DE60203307D1 - Wässrige emulsionspolymerisation in gegenwart von ethern als kettenübertragungsmitteln zur herstellung von fluorpolymeren - Google Patents
Wässrige emulsionspolymerisation in gegenwart von ethern als kettenübertragungsmitteln zur herstellung von fluorpolymerenInfo
- Publication number
- DE60203307D1 DE60203307D1 DE60203307T DE60203307T DE60203307D1 DE 60203307 D1 DE60203307 D1 DE 60203307D1 DE 60203307 T DE60203307 T DE 60203307T DE 60203307 T DE60203307 T DE 60203307T DE 60203307 D1 DE60203307 D1 DE 60203307D1
- Authority
- DE
- Germany
- Prior art keywords
- emulsion polymerization
- aqueous emulsion
- fluoropolymers
- ethernet
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000007720 emulsion polymerization reaction Methods 0.000 title abstract 2
- 229920002313 fluoropolymer Polymers 0.000 title abstract 2
- 239000004811 fluoropolymer Substances 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 abstract 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 2
- BZLVMXJERCGZMT-UHFFFAOYSA-N Methyl tert-butyl ether Chemical compound COC(C)(C)C BZLVMXJERCGZMT-UHFFFAOYSA-N 0.000 abstract 2
- 239000000178 monomer Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F259/00—Macromolecular compounds obtained by polymerising monomers on to polymers of halogen containing monomers as defined in group C08F14/00
- C08F259/08—Macromolecular compounds obtained by polymerising monomers on to polymers of halogen containing monomers as defined in group C08F14/00 on to polymers containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F14/18—Monomers containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F16/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical
- C08F16/12—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical by an ether radical
- C08F16/14—Monomers containing only one unsaturated aliphatic radical
- C08F16/24—Monomers containing halogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/38—Polymerisation using regulators, e.g. chain terminating agents, e.g. telomerisation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F210/02—Ethene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F214/18—Monomers containing fluorine
- C08F214/22—Vinylidene fluoride
- C08F214/222—Vinylidene fluoride with fluorinated vinyl ethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F214/18—Monomers containing fluorine
- C08F214/22—Vinylidene fluoride
- C08F214/225—Vinylidene fluoride with non-fluorinated comonomers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F214/18—Monomers containing fluorine
- C08F214/26—Tetrafluoroethene
- C08F214/265—Tetrafluoroethene with non-fluorinated comonomers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F216/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical
- C08F216/12—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical by an ether radical
- C08F216/14—Monomers containing only one unsaturated aliphatic radical
- C08F216/1408—Monomers containing halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
- Graft Or Block Polymers (AREA)
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US28824801P | 2001-05-02 | 2001-05-02 | |
US288248P | 2001-05-02 | ||
PCT/US2002/013689 WO2002088203A2 (en) | 2001-05-02 | 2002-04-30 | Aqueous emulsion polymerization in the presence of ethers as chain transfer agents to produce fluoropolymers |
EP02731593.6A EP1432744B2 (de) | 2001-05-02 | 2002-04-30 | Wässrige emulsionspolymerisation in gegenwart von ethern als kettenübertragungsmitteln zur herstellung von fluorpolymeren |
Publications (3)
Publication Number | Publication Date |
---|---|
DE60203307D1 true DE60203307D1 (de) | 2005-04-21 |
DE60203307T2 DE60203307T2 (de) | 2006-04-13 |
DE60203307T3 DE60203307T3 (de) | 2015-01-29 |
Family
ID=23106351
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE60203307.1T Expired - Lifetime DE60203307T3 (de) | 2001-05-02 | 2002-04-30 | Wässrige emulsionspolymerisation in gegenwart von ethern als kettenübertragungsmitteln zur herstellung von fluorpolymeren |
Country Status (9)
Country | Link |
---|---|
US (2) | US6750304B2 (de) |
EP (1) | EP1432744B2 (de) |
JP (1) | JP4624646B2 (de) |
CN (1) | CN1289547C (de) |
AT (1) | ATE291043T1 (de) |
AU (1) | AU2002303564A1 (de) |
CA (1) | CA2446014A1 (de) |
DE (1) | DE60203307T3 (de) |
WO (1) | WO2002088203A2 (de) |
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US7279522B2 (en) | 2001-09-05 | 2007-10-09 | 3M Innovative Properties Company | Fluoropolymer dispersions containing no or little low molecular weight fluorinated surfactant |
EP1587784B1 (de) | 2003-01-29 | 2014-10-15 | Greene, Tweed Of Delaware, Inc. | Vulkanisationsmittel auf bisaminophenylbasis und vulkanisationsmittel auf amidinbasis und vulkanisationsbeschleuniger für perfluorelastomere zusammensetzungen |
WO2005000917A1 (en) * | 2003-01-29 | 2005-01-06 | Greene, Tweed Of Delaware, Inc. | Bisaminopehnyl-based curatives curatives and amidine-based curatives and cure accelerators for perfluoroelastomeric compositions. |
JP2005036189A (ja) * | 2003-07-14 | 2005-02-10 | Rohm & Haas Co | 水性ポリマー分散体の調製のための水性重合方法 |
MXPA06000916A (es) * | 2003-07-24 | 2006-05-04 | Union Carbide Chem Plastic | Sistema de aislamiento de cable con flexibilidad, resistencia de deformacion a alta temperatura y grado reducido de pegajosidad. |
BRPI0414785A (pt) * | 2003-09-25 | 2006-11-21 | Laurel Products Llc | dispersões de politetrafluoroetileno de alta estabilidade e método de obtenção das mesmas |
US20050124773A1 (en) * | 2003-12-09 | 2005-06-09 | Tang Phan L. | Extrudable fluoroelastomer composition |
ATE433350T1 (de) * | 2004-03-01 | 2009-06-15 | 3M Innovative Properties Co | Verfahren zum beschichten eines gegenstands mit einer fluorhaltigen kunststoffsdispersion |
US7514506B2 (en) | 2004-03-31 | 2009-04-07 | Greene, Tweed Of Delaware, Inc. | Fast curing fluoroelastomeric compositions, adhesive fluoroelastomeric compositions and methods for bonding fluoroelastomeric compositions |
FR2871898B1 (fr) * | 2004-06-18 | 2006-09-08 | Alcatel Sa | Composant a fibre optique et fibre optique associee |
EP1630179B1 (de) * | 2004-08-25 | 2007-10-31 | Asahi Glass Company Ltd. | Fluorocopolymer |
GB2427170A (en) * | 2005-06-17 | 2006-12-20 | 3M Innovative Properties Co | Fluoropolymer film having glass microspheres |
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GB0525978D0 (en) | 2005-12-21 | 2006-02-01 | 3M Innovative Properties Co | Fluorinated Surfactants For Making Fluoropolymers |
GB0514387D0 (en) * | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant |
US7795332B2 (en) * | 2005-07-15 | 2010-09-14 | 3M Innovative Properties Company | Method of removing fluorinated carboxylic acid from aqueous liquid |
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US7754795B2 (en) * | 2006-05-25 | 2010-07-13 | 3M Innovative Properties Company | Coating composition |
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US7678859B2 (en) * | 2006-09-14 | 2010-03-16 | 3M Innovative Properties Company | Preparation and stabilization of fluoropolymer dispersions |
JP5332617B2 (ja) * | 2006-12-08 | 2013-11-06 | ダイキン工業株式会社 | フルオロモノマーの回収方法 |
WO2008127461A2 (en) * | 2006-12-12 | 2008-10-23 | 3M Innovative Properties Company | Thermally stable fluoropolymers |
CN100406480C (zh) * | 2006-12-28 | 2008-07-30 | 中昊晨光化工研究院 | 高氟含量的氟弹性体及其制备方法 |
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WO2008101137A1 (en) * | 2007-02-16 | 2008-08-21 | 3M Innovative Properties Company | System and process for the removal of fluorochemicals from water |
US20080264864A1 (en) | 2007-04-27 | 2008-10-30 | 3M Innovative Properties Company | PROCESS FOR REMOVING FLUORINATED EMULSIFIER FROM FLUOROPOLMER DISPERSIONS USING AN ANION-EXCHANGE RESIN AND A pH-DEPENDENT SURFACTANT AND FLUOROPOLYMER DISPERSIONS CONTAINING A pH-DEPENDENT SURFACTANT |
KR20100017848A (ko) * | 2007-05-23 | 2010-02-16 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 플루오르화 계면활성제의 수성 조성물 및 그의 사용 방법 |
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US6281296B1 (en) | 1998-08-10 | 2001-08-28 | Dupont Dow Elastomers L.L.C. | Curable perfluoroelastomer composition |
EP1141047B1 (de) | 1998-11-30 | 2009-03-11 | E.I. Du Pont De Nemours And Company | Fluoromonomerpolymerisation |
US6242548B1 (en) | 1999-05-13 | 2001-06-05 | Dyneon Llc | Fluoroplastic polymers with improved characteristics |
US6720360B1 (en) * | 2000-02-01 | 2004-04-13 | 3M Innovative Properties Company | Ultra-clean fluoropolymers |
US6716945B2 (en) * | 2000-05-19 | 2004-04-06 | North Carolina State University | Multimodal fluoropolymers and methods of making the same |
US6310141B1 (en) | 2000-06-27 | 2001-10-30 | Dyneon Llc | Fluoropolymer-containing compositions |
CN1290880C (zh) * | 2001-05-02 | 2006-12-20 | 3M创新有限公司 | 制备氟聚合物的无乳化剂水乳液聚合方法 |
JP4624646B2 (ja) * | 2001-05-02 | 2011-02-02 | スリーエム イノベイティブ プロパティズ カンパニー | フルオロポリマーを製造するための連鎖移動剤としてのエーテルの存在下での水性乳化重合 |
US7064170B2 (en) * | 2002-10-31 | 2006-06-20 | 3M Innovative Properties Company | Emulsifier free aqueous emulsion polymerization to produce copolymers of a fluorinated olefin and hydrocarbon olefin |
-
2002
- 2002-04-30 JP JP2002585500A patent/JP4624646B2/ja not_active Expired - Fee Related
- 2002-04-30 DE DE60203307.1T patent/DE60203307T3/de not_active Expired - Lifetime
- 2002-04-30 WO PCT/US2002/013689 patent/WO2002088203A2/en active IP Right Grant
- 2002-04-30 CN CN02811110.9A patent/CN1289547C/zh not_active Expired - Fee Related
- 2002-04-30 AU AU2002303564A patent/AU2002303564A1/en not_active Abandoned
- 2002-04-30 EP EP02731593.6A patent/EP1432744B2/de not_active Expired - Lifetime
- 2002-04-30 US US10/136,912 patent/US6750304B2/en not_active Expired - Fee Related
- 2002-04-30 CA CA002446014A patent/CA2446014A1/en not_active Abandoned
- 2002-04-30 AT AT02731593T patent/ATE291043T1/de not_active IP Right Cessation
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2004
- 2004-06-14 US US10/867,256 patent/US6861490B2/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
EP1432744B1 (de) | 2005-03-16 |
EP1432744A2 (de) | 2004-06-30 |
JP2004534118A (ja) | 2004-11-11 |
US20040235986A1 (en) | 2004-11-25 |
ATE291043T1 (de) | 2005-04-15 |
WO2002088203A2 (en) | 2002-11-07 |
US20030018148A1 (en) | 2003-01-23 |
US6750304B2 (en) | 2004-06-15 |
AU2002303564A1 (en) | 2002-11-11 |
WO2002088203A3 (en) | 2004-04-29 |
DE60203307T2 (de) | 2006-04-13 |
EP1432744B2 (de) | 2014-10-01 |
CA2446014A1 (en) | 2002-11-07 |
US6861490B2 (en) | 2005-03-01 |
DE60203307T3 (de) | 2015-01-29 |
JP4624646B2 (ja) | 2011-02-02 |
CN1529720A (zh) | 2004-09-15 |
CN1289547C (zh) | 2006-12-13 |
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