DE60010496T2 - Czochralski-Verfahren zur Herstellung Silizium-Einkristalle durch Steuerung der Abkühlgeschwindigkeit - Google Patents

Czochralski-Verfahren zur Herstellung Silizium-Einkristalle durch Steuerung der Abkühlgeschwindigkeit Download PDF

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Publication number
DE60010496T2
DE60010496T2 DE60010496T DE60010496T DE60010496T2 DE 60010496 T2 DE60010496 T2 DE 60010496T2 DE 60010496 T DE60010496 T DE 60010496T DE 60010496 T DE60010496 T DE 60010496T DE 60010496 T2 DE60010496 T2 DE 60010496T2
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region
axial length
constant diameter
defects
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Expired - Lifetime
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DE60010496T
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German (de)
English (en)
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DE60010496D1 (de
Inventor
Kirk D. Mccallum
Brock W. ALEXANDER
Mohsen Banan
Robert J. Falster
Joseph C. Holzer
Bayard K. Johnson
Chang B. Kim
Steven L. Kimbel
Zheng Lu
Paolo Mutti
Vladimir V. Voronkov
Luciano Mule'stagno
Jeffrey L. Libbert
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SunEdison Inc
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SunEdison Inc
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Publication of DE60010496T2 publication Critical patent/DE60010496T2/de
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    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02Elements
    • C30B29/06Silicon
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C30B15/20Controlling or regulating
    • C30B15/203Controlling or regulating the relationship of pull rate (v) to axial thermal gradient (G)
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C30B15/20Controlling or regulating
    • C30B15/206Controlling or regulating the thermal history of growing the ingot
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B33/00After-treatment of single crystals or homogeneous polycrystalline material with defined structure

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
DE60010496T 1999-09-23 2000-09-18 Czochralski-Verfahren zur Herstellung Silizium-Einkristalle durch Steuerung der Abkühlgeschwindigkeit Expired - Lifetime DE60010496T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US15572599P 1999-09-23 1999-09-23
US155725P 1999-09-23
PCT/US2000/025525 WO2001021861A1 (en) 1999-09-23 2000-09-18 Czochralski process for growing single crystal silicon by controlling the cooling rate

Publications (2)

Publication Number Publication Date
DE60010496D1 DE60010496D1 (de) 2004-06-09
DE60010496T2 true DE60010496T2 (de) 2005-04-07

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
DE60010496T Expired - Lifetime DE60010496T2 (de) 1999-09-23 2000-09-18 Czochralski-Verfahren zur Herstellung Silizium-Einkristalle durch Steuerung der Abkühlgeschwindigkeit

Country Status (7)

Country Link
US (1) US20030196587A1 (enExample)
EP (1) EP1222324B1 (enExample)
JP (1) JP2003510235A (enExample)
KR (1) KR100745311B1 (enExample)
DE (1) DE60010496T2 (enExample)
TW (1) TW571006B (enExample)
WO (1) WO2001021861A1 (enExample)

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US7105050B2 (en) 2000-11-03 2006-09-12 Memc Electronic Materials, Inc. Method for the production of low defect density silicon
US6858307B2 (en) 2000-11-03 2005-02-22 Memc Electronic Materials, Inc. Method for the production of low defect density silicon
US8529695B2 (en) 2000-11-22 2013-09-10 Sumco Corporation Method for manufacturing a silicon wafer
DE10066124B4 (de) * 2000-11-24 2007-12-13 Mitsubishi Materials Silicon Corp. Silicium-Wafer
EP2295619B1 (en) * 2001-01-26 2014-04-23 MEMC Electronic Materials, Inc. Process for producing Low Defect Density Silicon Having a Vacancy-Dominated Core Substantially Free of Oxidation Induced Stacking Faults
CN1327041C (zh) 2002-11-12 2007-07-18 Memc电子材料有限公司 用于生长单晶锭的拉晶机和方法
WO2005029547A2 (en) 2003-09-16 2005-03-31 The Trustees Of Columbia University In The City Of New York Enhancing the width of polycrystalline grains with mask
KR101385810B1 (ko) * 2006-05-19 2014-04-16 엠이엠씨 일렉트로닉 머티리얼즈, 인크. Cz 성장 동안에 실리콘 단결정의 측면에 의해 유도되는 응집된 점 결함 및 산소 클러스터 형성을 제어하는 방법
ITTO20110335A1 (it) * 2011-04-14 2012-10-15 Consiglio Nazionale Ricerche Procedimento di formazione di cristalli massivi, in particolare monocristalli di fluoruri drogati con ioni di terre rare
JP6716344B2 (ja) * 2016-06-01 2020-07-01 グローバルウェーハズ・ジャパン株式会社 シリコンウェーハの熱処理方法
SG11202110994TA (en) 2019-04-11 2021-10-28 Globalwafers Co Ltd Process for preparing ingot having reduced distortion at late body length
CN113728129B (zh) 2019-04-18 2024-09-03 环球晶圆股份有限公司 使用连续柴可斯基(czochralski)方法生长单晶硅锭的方法
EP4028583B1 (en) 2019-09-13 2023-10-04 GlobalWafers Co., Ltd. Method for growing a nitrogen doped single crystal silicon ingot using continuous czochralski method
CN114182355B (zh) * 2021-11-30 2023-03-28 徐州鑫晶半导体科技有限公司 消除间隙型缺陷B-swirl的方法、硅片及电子器件
US20250293073A1 (en) 2024-03-18 2025-09-18 Globalwafers Co., Ltd. Reclaimable donor substrates for use in preparing multiple silicon-on-insulator structures

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JPS59232995A (ja) * 1983-06-10 1984-12-27 Sumitomo Electric Ind Ltd 引上単結晶の冷却方法
US5264189A (en) * 1988-02-23 1993-11-23 Mitsubishi Materials Corporation Apparatus for growing silicon crystals
US4981549A (en) * 1988-02-23 1991-01-01 Mitsubishi Kinzoku Kabushiki Kaisha Method and apparatus for growing silicon crystals
IT1280041B1 (it) * 1993-12-16 1997-12-29 Wacker Chemitronic Procedimento per il tiraggio di un monocristallo di silicio
JP3285111B2 (ja) * 1994-12-05 2002-05-27 信越半導体株式会社 結晶欠陥の少ないシリコン単結晶の製造方法
JP3085146B2 (ja) * 1995-05-31 2000-09-04 住友金属工業株式会社 シリコン単結晶ウェーハおよびその製造方法
JPH08337490A (ja) * 1995-06-09 1996-12-24 Shin Etsu Handotai Co Ltd 結晶欠陥の少ないシリコン単結晶及びその製造方法
JP3006669B2 (ja) * 1995-06-20 2000-02-07 信越半導体株式会社 結晶欠陥の均一なシリコン単結晶の製造方法およびその製造装置
US5676751A (en) * 1996-01-22 1997-10-14 Memc Electronic Materials, Inc. Rapid cooling of CZ silicon crystal growth system
US5840120A (en) * 1996-01-22 1998-11-24 Memc Electronic Materials, Inc. Apparatus for controlling nucleation of oxygen precipitates in silicon crystals
DE19637182A1 (de) * 1996-09-12 1998-03-19 Wacker Siltronic Halbleitermat Verfahren zur Herstellung von Halbleiterscheiben aus Silicium mit geringer Defektdichte
JPH10152395A (ja) * 1996-11-21 1998-06-09 Komatsu Electron Metals Co Ltd シリコン単結晶の製造方法
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US6236104B1 (en) * 1998-09-02 2001-05-22 Memc Electronic Materials, Inc. Silicon on insulator structure from low defect density single crystal silicon
US6336968B1 (en) * 1998-09-02 2002-01-08 Memc Electronic Materials, Inc. Non-oxygen precipitating czochralski silicon wafers
US6361619B1 (en) * 1998-09-02 2002-03-26 Memc Electronic Materials, Inc. Thermally annealed wafers having improved internal gettering
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Also Published As

Publication number Publication date
WO2001021861A1 (en) 2001-03-29
TW571006B (en) 2004-01-11
KR20020042689A (ko) 2002-06-05
DE60010496D1 (de) 2004-06-09
US20030196587A1 (en) 2003-10-23
KR100745311B1 (ko) 2007-08-01
EP1222324A1 (en) 2002-07-17
EP1222324B1 (en) 2004-05-06
JP2003510235A (ja) 2003-03-18

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