spa | Procedimento e dispositivo per l'iniezione di volumi elevati di campioni liquidi in un gascromatografo |
WO1997013570A1 (en) * | 1995-10-13 | 1997-04-17 | Ledford Edward B Jr | Apparatus and method for chemical modulation |
DE69637079T2 (de) * | 1995-10-16 | 2008-01-24 | Thermo Orion Inc., Beverly | Hochgeschwindigkeitschromatographie |
US6131440A (en) | 1996-10-15 | 2000-10-17 | Universite De Montreal | Selective removal of volatile substances injected into a chromatographic packing filled column |
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WO1999040422A1 (en) * | 1998-02-10 | 1999-08-12 | Haley Lawrence V | A valveless gas chromatographic system with pulsed injection and temperature programmed elution |
AU2668099A (en) | 1998-02-11 | 1999-08-30 | Lawrence V. Haley | Hand-held detection system using gc/ims |
US6866786B2 (en) * | 1998-04-03 | 2005-03-15 | Symyx Technologies, Inc. | Rapid characterization of polymers |
US6209386B1 (en) | 1998-06-05 | 2001-04-03 | Rvm Scientific, Inc. | Electrically insulated gas chromatograph assembly and method of fabricating same |
US6855258B2 (en) * | 1999-04-02 | 2005-02-15 | Symyx Technologies, Inc. | Methods for characterization of polymers using multi-dimensional liquid chromatography with parallel second-dimension sampling |
IT1313967B1 (it) * | 1999-12-27 | 2002-09-26 | Thermoquest Italia Spa | Sistema e metodo per controllare la temperatura di una colonna percromatografia. |
AU2001229406A1 (en) | 2000-01-12 | 2001-07-24 | Zoex Corporation | Transverse thermal modulation |
US6423120B1 (en) | 2000-07-17 | 2002-07-23 | Agilent Technologies, Inc. | Sample introduction systems and methods |
ATE317120T1 (de) * | 2000-12-19 | 2006-02-15 | Thermo Electron Spa | Modulator für die gaschromatographie |
US6632268B2 (en) * | 2001-02-08 | 2003-10-14 | Oakland University | Method and apparatus for comprehensive two-dimensional gas chromatography |
US6989129B2 (en) * | 2001-04-05 | 2006-01-24 | The President And Fellows Of Harvard College | Automated capillary liquid chromatography small volume analysis system |
EP1275958A1 (de) * | 2001-07-05 | 2003-01-15 | Agilent Technologies, Inc. (a Delaware corporation) | Verfahren zur Verringerung von Nulllinieninstabilitäten in flüssigchromatographischen Messungen und Flüssigchromatographievorrichtung |
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US7104112B2 (en) * | 2002-09-27 | 2006-09-12 | Honeywell International Inc. | Phased micro analyzer IV |
JP2006515667A (ja) * | 2002-09-27 | 2006-06-01 | ハネウェル・インターナショナル・インコーポレーテッド | 位相マイクロ型分析器 |
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CA2554997A1 (en) | 2004-02-02 | 2005-08-18 | Sionex Corporation | Compact sample analysis systems and related methods using combined chromatography and mobility spectrometry techniques |
WO2005079944A1 (en) * | 2004-02-17 | 2005-09-01 | California Institute Of Technology | On-chip temperature controlled liquid chromatography methods and devices |
US7284409B2 (en) * | 2004-05-05 | 2007-10-23 | The Regents Of The University Of Michigan | Thermal modulation for gas chromatography |
EP1721153A2 (de) | 2004-03-05 | 2006-11-15 | The Regents Of The University Of Michigan | Thermische modulation für die gaschromatographie |
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EP3046650B1 (de) * | 2013-09-16 | 2019-11-13 | Brigham Young University | Gaschromatografie mit einem monotonen nicht ansteigenden thermischen gradienten und positiver zweiter ableitung |
CN105814274A (zh) | 2013-12-16 | 2016-07-27 | 陶氏环球技术有限责任公司 | 油回收生产流体中化学添加剂的痕量的分析方法 |
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ES2951785T3 (es) | 2016-10-04 | 2023-10-24 | Univ Michigan Regents | Cromatografía de gases completa multidimensional multicanal |
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JP7072134B2 (ja) | 2017-10-25 | 2022-05-20 | エンテック インスツルメンツ インコーポレイテッド | ガスクロマトグラフィで使用するための試料予備濃縮システム及び方法 |
US11162925B2 (en) | 2017-11-03 | 2021-11-02 | Entech Instruments Inc. | High performance sub-ambient temperature multi-capillary column preconcentration system for volatile chemical analysis by gas chromatography |
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JP6840420B2 (ja) * | 2019-02-04 | 2021-03-10 | Nissha株式会社 | ガスクロマトグラフ装置 |
JP7379862B2 (ja) * | 2019-05-09 | 2023-11-15 | 株式会社島津製作所 | 短鎖塩素化パラフィンの同族体の検出方法 |
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CN111855790A (zh) * | 2020-08-20 | 2020-10-30 | 中国科学院生态环境研究中心 | 一种识别复杂环境样品中特定芳烃类化合物的方法 |
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US3225520A (en) * | 1962-06-04 | 1965-12-28 | Gulf Research Development Co | Sample preparation and collection means for gas chromatographic columns |
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US3449938A (en) * | 1967-08-03 | 1969-06-17 | Univ Utah | Method for separating and detecting fluid materials |
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FR2227890B1 (de) * | 1973-05-04 | 1975-12-26 | Erap | |
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GB1482611A (en) * | 1974-04-08 | 1977-08-10 | Lovelock J | Selective detection of a component in an atmosphere |
FR2317654A1 (fr) * | 1975-07-09 | 1977-02-04 | Intersmat Sa | Chromatographe modulaire, notamment pour chromatographie en phase gazeuse |
DE2823445A1 (de) * | 1978-05-29 | 1979-12-06 | Inst Chromatographie | System zur elektronischen oder elektromechanischen polaritaetsoptimierung in der gas-chromatographie |
IT1134198B (it) * | 1980-11-06 | 1986-07-31 | Erba Strumentazione | Dispositivo per l'iniezione a vaporizzazione in una colonna gas-cromatografica |
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US5028243A (en) * | 1988-12-22 | 1991-07-02 | University Of Dayton | Gas chromatography methods and apparatus |
US4923486A (en) * | 1988-12-22 | 1990-05-08 | University Of Dayton | Gas chromatography methods and apparatus |
EP0459677A3 (en) * | 1990-05-29 | 1993-02-03 | Thermedics, Inc. | Selective, high speed detection of vapors with analysis of multiple gc-separated portions |
-
1991
- 1991-01-30 US US07/647,790 patent/US5135549A/en not_active Expired - Lifetime
-
1992
- 1992-01-30 EP EP92906061A patent/EP0522150B1/de not_active Expired - Lifetime
- 1992-01-30 WO PCT/US1992/000747 patent/WO1992013622A1/en active IP Right Grant
- 1992-01-30 JP JP50628192A patent/JP3320065B2/ja not_active Expired - Lifetime
- 1992-01-30 DE DE69227733T patent/DE69227733T2/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
JPH05506315A (ja) | 1993-09-16 |
WO1992013622A1 (en) | 1992-08-20 |
DE69227733T2 (de) | 1999-07-22 |
JP3320065B2 (ja) | 2002-09-03 |
EP0522150A4 (en) | 1993-11-03 |
US5135549A (en) | 1992-08-04 |
EP0522150B1 (de) | 1998-12-02 |
EP0522150A1 (de) | 1993-01-13 |
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