DE3600415A1 - Verfahren und vorrichtung zur vorbehandlung von zum galvanisieren vorgesehenem aluminiummaterial - Google Patents
Verfahren und vorrichtung zur vorbehandlung von zum galvanisieren vorgesehenem aluminiummaterialInfo
- Publication number
- DE3600415A1 DE3600415A1 DE19863600415 DE3600415A DE3600415A1 DE 3600415 A1 DE3600415 A1 DE 3600415A1 DE 19863600415 DE19863600415 DE 19863600415 DE 3600415 A DE3600415 A DE 3600415A DE 3600415 A1 DE3600415 A1 DE 3600415A1
- Authority
- DE
- Germany
- Prior art keywords
- aluminum
- alkaline solution
- components
- containers
- cleaning
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 48
- 229910052782 aluminium Inorganic materials 0.000 title claims abstract description 40
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims abstract description 40
- 239000004411 aluminium Substances 0.000 title abstract 4
- 238000009713 electroplating Methods 0.000 title description 4
- 239000000463 material Substances 0.000 title description 4
- 239000012670 alkaline solution Substances 0.000 claims abstract description 25
- 238000004140 cleaning Methods 0.000 claims abstract description 19
- 239000000203 mixture Substances 0.000 claims abstract description 12
- 239000000243 solution Substances 0.000 claims abstract description 12
- 238000002604 ultrasonography Methods 0.000 claims abstract description 10
- 229910000838 Al alloy Inorganic materials 0.000 claims abstract description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000011260 aqueous acid Substances 0.000 claims abstract description 6
- 239000003112 inhibitor Substances 0.000 claims abstract description 5
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 3
- 150000002222 fluorine compounds Chemical class 0.000 claims abstract description 3
- 239000004094 surface-active agent Substances 0.000 claims abstract description 3
- 230000008569 process Effects 0.000 claims description 15
- 229910045601 alloy Inorganic materials 0.000 claims description 13
- 239000000956 alloy Substances 0.000 claims description 13
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 239000012528 membrane Substances 0.000 claims description 6
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 4
- 244000060011 Cocos nucifera Species 0.000 claims description 4
- 150000001412 amines Chemical class 0.000 claims description 4
- 229910021538 borax Inorganic materials 0.000 claims description 4
- XPPKVPWEQAFLFU-UHFFFAOYSA-J diphosphate(4-) Chemical compound [O-]P([O-])(=O)OP([O-])([O-])=O XPPKVPWEQAFLFU-UHFFFAOYSA-J 0.000 claims description 4
- 235000011180 diphosphates Nutrition 0.000 claims description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 4
- 239000004328 sodium tetraborate Substances 0.000 claims description 4
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 4
- 230000004913 activation Effects 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- 238000005530 etching Methods 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 claims description 2
- 238000009835 boiling Methods 0.000 claims description 2
- 230000008030 elimination Effects 0.000 claims description 2
- 238000003379 elimination reaction Methods 0.000 claims description 2
- 239000002736 nonionic surfactant Substances 0.000 claims description 2
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 claims description 2
- 150000007524 organic acids Chemical class 0.000 claims description 2
- 235000005985 organic acids Nutrition 0.000 claims description 2
- 238000005554 pickling Methods 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 2
- 230000003213 activating effect Effects 0.000 claims 1
- 239000002244 precipitate Substances 0.000 claims 1
- 238000011109 contamination Methods 0.000 abstract description 5
- 239000003513 alkali Substances 0.000 abstract 1
- 239000002253 acid Substances 0.000 description 12
- 239000000356 contaminant Substances 0.000 description 7
- 150000007513 acids Chemical class 0.000 description 6
- 238000000576 coating method Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical class F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000005246 galvanizing Methods 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000005352 clarification Methods 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 238000005238 degreasing Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000002203 pretreatment Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000004506 ultrasonic cleaning Methods 0.000 description 2
- 238000011144 upstream manufacturing Methods 0.000 description 2
- YZCKVEUIGOORGS-OUBTZVSYSA-N Deuterium Chemical compound [2H] YZCKVEUIGOORGS-OUBTZVSYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- LDDQLRUQCUTJBB-UHFFFAOYSA-O azanium;hydrofluoride Chemical compound [NH4+].F LDDQLRUQCUTJBB-UHFFFAOYSA-O 0.000 description 1
- 238000009924 canning Methods 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 229940071182 stannate Drugs 0.000 description 1
- 125000005402 stannate group Chemical group 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/14—Cleaning or pickling metallic material with solutions or molten salts with alkaline solutions
- C23G1/22—Light metals
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/78—Pretreatment of the material to be coated
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
- C25D5/34—Pretreatment of metallic surfaces to be electroplated
- C25D5/42—Pretreatment of metallic surfaces to be electroplated of light metals
- C25D5/44—Aluminium
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Electrochemistry (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863600415 DE3600415A1 (de) | 1986-01-09 | 1986-01-09 | Verfahren und vorrichtung zur vorbehandlung von zum galvanisieren vorgesehenem aluminiummaterial |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863600415 DE3600415A1 (de) | 1986-01-09 | 1986-01-09 | Verfahren und vorrichtung zur vorbehandlung von zum galvanisieren vorgesehenem aluminiummaterial |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3600415A1 true DE3600415A1 (de) | 1987-07-16 |
| DE3600415C2 DE3600415C2 (enrdf_load_stackoverflow) | 1989-03-23 |
Family
ID=6291567
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19863600415 Granted DE3600415A1 (de) | 1986-01-09 | 1986-01-09 | Verfahren und vorrichtung zur vorbehandlung von zum galvanisieren vorgesehenem aluminiummaterial |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE3600415A1 (enrdf_load_stackoverflow) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0282921A1 (de) * | 1987-03-19 | 1988-09-21 | Henkel Kommanditgesellschaft auf Aktien | Flüssige, phosphatfreie Einphasen-Entfettungsmittel für Aluminiumoberflächen |
| DE3937442A1 (de) * | 1989-11-10 | 1991-05-16 | Nokia Unterhaltungselektronik | Verfahren zum bereichsweisen entfernen von schichten von einem substrat |
| WO2003023088A1 (en) * | 2001-09-07 | 2003-03-20 | The Board Of Regents For Oklahoma State University | Removal of organically modified silicate films from metal substrates |
| WO2004054699A3 (de) * | 2002-12-18 | 2004-09-23 | Siemens Ag | Verfahren zur verbesserung der wechselwirkung zwischen einem medium und einem bauteil |
| WO2006122852A1 (en) * | 2005-05-19 | 2006-11-23 | Hydro Aluminium Deutschland Gmbh | Conditioning of a litho strip |
| WO2007056992A1 (de) * | 2005-11-21 | 2007-05-24 | Eric Blauenstein | Verfahren und mittel zur elektrolytischen reinigung und entzunderung eines metallischen werkstücks |
| WO2007141300A1 (en) * | 2006-06-06 | 2007-12-13 | Hydro Aluminium Deutschland Gmbh | Method for cleaning an aluminium workpiece |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD240966A1 (de) * | 1985-09-11 | 1986-11-19 | Kuehlautomat Veb | Schalldaempfer |
-
1986
- 1986-01-09 DE DE19863600415 patent/DE3600415A1/de active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD240966A1 (de) * | 1985-09-11 | 1986-11-19 | Kuehlautomat Veb | Schalldaempfer |
Non-Patent Citations (3)
| Title |
|---|
| DETTNER, ELZE: Handbuch der Galvano- technik, Bd. I, T. 2, 1964, S.1034/1035, Carl Hanser Verlag, München * |
| Galvanotechnik, 69, 1978, H. 1, S.24-34, Eugen G. Leuze Verlag, Saulgau * |
| Metalloberfläche, 32, 1978, H. 1, S.8-14, Carl Hanser Verlag, München * |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0282921A1 (de) * | 1987-03-19 | 1988-09-21 | Henkel Kommanditgesellschaft auf Aktien | Flüssige, phosphatfreie Einphasen-Entfettungsmittel für Aluminiumoberflächen |
| US4844744A (en) * | 1987-03-19 | 1989-07-04 | Henkel Kommanditgesellschaft Auf Aktien | Liquid, phosphate-free single phase degreasing compositions |
| DE3937442A1 (de) * | 1989-11-10 | 1991-05-16 | Nokia Unterhaltungselektronik | Verfahren zum bereichsweisen entfernen von schichten von einem substrat |
| WO2003023088A1 (en) * | 2001-09-07 | 2003-03-20 | The Board Of Regents For Oklahoma State University | Removal of organically modified silicate films from metal substrates |
| US6709707B2 (en) | 2001-09-07 | 2004-03-23 | The Board Of Regents For Oklahoma State University | Removal of Ormosil films from metal substrates |
| WO2004054699A3 (de) * | 2002-12-18 | 2004-09-23 | Siemens Ag | Verfahren zur verbesserung der wechselwirkung zwischen einem medium und einem bauteil |
| WO2006122852A1 (en) * | 2005-05-19 | 2006-11-23 | Hydro Aluminium Deutschland Gmbh | Conditioning of a litho strip |
| EP2460909A1 (en) * | 2005-05-19 | 2012-06-06 | Hydro Aluminium Deutschland GmbH | Conditioning of a litho strip |
| US8211622B2 (en) | 2005-05-19 | 2012-07-03 | Hydro Aluminium Deutschland Gmbh | Conditioning of a litho strip |
| US8632955B2 (en) | 2005-05-19 | 2014-01-21 | Hydro Aluminium Deutschland Gmbh | Conditioning a surface of an aluminium strip |
| WO2007056992A1 (de) * | 2005-11-21 | 2007-05-24 | Eric Blauenstein | Verfahren und mittel zur elektrolytischen reinigung und entzunderung eines metallischen werkstücks |
| WO2007141300A1 (en) * | 2006-06-06 | 2007-12-13 | Hydro Aluminium Deutschland Gmbh | Method for cleaning an aluminium workpiece |
| EP2468525A1 (en) * | 2006-06-06 | 2012-06-27 | Hydro Aluminium Rolled Products GmbH | Method for cleaning an aluminium workpiece |
| US8293021B2 (en) | 2006-06-06 | 2012-10-23 | Hydro Aluminium Deutschalnd GmbH | Instrument for cleaning an aluminum workpiece |
| US8449689B2 (en) | 2006-06-06 | 2013-05-28 | Hydro Aluminium Deutschland Gmbh | Instrument for cleaning an aluminum workpiece |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3600415C2 (enrdf_load_stackoverflow) | 1989-03-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: MAC DERMID CANNING GMBH, 40472 DUESSELDORF, DE |
|
| 8339 | Ceased/non-payment of the annual fee |