DE602004004639D1 - Kontinuierliches verfahren und system zur herstellung von polyetherpolyolen - Google Patents

Kontinuierliches verfahren und system zur herstellung von polyetherpolyolen

Info

Publication number
DE602004004639D1
DE602004004639D1 DE602004004639T DE602004004639T DE602004004639D1 DE 602004004639 D1 DE602004004639 D1 DE 602004004639D1 DE 602004004639 T DE602004004639 T DE 602004004639T DE 602004004639 T DE602004004639 T DE 602004004639T DE 602004004639 D1 DE602004004639 D1 DE 602004004639D1
Authority
DE
Germany
Prior art keywords
loop reactor
rate
reactor
catalyst
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE602004004639T
Other languages
English (en)
Other versions
DE602004004639T2 (de
Inventor
W Verwijs
J Papadopulos
W Weston
J Elwell
M Villa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Global Technologies LLC
Original Assignee
Dow Global Technologies LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies LLC filed Critical Dow Global Technologies LLC
Publication of DE602004004639D1 publication Critical patent/DE602004004639D1/de
Application granted granted Critical
Publication of DE602004004639T2 publication Critical patent/DE602004004639T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1812—Tubular reactors
    • B01J19/1837—Loop-type reactors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Toxicology (AREA)
  • Polyethers (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
DE602004004639T 2003-03-07 2004-03-05 Kontinuierliches verfahren und system zur herstellung von polyetherpolyolen Expired - Fee Related DE602004004639T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US45307303P 2003-03-07 2003-03-07
US453073P 2003-03-07
PCT/US2004/006643 WO2004081082A1 (en) 2003-03-07 2004-03-05 Continuous process and system of producing polyether polyols

Publications (2)

Publication Number Publication Date
DE602004004639D1 true DE602004004639D1 (de) 2007-03-22
DE602004004639T2 DE602004004639T2 (de) 2007-11-08

Family

ID=32990720

Family Applications (1)

Application Number Title Priority Date Filing Date
DE602004004639T Expired - Fee Related DE602004004639T2 (de) 2003-03-07 2004-03-05 Kontinuierliches verfahren und system zur herstellung von polyetherpolyolen

Country Status (13)

Country Link
US (2) US7378559B2 (de)
EP (1) EP1603965B1 (de)
JP (1) JP2007524719A (de)
KR (1) KR20050107604A (de)
CN (1) CN1867609A (de)
AT (1) ATE353348T1 (de)
AU (1) AU2004220072A1 (de)
BR (1) BRPI0408669A (de)
CA (1) CA2518201A1 (de)
DE (1) DE602004004639T2 (de)
MX (1) MXPA05009512A (de)
WO (1) WO2004081082A1 (de)
ZA (1) ZA200506576B (de)

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EP2035479B1 (de) * 2006-06-23 2010-07-07 Basf Se Verfahren zur kontinuierlichen herstellung von polyetheralkoholen
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AR073933A1 (es) * 2008-05-19 2010-12-15 Dow Global Technologies Inc Procedimiento de flujo de recirculacion continuo para la produccion de poliol de polieter
CN102177117A (zh) * 2008-10-13 2011-09-07 陶氏环球技术有限责任公司 用于生产氯化和/或氟化丙烯的方法
EP2485996B1 (de) * 2009-10-09 2016-06-15 Blue Cube IP LLC Verfahren zur herstellung chlorinierter und/oder fluorinierter propene
BR112012007914A2 (pt) 2009-10-09 2019-09-24 Dow Global Technologies Llc reator isotérmico de tubos múltiplos, processo para produzir um propeno clorado ou fluorado e processo para preparar 2,3,3,3- tetrafluorprop-1-eno (hfo-1234yf) ou 1,3,3,3- tetrafluorprop-1-eno (hfo-1234ze)
EP2485997B1 (de) * 2009-10-09 2015-09-09 Dow Global Technologies LLC Verfahren zur herstellung von chlorierten und/oder fluorierten probenen und höheren alkenen
CN102753603B (zh) 2009-12-14 2015-01-14 陶氏环球技术有限责任公司 使用双金属氰化物催化剂连续制备低当量多元醇的方法
WO2011089120A1 (de) 2010-01-20 2011-07-28 Bayer Materialscience Ag Verfahren zur aktivierung von doppelmetallcyanidkatalysatoren zur herstellung von polyethercarbonatpolyolen
DE102010008410A1 (de) 2010-02-18 2011-08-18 Bayer MaterialScience AG, 51373 Verfahren zur Herstellung von Polyethercarbonatpolyolen
JP2013522438A (ja) 2010-03-24 2013-06-13 バイエル・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツング ポリエーテルカーボネートポリオールの製造方法
US8946466B2 (en) 2010-05-18 2015-02-03 Bayer Intellectual Property Gmbh Method for producing polyether carbonate polyols
DE102010040517A1 (de) 2010-09-09 2012-03-15 Bayer Materialscience Aktiengesellschaft Verfahren zur Herstellung von Polyetherpolyolen
DE102010043409A1 (de) 2010-11-04 2012-05-10 Bayer Materialscience Aktiengesellschaft Verfahren zur Herstellung von Polycarbonatpolyolen durch immortale Polymerisation von cyclischen Carbonaten
EP2465890A1 (de) 2010-12-17 2012-06-20 Bayer MaterialScience AG Verfahren zur Herstellung von Polyethercarbonatpolyolen mit primären Hydroxyl-Endgruppen und daraus hergestellte Polyurethanpolymere
ES2528910T3 (es) * 2011-02-24 2015-02-13 Shell Internationale Research Maatschappij B.V. Proceso para la preparación de poliéter polioles
JP5918358B2 (ja) 2011-05-31 2016-05-18 ブルー キューブ アイピー エルエルシー 塩素化プロペンの製造方法
WO2012166393A1 (en) 2011-05-31 2012-12-06 Dow Global Technologies, Llc Process for the production of chlorinated propenes
US8927792B2 (en) 2011-06-08 2015-01-06 Dow Agrosciences, Llc Process for the production of chlorinated and/or fluorinated propenes
US9233896B2 (en) 2011-08-07 2016-01-12 Blue Cube Ip Llc Process for the production of chlorinated propenes
WO2013022676A1 (en) 2011-08-07 2013-02-14 Dow Global Technologies, Llc Process for the production of chlorinated propenes
IN2014CN03748A (de) 2011-11-21 2015-09-25 Dow Global Technologies Llc
CN104024187B (zh) 2011-12-02 2017-04-12 蓝立方知识产权有限责任公司 生产氯化烷烃的方法
EP2785670B1 (de) 2011-12-02 2017-10-25 Blue Cube IP LLC Verfahren zur herstellung von chlorierten alkanen
JP6170068B2 (ja) 2011-12-13 2017-07-26 ブルー キューブ アイピー エルエルシー 塩素化プロパン及びプロペンの製造方法
WO2013096311A1 (en) 2011-12-22 2013-06-27 Dow Global Technologies, Llc Process for the production of tetrachloromethane
EP2794521B1 (de) 2011-12-23 2016-09-21 Dow Global Technologies LLC Verfahren zur herstellung von alkenen und/oder geschmacksstoffen
CN104755448A (zh) 2012-09-20 2015-07-01 陶氏环球技术有限公司 用于制造氯化丙烯的方法
EP2897930A1 (de) 2012-09-20 2015-07-29 Dow Global Technologies LLC Verfahren zur herstellung von chlorierten propenen
EP2900364B1 (de) 2012-09-30 2018-06-13 Blue Cube IP LLC Wehrlöschung und verfahren damit
US10065157B2 (en) 2012-10-26 2018-09-04 Blue Cube Ip Llc Mixer and processes incorporating the same
CA2893841C (en) 2012-12-18 2018-07-24 Dow Global Technologies Llc Process for the production of chlorinated propenes
EP2935166A1 (de) 2012-12-19 2015-10-28 Blue Cube IP LLC Verfahren zur herstellung von chlorierten propenen
EP2961722A2 (de) 2013-02-27 2016-01-06 Blue Cube IP LLC Verfahren zur herstellung von chlorierten propenen
WO2014164368A1 (en) 2013-03-09 2014-10-09 Dow Global Technologies Llc Process for the production of chlorinated alkanes
KR20160018546A (ko) 2013-06-13 2016-02-17 코베스트로 도이칠란트 아게 폴리에테르카르보네이트-폴리옥시메틸렌 블록 공중합체
EP4007788B1 (de) 2019-08-01 2023-08-09 Dow Global Technologies LLC Verfahren zur reinigung von polyetherpolyolen

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Also Published As

Publication number Publication date
KR20050107604A (ko) 2005-11-14
CN1867609A (zh) 2006-11-22
ZA200506576B (en) 2006-12-27
CA2518201A1 (en) 2004-09-23
ATE353348T1 (de) 2007-02-15
US20060155151A1 (en) 2006-07-13
US20080221281A1 (en) 2008-09-11
DE602004004639T2 (de) 2007-11-08
JP2007524719A (ja) 2007-08-30
BRPI0408669A (pt) 2006-03-28
EP1603965A1 (de) 2005-12-14
MXPA05009512A (es) 2006-02-22
WO2004081082A1 (en) 2004-09-23
AU2004220072A1 (en) 2004-09-23
US7378559B2 (en) 2008-05-27
EP1603965B1 (de) 2007-02-07

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