DE317755C - - Google Patents
Info
- Publication number
- DE317755C DE317755C DENDAT317755D DE317755DA DE317755C DE 317755 C DE317755 C DE 317755C DE NDAT317755 D DENDAT317755 D DE NDAT317755D DE 317755D A DE317755D A DE 317755DA DE 317755 C DE317755 C DE 317755C
- Authority
- DE
- Germany
- Prior art keywords
- naphthalene
- parts
- water
- weight
- percent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000000460 chlorine Substances 0.000 claims description 9
- UFWIBTONFRDIAS-UHFFFAOYSA-N naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 claims description 9
- 229910052801 chlorine Inorganic materials 0.000 claims description 7
- ZAMOUSCENKQFHK-UHFFFAOYSA-N chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 7
- GRYLNZFGIOXLOG-UHFFFAOYSA-N nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 6
- RJKGJBPXVHTNJL-UHFFFAOYSA-N 1-nitronaphthalene Chemical class C1=CC=C2C([N+](=O)[O-])=CC=CC2=C1 RJKGJBPXVHTNJL-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 2
- 239000011230 binding agent Substances 0.000 claims description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 10
- UHOVQNZJYSORNB-UHFFFAOYSA-N benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 10
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 10
- 238000002844 melting Methods 0.000 description 8
- 239000000126 substance Substances 0.000 description 7
- WMDWNYHVFMGYNB-UHFFFAOYSA-L [Cl-].[Cl-].C1=CC=CC2=CC=CC=C21 Chemical compound [Cl-].[Cl-].C1=CC=CC2=CC=CC=C21 WMDWNYHVFMGYNB-UHFFFAOYSA-L 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- DOUCHCULYHWMTQ-UHFFFAOYSA-J [Cl-].[Cl-].[Cl-].[Cl-].C1=CC=CC2=CC=CC=C12 Chemical compound [Cl-].[Cl-].[Cl-].[Cl-].C1=CC=CC2=CC=CC=C12 DOUCHCULYHWMTQ-UHFFFAOYSA-J 0.000 description 5
- 238000000354 decomposition reaction Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- UFYHMOUUBQRTOS-UHFFFAOYSA-N 1,4-dichloro-5-nitronaphthalene Chemical compound C1=CC(Cl)=C2C([N+](=O)[O-])=CC=CC2=C1Cl UFYHMOUUBQRTOS-UHFFFAOYSA-N 0.000 description 2
- JXGMSAJQMIINOP-UHFFFAOYSA-N 2,3-dichloro-1-nitronaphthalene Chemical compound C1=CC=C2C([N+](=O)[O-])=C(Cl)C(Cl)=CC2=C1 JXGMSAJQMIINOP-UHFFFAOYSA-N 0.000 description 2
- UYEFXKQQSBRCGB-UHFFFAOYSA-N 2-chloro-1-nitronaphthalene Chemical compound C1=CC=C2C([N+](=O)[O-])=C(Cl)C=CC2=C1 UYEFXKQQSBRCGB-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M NaHCO3 Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 229910052736 halogen Inorganic materials 0.000 description 2
- 150000002367 halogens Chemical class 0.000 description 2
- CPELXLSAUQHCOX-UHFFFAOYSA-N hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- SBABEHDRJFHMEU-UHFFFAOYSA-N 2-bromo-1-nitronaphthalene Chemical compound C1=CC=C2C([N+](=O)[O-])=C(Br)C=CC2=C1 SBABEHDRJFHMEU-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L Calcium hydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- GNMTXWCTSSOHHL-UHFFFAOYSA-N N,N-dichloronaphthalen-1-amine Chemical compound C1=CC=C2C(N(Cl)Cl)=CC=CC2=C1 GNMTXWCTSSOHHL-UHFFFAOYSA-N 0.000 description 1
- VMICULCQFMPUQV-UHFFFAOYSA-N N-chloronaphthalen-1-amine Chemical compound C1=CC=C2C(NCl)=CC=CC2=C1 VMICULCQFMPUQV-UHFFFAOYSA-N 0.000 description 1
- XMVJITFPVVRMHC-UHFFFAOYSA-N Roxarsone Chemical group OC1=CC=C([As](O)(O)=O)C=C1[N+]([O-])=O XMVJITFPVVRMHC-UHFFFAOYSA-N 0.000 description 1
- HPGGPRDJHPYFRM-UHFFFAOYSA-J Tin(IV) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical compound BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910000042 hydrogen bromide Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- -1 nitronaphthalene dichloride Chemical compound 0.000 description 1
- 150000003021 phthalic acid derivatives Chemical class 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N tin hydride Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE317755C true DE317755C (US07601507-20091013-C00023.png) |
Family
ID=570391
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT317755D Active DE317755C (US07601507-20091013-C00023.png) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE317755C (US07601507-20091013-C00023.png) |
-
0
- DE DENDAT317755D patent/DE317755C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2313496C3 (de) | Verfahren zur Herstellung von m- und p- Phenylendiamin | |
| DE2837341A1 (de) | Verfahren zur herstellung von organischen mono- und polyisocyanaten durch thermische spaltung der hydrochloride trisubstituierter harnstoffe | |
| CH626039A5 (US07601507-20091013-C00023.png) | ||
| DE1943404A1 (de) | Adamantanylalkylamin-Derivate und Verfahren zu ihrer Herstellung | |
| DE317755C (US07601507-20091013-C00023.png) | ||
| EP0220135B1 (de) | Verfahren zur Herstellung von Chloranil | |
| DE1900133B2 (de) | Verfahren zur herstellung von 2- (morpholinothio)-benzothiazol | |
| CH634042A5 (de) | Verfahren zur herstellung von cyanopinakolon. | |
| DE1123663B (de) | Verfahren zur Herstellung von hochchlorierten Arylsulfiden | |
| CH413814A (de) | Verfahren zur Herstellung von 2,5-Dichlor-, 2,5-Dibrom- und 2,5-Dijod-terephthalsäure | |
| EP0077537B1 (de) | Verfahren zur Herstellung von 6-Chlor-3-toluidin-4-sulfonsäure | |
| CH405271A (de) | Verfahren zur Herstellung von 2-Chlor-3-brompropen und Propargylbromid | |
| DE1232944B (de) | Verfahren zur Herstellung von meso-2, 3-Dibrombernsteinsaeure | |
| CH681982A5 (US07601507-20091013-C00023.png) | ||
| DE2502411C2 (de) | Verfahren zur herstellung von bis-n-chloramiden gesaettigter aliphatischer dicarbonsaeuren | |
| DE1593389C3 (de) | Verfahren zur Herstellung von 4,5,6,7,8,8-Heptachlor-4,7-methano-3a, 4,7,7a-tetrahydroindan | |
| AT213390B (de) | Verfahren zur Herstellung von α-Monohalogen-ω-lactamen | |
| AT218510B (de) | Verfahren zur Herstellung von 2, 6-Dichlorbenzalchlorid oder 2, 6-Dichlorbenzaldehyd | |
| DE2117034A1 (de) | Verfahren zur Herstellung von 2,4,7 Tn mtrofluorenon | |
| AT315847B (de) | Verfahren zur herstellung von 7-chlor-1,3-dihydro-1-methyl-5-phenyl-2h-1,4-benzodiazepin-2-on | |
| DE2513952C2 (de) | Verfahren zur herstellung von monochlorbenzoesaeuren | |
| AT253488B (de) | Verfahren zur Herstellung von 2-Methyl-4-chlorphenoxyalkansäuren | |
| AT217041B (de) | Verfahren zur direkten Herstellung von Cyanurchlorid | |
| DE1913405A1 (de) | Verfahren zur Herstellung von Trifluorbrommethan und Tetrabrommethan | |
| DE1545690A1 (de) | Neues Verfahren zur Herstellung von Phthalazinen und Phthalazonen |
