DE60115384T2 - Chemisches verfahren - Google Patents

Chemisches verfahren Download PDF

Info

Publication number
DE60115384T2
DE60115384T2 DE60115384T DE60115384T DE60115384T2 DE 60115384 T2 DE60115384 T2 DE 60115384T2 DE 60115384 T DE60115384 T DE 60115384T DE 60115384 T DE60115384 T DE 60115384T DE 60115384 T2 DE60115384 T2 DE 60115384T2
Authority
DE
Germany
Prior art keywords
reactor
hydrogenation
reaction
reaction mixture
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Revoked
Application number
DE60115384T
Other languages
German (de)
English (en)
Other versions
DE60115384D1 (de
Inventor
Marius Vaarkamp
Hendrik Bernard REESINK
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF Catalysts LLC
Original Assignee
Engelhard Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=8170975&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE60115384(T2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Engelhard Corp filed Critical Engelhard Corp
Application granted granted Critical
Publication of DE60115384D1 publication Critical patent/DE60115384D1/de
Publication of DE60115384T2 publication Critical patent/DE60115384T2/de
Anticipated expiration legal-status Critical
Revoked legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2455Stationary reactors without moving elements inside provoking a loop type movement of the reactants
    • B01J19/2465Stationary reactors without moving elements inside provoking a loop type movement of the reactants externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/007Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor in the presence of catalytically active bodies, e.g. porous plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/248Reactors comprising multiple separated flow channels
    • B01J19/2485Monolithic reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/32Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00Catalysts, in general, characterised by their form or physical properties
    • B01J35/50Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/56Foraminous structures having flow-through passages or channels, e.g. grids or three-dimensional [3D] monoliths
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B35/00Reactions without formation or introduction of functional groups containing hetero atoms, involving a change in the type of bonding between two carbon atoms already directly linked
    • C07B35/02Reduction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00085Plates; Jackets; Cylinders
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322Basic shape of the elements
    • B01J2219/32296Honeycombs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/324Composition or microstructure of the elements
    • B01J2219/32408Metal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/324Composition or microstructure of the elements
    • B01J2219/32425Ceramic
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/324Composition or microstructure of the elements
    • B01J2219/32466Composition or microstructure of the elements comprising catalytically active material

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
DE60115384T 2000-02-03 2001-02-05 Chemisches verfahren Revoked DE60115384T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP00200371 2000-02-03
EP00200371A EP1121976A1 (en) 2000-02-03 2000-02-03 Chemical process in reactor with structured catalyst
PCT/NL2001/000088 WO2001056692A1 (en) 2000-02-03 2001-02-05 Chemical process

Publications (2)

Publication Number Publication Date
DE60115384D1 DE60115384D1 (de) 2006-01-05
DE60115384T2 true DE60115384T2 (de) 2006-07-13

Family

ID=8170975

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60115384T Revoked DE60115384T2 (de) 2000-02-03 2001-02-05 Chemisches verfahren

Country Status (11)

Country Link
US (1) US6800773B2 (https=)
EP (2) EP1121976A1 (https=)
JP (1) JP2003521525A (https=)
KR (1) KR100826346B1 (https=)
AT (1) ATE311247T1 (https=)
AU (1) AU2001237798A1 (https=)
CA (1) CA2398966C (https=)
DE (1) DE60115384T2 (https=)
DK (1) DK1253974T3 (https=)
ES (1) ES2249414T3 (https=)
WO (1) WO2001056692A1 (https=)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7109378B2 (en) * 2001-08-30 2006-09-19 Air Products And Chemicals, Inc. Monolith catalytic reactor coupled to static mixer
WO2009093093A1 (en) * 2008-01-21 2009-07-30 Rosario Rocco Tulino Industrial production process of diethyl carbonate (dec) by means of heterogeneous catalytic synthesis reactor fed by ethylic ether and carbon dioxide
US7524995B1 (en) * 2008-06-12 2009-04-28 E.I. Du Pont De Nemours And Company Continuous process to produce hexafluoroisopropanol
US8697015B2 (en) 2011-12-01 2014-04-15 Chevron U.S.A. Inc. Flow distribution for monolithic reactors
CN104190329B (zh) * 2014-08-29 2016-05-25 武汉工程大学 一种双夹套式固定床反应器
KR101988863B1 (ko) * 2017-12-04 2019-06-13 한국과학기술연구원 과산화수소 증기 제독 시스템
CN110639598A (zh) * 2018-06-27 2020-01-03 中国石化工程建设有限公司 用于催化剂再生工艺的催化剂氧氯化及干燥的方法及催化剂再生工艺

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE431532B (sv) * 1982-09-08 1984-02-13 Eka Ab Forfarande vid framstellning av veteperoxid
EP0233642A3 (en) * 1986-02-18 1989-09-06 W.R. Grace & Co.-Conn. Process for hydrogenation of organic compounds
DE4243424A1 (de) * 1992-12-16 1994-06-23 Auf Adlershofer Umweltschutzte Verfahren und Vorrichtung zur Reaktionsführung in Schlaufenreaktoren mit Wabenkörpern
AT398759B (de) * 1993-03-12 1995-01-25 Chemie Linz Gmbh Hydrogenolytische reduktion peroxidischer ozonolyseprodukte und vorrichtung zu ihrer durchführung
DE4414274A1 (de) * 1994-04-23 1995-10-26 Chemie Linz Deutschland Hydrogenolytische Reduktion eines Aldehyds oder dessen Halbacetals oder dessen Vollacetals zu einem Alkohol
NL1004961C2 (nl) * 1997-01-09 1998-07-13 Dsm Nv Monolietreactor.
SI9800182A (sl) * 1998-06-26 1999-12-31 Kemijski inštitut Proces za čiščenje z nitratnim ionom onesnaženih voda
US6005143A (en) * 1998-08-07 1999-12-21 Air Products And Chemicals, Inc. Use of a monolith catalyst for the hydrogenation of dinitrotoluene to toluenediamine

Also Published As

Publication number Publication date
DK1253974T3 (da) 2005-12-27
ATE311247T1 (de) 2005-12-15
JP2003521525A (ja) 2003-07-15
EP1253974A1 (en) 2002-11-06
KR100826346B1 (ko) 2008-05-02
CA2398966A1 (en) 2001-08-09
KR20030004339A (ko) 2003-01-14
US6800773B2 (en) 2004-10-05
EP1121976A1 (en) 2001-08-08
WO2001056692A1 (en) 2001-08-09
ES2249414T3 (es) 2006-04-01
DE60115384D1 (de) 2006-01-05
EP1253974B1 (en) 2005-11-30
CA2398966C (en) 2010-02-02
AU2001237798A1 (en) 2001-08-14
US20030144537A1 (en) 2003-07-31

Similar Documents

Publication Publication Date Title
DE60127344T2 (de) Katalysator und Verfahren zur direkten Synthese von Wasserstoffperoxid
DE69906893T2 (de) Verfahren zur Hydrierung von Dinitrotoluol zu Toluenediamin mittels eines monolithischen Katalysators
EP1669337B1 (de) Verfahren zur Herstellung von Alkoholen aus Olefinen durch Hydroformylierung und Hydrierung
DE69209948T2 (de) Verfahren zur Aktivierung eines Fischer-Tropsch Katalysators und der aktivierte Katalysator
DE60129569T2 (de) Verfahren zur herstellung von synthesegas mit lanthanid-dotierter rhodiumkatalysatoren
EP3938337B1 (de) Verfahren und anlage zur herstellung eines oder mehrerer olefine
EP1127864A2 (de) Verbessertes Verfahren zur Hydroformylierung von Olefinen durch Reduzierung der Ameisensäurekonzentration
EP3750866A1 (de) Verfahren zur herstellung eines alkohols aus kohlenwasserstoffen
EP3750620A1 (de) Verfahren zur herstellung eines esters durch alkoxycarbonylierung
DE2166779A1 (de) Verfahren zur herstellung eines hydrierungskatalysators hoher druckfestigkeit
EP1330422A2 (de) Verfahren zur hydrierung von unsubstituierten oder alkylsubstituierten aromaten unter verwendung eines katalysators mit einem strukturierten oder monolithischen träger
DE60115384T2 (de) Chemisches verfahren
EP1257518A1 (de) Verfahren zur herstellung von c 9-alkoholen und verfahren zur integrierten herstellung von c 9-alkoholen und c 10-alkoholen
EP0724907B1 (de) Palladium-Trägerkatalysatoren
DE2743693A1 (de) Verfahren zur herstellung von feststoffkatalysatoren
DE60302773T2 (de) Verfahren zur herstellung von wasserstoffperoxid
EP1404725B1 (de) Kolloidkatalysierte gasübertragung in überkritischer phase
DE3623777A1 (de) Verfahren zur hydrierung von olefinen in gegenwart von (gamma)thern
EP2448892B1 (de) Verfahren zur herstellung von geruchsarmem n-butan
DE60123504T2 (de) Verfahren zur Herstellung von sauerstoffenthaltendem Brennstoff
DE60024297T2 (de) Geträgerte ferrocen-enthaltende katalysatoren zur selektiven aldehyd hydrierung
DE2360379C2 (de) Zweistufiges Verfahren zur Herstellung medizinischer Öle mittels katalytisch hydrierender Behandlung
EP0571920A1 (de) Verfahren zur Herstellung von Fluorkohlenwasserstoffen
DE2653445C2 (de) Verfahren zur Hydrierung von 4-Acetoxycrotonaldehyd enthaltendem 1,4-Diacetoxybuten-2
DE2638798A1 (de) Hydroformylierungsverfahren

Legal Events

Date Code Title Description
8363 Opposition against the patent
8331 Complete revocation