DE3618426C1 - Verfahren zur Herstellung von Kohlenstoffmolekularsieben - Google Patents
Verfahren zur Herstellung von KohlenstoffmolekularsiebenInfo
- Publication number
- DE3618426C1 DE3618426C1 DE3618426A DE3618426A DE3618426C1 DE 3618426 C1 DE3618426 C1 DE 3618426C1 DE 3618426 A DE3618426 A DE 3618426A DE 3618426 A DE3618426 A DE 3618426A DE 3618426 C1 DE3618426 C1 DE 3618426C1
- Authority
- DE
- Germany
- Prior art keywords
- vibro
- carbon
- countercurrent
- vol
- inert gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims description 24
- 229910052799 carbon Inorganic materials 0.000 title claims description 21
- 239000002808 molecular sieve Substances 0.000 title claims description 19
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 title claims description 19
- 238000000034 method Methods 0.000 title claims description 9
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 27
- 239000000463 material Substances 0.000 claims description 18
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 16
- 239000011261 inert gas Substances 0.000 claims description 10
- 229910052757 nitrogen Inorganic materials 0.000 claims description 8
- 239000011148 porous material Substances 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 5
- 239000001301 oxygen Substances 0.000 claims description 5
- 229910052760 oxygen Inorganic materials 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- 229930195733 hydrocarbon Natural products 0.000 claims description 4
- 150000002430 hydrocarbons Chemical class 0.000 claims description 4
- 238000003763 carbonization Methods 0.000 claims 3
- 238000010438 heat treatment Methods 0.000 description 9
- 230000004913 activation Effects 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 3
- 239000012495 reaction gas Substances 0.000 description 3
- MQLRCIFIYCHDKV-UHFFFAOYSA-N [N].C1=CC=CC=C1 Chemical compound [N].C1=CC=CC=C1 MQLRCIFIYCHDKV-UHFFFAOYSA-N 0.000 description 2
- 239000005539 carbonized material Substances 0.000 description 2
- 238000003795 desorption Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- 239000003575 carbonaceous material Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/28—Moving reactors, e.g. rotary drums
- B01J19/285—Shaking or vibrating reactors; reactions under the influence of low-frequency vibrations or pulsations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
- C01B13/02—Preparation of oxygen
- C01B13/0229—Purification or separation processes
- C01B13/0248—Physical processing only
- C01B13/0259—Physical processing only by adsorption on solids
- C01B13/0262—Physical processing only by adsorption on solids characterised by the adsorbent
- C01B13/0266—Carbon based materials
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/04—Purification or separation of nitrogen
- C01B21/0405—Purification or separation processes
- C01B21/0433—Physical processing only
- C01B21/045—Physical processing only by adsorption in solids
- C01B21/0455—Physical processing only by adsorption in solids characterised by the adsorbent
- C01B21/0461—Carbon based materials
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/306—Active carbon with molecular sieve properties
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/39—Apparatus for the preparation thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2210/00—Purification or separation of specific gases
- C01B2210/0043—Impurity removed
- C01B2210/0045—Oxygen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2210/00—Purification or separation of specific gases
- C01B2210/0043—Impurity removed
- C01B2210/0046—Nitrogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Carbon And Carbon Compounds (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3618426A DE3618426C1 (de) | 1986-05-31 | 1986-05-31 | Verfahren zur Herstellung von Kohlenstoffmolekularsieben |
| JP62503239A JPH01502743A (ja) | 1986-05-31 | 1987-05-22 | 炭素モレキユラーシーブの製造法 |
| US07/272,694 US4880765A (en) | 1986-05-31 | 1987-05-22 | Process for producing carbon molecular sieves |
| EP87903311A EP0308409B1 (de) | 1986-05-31 | 1987-05-22 | Verfahren zur herstellung von kohlenstoffmolekularsieben |
| PCT/EP1987/000268 WO1987007249A1 (fr) | 1986-05-31 | 1987-05-22 | Procede de fabrication de tamis moleculaires de carbone |
| DE8787903311T DE3769648D1 (de) | 1986-05-31 | 1987-05-22 | Verfahren zur herstellung von kohlenstoffmolekularsieben. |
| AT87903311T ATE62895T1 (de) | 1986-05-31 | 1987-05-22 | Verfahren zur herstellung von kohlenstoffmolekularsieben. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3618426A DE3618426C1 (de) | 1986-05-31 | 1986-05-31 | Verfahren zur Herstellung von Kohlenstoffmolekularsieben |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3618426C1 true DE3618426C1 (de) | 1987-07-02 |
Family
ID=6302082
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE3618426A Expired DE3618426C1 (de) | 1986-05-31 | 1986-05-31 | Verfahren zur Herstellung von Kohlenstoffmolekularsieben |
| DE8787903311T Expired - Fee Related DE3769648D1 (de) | 1986-05-31 | 1987-05-22 | Verfahren zur herstellung von kohlenstoffmolekularsieben. |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8787903311T Expired - Fee Related DE3769648D1 (de) | 1986-05-31 | 1987-05-22 | Verfahren zur herstellung von kohlenstoffmolekularsieben. |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4880765A (enExample) |
| EP (1) | EP0308409B1 (enExample) |
| JP (1) | JPH01502743A (enExample) |
| DE (2) | DE3618426C1 (enExample) |
| WO (1) | WO1987007249A1 (enExample) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1991004788A1 (de) * | 1989-10-06 | 1991-04-18 | Bergwerksverband Gmbh | Kohlenstoff-molekularsieb zur zerlegung von luft in stickstoff und sauerstoff durch druckwechseltechnik |
| DE4031580A1 (de) * | 1990-10-05 | 1992-04-09 | Bergwerksverband Gmbh | Verfahren zur herstellung von kohlenstoffmolekularsieben |
| DE4031578A1 (de) * | 1990-10-05 | 1992-04-09 | Bergwerksverband Gmbh | Verfahren zur herstellung von kohlenstoffmolekularsieben |
| EP0474106A3 (en) * | 1990-08-30 | 1992-04-15 | Air Products And Chemicals, Inc. | Modified carbon molecular sieves for gas separation |
| EP0481218A1 (en) * | 1990-09-14 | 1992-04-22 | Air Products And Chemicals, Inc. | A process for making modified carbon molecular sieve adsorbents |
| DE4132971A1 (de) * | 1991-10-04 | 1993-04-08 | Bergwerksverband Gmbh | Verfahren zur herstellung von kohlenstoffmolekularsieben |
| FR2702392A1 (fr) * | 1993-03-12 | 1994-09-16 | Inst Francais Du Petrole | Procédé et dispositif de régénération d'absorbant régénérables. |
| DE10127768A1 (de) * | 2001-06-07 | 2002-12-19 | Carbo Tech Aktivkohlen Gmbh | Verfahren zur Herstellung von Kohlenstoffmolekularsieben für die Gewinnung von Stickstoff aus Luft |
| US6527827B2 (en) | 1998-10-26 | 2003-03-04 | Andreas Noack | Thermomembrane method and device |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5507860A (en) * | 1989-11-14 | 1996-04-16 | Air Products And Chemicals, Inc. | Composite porous carbonaceous membranes |
| US5071820A (en) * | 1990-05-25 | 1991-12-10 | Atlanta Gas Light Company | Carbonaceous material with high micropore and low macropore volume and process for producing same |
| US5086033A (en) * | 1990-08-30 | 1992-02-04 | Air Products And Chemicals, Inc. | Use of helium and argon diluent gases in modification of carbon molecular sieves |
| US5164355A (en) * | 1991-01-23 | 1992-11-17 | Air Products And Chemicals, Inc. | High capacity coconut shell char for carbon molecular sieves |
| US5482915A (en) * | 1993-09-20 | 1996-01-09 | Air Products And Chemicals, Inc. | Transition metal salt impregnated carbon |
| US5447557A (en) * | 1994-03-23 | 1995-09-05 | Air Products And Chemicals, Inc. | Oxygen selective adsorbents |
| RU2116962C1 (ru) * | 1996-10-03 | 1998-08-10 | Владимир Дмитриевич Назаров | Способ получения активных углей |
| CN1239253C (zh) | 2001-08-29 | 2006-02-01 | 日本酸素株式会社 | 用于从氧气·氮气混合气体中分离氮气的吸附剂以及使用它的氮气制造方法 |
| US6991671B2 (en) | 2002-12-09 | 2006-01-31 | Advanced Technology Materials, Inc. | Rectangular parallelepiped fluid storage and dispensing vessel |
| US8002880B2 (en) | 2002-12-10 | 2011-08-23 | Advanced Technology Materials, Inc. | Gas storage and dispensing system with monolithic carbon adsorbent |
| US6743278B1 (en) | 2002-12-10 | 2004-06-01 | Advanced Technology Materials, Inc. | Gas storage and dispensing system with monolithic carbon adsorbent |
| US7494530B2 (en) | 2002-12-10 | 2009-02-24 | Advanced Technology Materials, Inc. | Gas storage and dispensing system with monolithic carbon adsorbent |
| GB2399775B (en) * | 2003-03-28 | 2005-07-27 | Council Scient Ind Res | Process for the preparation of a molecular sieve adsorbent for the size/shape selective separation of air |
| US7319082B2 (en) * | 2003-10-27 | 2008-01-15 | Council Of Scientific And Industrial Research | Process for the preparation of molecular sieve adsorbent for selective adsorption of oxygen from air |
| US8679231B2 (en) | 2011-01-19 | 2014-03-25 | Advanced Technology Materials, Inc. | PVDF pyrolyzate adsorbent and gas storage and dispensing system utilizing same |
| WO2013181295A1 (en) | 2012-05-29 | 2013-12-05 | Advanced Technology Materials, Inc. | Carbon adsorbent for hydrogen sulfide removal from gases containing same, and regeneration of adsorbent |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1364674A (en) * | 1971-04-23 | 1974-08-29 | Bergwerksverband Gmbh | Carbon-containing molecular sieves |
| US4015956A (en) * | 1971-04-23 | 1977-04-05 | Bergwerksverband Gmbh | Process and arrangement for the enrichment of gases |
| US3960769A (en) * | 1971-04-23 | 1976-06-01 | Bergwerksverband Gmbh | Carbon-containing molecular sieves |
| US3960522A (en) * | 1971-04-23 | 1976-06-01 | Bergwerksverband Gmbh | Carbon-containing molecular sieves |
| US3979330A (en) * | 1971-04-23 | 1976-09-07 | Bergwerksverband Gmbh | Carbon containing molecular sieves |
| US4083810A (en) * | 1974-01-29 | 1978-04-11 | Varta Batterie Aktiengesellschaft | Processing of catalyst powder |
| BE823966A (fr) * | 1974-01-29 | 1975-04-16 | Procede pour l'execution de reactions entre des substances pulverulentes et des substances gazeuses | |
| JPS5324190B2 (enExample) * | 1974-03-05 | 1978-07-19 | ||
| DE3141906A1 (de) * | 1981-10-08 | 1983-04-21 | Degussa Ag, 6000 Frankfurt | Verfahren und vorrichtung zur durchfuehrung von gas/feststoff-reaktionen, insbesondere zum aktivieren und reaktivieren von aktivkohle |
| US4594163A (en) * | 1982-09-07 | 1986-06-10 | Calgon Carbon Corporation | Use of carbon molecular sieves for separating gas or liquid mixtures |
| US4540678A (en) * | 1982-09-07 | 1985-09-10 | Calgon Carbon Corporation | Carbon molecular sieves and a process for their preparation and use |
| ES8606827A1 (es) * | 1982-09-07 | 1985-10-01 | Calgon Carbon Corp | Un procedimiento para la manufactura continua de tamices moleculares de carbono |
| EP0146909A3 (en) * | 1983-12-21 | 1986-05-28 | Air Products And Chemicals, Inc. | Method of removing oxygen from a gas mixture containing oxygen and argon |
-
1986
- 1986-05-31 DE DE3618426A patent/DE3618426C1/de not_active Expired
-
1987
- 1987-05-22 WO PCT/EP1987/000268 patent/WO1987007249A1/de not_active Ceased
- 1987-05-22 DE DE8787903311T patent/DE3769648D1/de not_active Expired - Fee Related
- 1987-05-22 US US07/272,694 patent/US4880765A/en not_active Expired - Lifetime
- 1987-05-22 JP JP62503239A patent/JPH01502743A/ja active Granted
- 1987-05-22 EP EP87903311A patent/EP0308409B1/de not_active Expired - Lifetime
Non-Patent Citations (1)
| Title |
|---|
| NICHTS-ERMITTELT * |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1991004788A1 (de) * | 1989-10-06 | 1991-04-18 | Bergwerksverband Gmbh | Kohlenstoff-molekularsieb zur zerlegung von luft in stickstoff und sauerstoff durch druckwechseltechnik |
| EP0474106A3 (en) * | 1990-08-30 | 1992-04-15 | Air Products And Chemicals, Inc. | Modified carbon molecular sieves for gas separation |
| EP0481218A1 (en) * | 1990-09-14 | 1992-04-22 | Air Products And Chemicals, Inc. | A process for making modified carbon molecular sieve adsorbents |
| DE4031580A1 (de) * | 1990-10-05 | 1992-04-09 | Bergwerksverband Gmbh | Verfahren zur herstellung von kohlenstoffmolekularsieben |
| DE4031578A1 (de) * | 1990-10-05 | 1992-04-09 | Bergwerksverband Gmbh | Verfahren zur herstellung von kohlenstoffmolekularsieben |
| WO1992005868A1 (de) * | 1990-10-05 | 1992-04-16 | Bergwerksverband Gmbh | Verfahren zur herstellung von kohlenstoffmolekularsieben |
| DE4132971A1 (de) * | 1991-10-04 | 1993-04-08 | Bergwerksverband Gmbh | Verfahren zur herstellung von kohlenstoffmolekularsieben |
| US5498589A (en) * | 1991-10-04 | 1996-03-12 | Bergwerksverband Gmbh | Process for the production of carbon molecular sieves |
| FR2702392A1 (fr) * | 1993-03-12 | 1994-09-16 | Inst Francais Du Petrole | Procédé et dispositif de régénération d'absorbant régénérables. |
| US6527827B2 (en) | 1998-10-26 | 2003-03-04 | Andreas Noack | Thermomembrane method and device |
| DE10127768A1 (de) * | 2001-06-07 | 2002-12-19 | Carbo Tech Aktivkohlen Gmbh | Verfahren zur Herstellung von Kohlenstoffmolekularsieben für die Gewinnung von Stickstoff aus Luft |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0549605B2 (enExample) | 1993-07-26 |
| WO1987007249A1 (fr) | 1987-12-03 |
| US4880765A (en) | 1989-11-14 |
| EP0308409B1 (de) | 1991-04-24 |
| DE3769648D1 (de) | 1991-05-29 |
| EP0308409A1 (de) | 1989-03-29 |
| JPH01502743A (ja) | 1989-09-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8100 | Publication of the examined application without publication of unexamined application | ||
| D1 | Grant (no unexamined application published) patent law 81 | ||
| 8364 | No opposition during term of opposition | ||
| 8330 | Complete disclaimer |