DE2820704C2 - Verfahren zum Herstellen einer mit Wachs desensibilisierten Sprengstoffmasse - Google Patents
Verfahren zum Herstellen einer mit Wachs desensibilisierten SprengstoffmasseInfo
- Publication number
- DE2820704C2 DE2820704C2 DE2820704A DE2820704A DE2820704C2 DE 2820704 C2 DE2820704 C2 DE 2820704C2 DE 2820704 A DE2820704 A DE 2820704A DE 2820704 A DE2820704 A DE 2820704A DE 2820704 C2 DE2820704 C2 DE 2820704C2
- Authority
- DE
- Germany
- Prior art keywords
- wax
- explosive
- process according
- liquid medium
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002360 explosive Substances 0.000 title claims description 75
- 238000000034 method Methods 0.000 title claims description 32
- 230000008569 process Effects 0.000 title claims description 24
- 239000007788 liquid Substances 0.000 claims description 29
- 239000000203 mixture Substances 0.000 claims description 27
- 238000003756 stirring Methods 0.000 claims description 15
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 14
- 229910052782 aluminium Inorganic materials 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 238000000354 decomposition reaction Methods 0.000 claims description 10
- 238000002844 melting Methods 0.000 claims description 6
- 230000008018 melting Effects 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 239000000080 wetting agent Substances 0.000 claims description 5
- XTFIVUDBNACUBN-UHFFFAOYSA-N 1,3,5-trinitro-1,3,5-triazinane Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)C1 XTFIVUDBNACUBN-UHFFFAOYSA-N 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 3
- -1 fatty acid ester Chemical class 0.000 claims description 3
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 229930195729 fatty acid Natural products 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims 1
- 239000001993 wax Substances 0.000 description 89
- 239000002245 particle Substances 0.000 description 20
- 239000000463 material Substances 0.000 description 16
- 238000000576 coating method Methods 0.000 description 11
- 239000011248 coating agent Substances 0.000 description 9
- 238000009835 boiling Methods 0.000 description 8
- 239000000843 powder Substances 0.000 description 7
- 239000004411 aluminium Substances 0.000 description 6
- 238000000586 desensitisation Methods 0.000 description 5
- 230000035945 sensitivity Effects 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- BJXXCOMGRRCAGN-XPWSMXQVSA-N [2,2-bis(hydroxymethyl)-3-[(e)-octadec-9-enoyl]oxypropyl] (e)-octadec-9-enoate Chemical compound CCCCCCCC\C=C\CCCCCCCC(=O)OCC(CO)(CO)COC(=O)CCCCCCC\C=C\CCCCCCCC BJXXCOMGRRCAGN-XPWSMXQVSA-N 0.000 description 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000005474 detonation Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- CBCKQZAAMUWICA-UHFFFAOYSA-N 1,4-phenylenediamine Chemical compound NC1=CC=C(N)C=C1 CBCKQZAAMUWICA-UHFFFAOYSA-N 0.000 description 1
- IDCPFAYURAQKDZ-UHFFFAOYSA-N 1-nitroguanidine Chemical compound NC(=N)N[N+]([O-])=O IDCPFAYURAQKDZ-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 229940090898 Desensitizer Drugs 0.000 description 1
- TZRXHJWUDPFEEY-UHFFFAOYSA-N Pentaerythritol Tetranitrate Chemical compound [O-][N+](=O)OCC(CO[N+]([O-])=O)(CO[N+]([O-])=O)CO[N+]([O-])=O TZRXHJWUDPFEEY-UHFFFAOYSA-N 0.000 description 1
- 239000000026 Pentaerythritol tetranitrate Substances 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000001427 coherent effect Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000002223 garnet Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 229920001684 low density polyethylene Polymers 0.000 description 1
- 239000004702 low-density polyethylene Substances 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- UZGLIIJVICEWHF-UHFFFAOYSA-N octogen Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)CN([N+]([O-])=O)C1 UZGLIIJVICEWHF-UHFFFAOYSA-N 0.000 description 1
- 229960004321 pentaerithrityl tetranitrate Drugs 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000004525 petroleum distillation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000700 radioactive tracer Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B23/00—Compositions characterised by non-explosive or non-thermic constituents
- C06B23/005—Desensitisers, phlegmatisers
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0083—Treatment of solid structures, e.g. for coating or impregnating with a modifier
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Developing Agents For Electrophotography (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Lubricants (AREA)
- Battery Electrode And Active Subsutance (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB19868/77A GB1596402A (en) | 1977-05-11 | 1977-05-11 | Desensitizing explosives |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2820704A1 DE2820704A1 (de) | 1978-11-16 |
| DE2820704C2 true DE2820704C2 (de) | 1987-01-22 |
Family
ID=10136527
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2820704A Expired DE2820704C2 (de) | 1977-05-11 | 1978-05-11 | Verfahren zum Herstellen einer mit Wachs desensibilisierten Sprengstoffmasse |
Country Status (6)
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3711995A1 (de) * | 1987-04-09 | 1988-10-20 | Messerschmitt Boelkow Blohm | Verfahren zum phlegmatisieren von spreng- und treibstoffen |
| AT404831B (de) * | 1992-05-31 | 1999-03-25 | Meissner Gmbh & Co Kg Josef | Aufbereitung wasserhaltiger sprengstoffschlämme |
| DE102019205276A1 (de) * | 2019-04-11 | 2020-10-15 | Christof-Herbert Diener | Beschichtungsverfahren eines energetischen Materials und Beschichtungsanlage zur Beschichtung des energetischen Materials durch ein solches Beschichtungsverfahren |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1596403A (en) | 1977-05-11 | 1981-08-26 | Secr Defence | Desensitizing explosives |
| GB2129708B (en) * | 1982-11-05 | 1986-01-22 | Mini Ind Minerals | Method of inhibiting degeneration of direct reduced iron |
| ATE71927T1 (de) * | 1985-09-27 | 1992-02-15 | Nobel Kemi Ab | Verfahren zur phlegmatisierung von kristallinen sprengstoffen und sonstigen kristallinen explosiven substanzen sowie verfahren zur herstellung von kunststoffgebundenen sprengstoffmischungen und nach dem verfahren hergestellte substanzen. |
| SE452760B (sv) * | 1985-09-27 | 1987-12-14 | Nobel Kemi Ab | Sett att framstella blandsprengemnen av typen hexotonal och oktonal |
| DE3614173C1 (de) * | 1986-04-26 | 1989-03-02 | Dynamit Nobel Ag | Granuliertes,stabilisiertes alpha- und beta-Oktogen und Verfahren zur Herstellung von alpha-Oktogen |
| US6932878B1 (en) * | 1988-05-11 | 2005-08-23 | Bae Systems Plc | Explosive compositions |
| US5067995A (en) * | 1989-06-15 | 1991-11-26 | The United States Of America As Represented By The United States Department Of Energy | Method for enhancing stability of high explosives, for purposes of transport or storage, and the stabilized high explosives |
| US5049212A (en) * | 1991-03-27 | 1991-09-17 | The United States Of America As Represented By The Secretary Of The Navy | High energy explosive yield enhancer using microencapsulation |
| US5506366A (en) * | 1994-03-25 | 1996-04-09 | Aerojet General Corporation | Desensitization of cured energetic compositions in aqueous media |
| US5587042A (en) * | 1994-09-19 | 1996-12-24 | E. R. St. Denis & Sons Ltd. | Adhesive curing system and method for a hemming machine |
| US5523517A (en) * | 1995-02-09 | 1996-06-04 | Thiokol Corporation | Destruction of nitramines employing aqueous dispersions of metal powders |
| CA2180617A1 (en) * | 1995-07-07 | 1997-01-08 | Barton White | Explosive or fertiliser composition |
| JP2000510089A (ja) * | 1996-05-03 | 2000-08-08 | イーストマン ケミカル カンパニー | 爆発性調合物 |
| AU3069697A (en) * | 1996-05-03 | 1997-11-26 | Eastman Chemical Company | Explosive formulations |
| US5808234A (en) * | 1996-05-06 | 1998-09-15 | Eastman Chemical Company | Explosive formulations |
| AU3129097A (en) * | 1996-10-15 | 1998-05-11 | Eastman Chemical Company | Explosive formulations |
| GB2517119B (en) * | 2013-01-17 | 2021-03-03 | Utm Ltd | Explosive composition for use in telescopically expanding non-lethal training ammunition |
| EP3255028A1 (de) | 2016-06-08 | 2017-12-13 | Umwelt-Technik-Metallrecycling GmbH | Verfahren zur phlegmatisierung von explosivstoffen sowie dadurch erhältliche phlegmatisierte explosivstoffe |
| CN111620753B (zh) * | 2019-12-31 | 2023-12-01 | 湖北帅力化工有限公司 | 粉状乳化炸药矿物质添加剂表面改性方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2719153A (en) | 1955-09-27 | Free flowing cyclotmmethylene | ||
| GB574271A (en) * | 1942-09-09 | 1945-12-31 | Ernest Gordon Cockbain | Desensitization of explosives |
| GB776539A (en) * | 1946-01-30 | 1957-06-05 | Mini Of Supply | Preparation of explosive substances in thermoplastic or pourable form |
| US3348986A (en) | 1955-02-04 | 1967-10-24 | Charles W Sauer | Process of preparing plastic coated high explosive particles and articles |
| US2867647A (en) | 1957-02-04 | 1959-01-06 | Ici Ltd | Pentaerythritol tetranitrate |
| US3403061A (en) | 1960-02-01 | 1968-09-24 | Atomic Energy Commission Usa | Process of conditioning particulate materials for use in organic explosives |
| GB1089403A (en) | 1965-07-23 | 1967-11-01 | Ici Ltd | Explosive compositions |
| US3544360A (en) | 1968-04-18 | 1970-12-01 | Nat Defence Canada | Process for desensitizing solid explosive particles by coating with wax |
| US3740279A (en) | 1969-09-02 | 1973-06-19 | Hercules Inc | Ethylene copolymer composite propellant |
| FR2135534B1 (US07122547-20061017-C00032.png) | 1971-05-06 | 1973-06-29 | Wasagchemie Ag | |
| US4092187A (en) | 1976-08-18 | 1978-05-30 | The United States Of America As Represented By The Secretary Of The Army | Process for coating crystalline high explosives |
| US4097317A (en) | 1977-03-25 | 1978-06-27 | The United States Of America As Represented By The Secretary Of The Navy | Desensitizing agent for compositions containing crystalline high-energy nitrates or nitrites |
-
1977
- 1977-05-11 GB GB19868/77A patent/GB1596402A/en not_active Expired
-
1978
- 1978-05-09 NO NO781642A patent/NO145837C/no unknown
- 1978-05-10 CH CH510678A patent/CH634807A5/de not_active IP Right Cessation
- 1978-05-10 FR FR7813898A patent/FR2390405A1/fr active Granted
- 1978-05-11 DE DE2820704A patent/DE2820704C2/de not_active Expired
-
1980
- 1980-07-29 US US06/173,396 patent/US4430132A/en not_active Expired - Lifetime
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3711995A1 (de) * | 1987-04-09 | 1988-10-20 | Messerschmitt Boelkow Blohm | Verfahren zum phlegmatisieren von spreng- und treibstoffen |
| AT404831B (de) * | 1992-05-31 | 1999-03-25 | Meissner Gmbh & Co Kg Josef | Aufbereitung wasserhaltiger sprengstoffschlämme |
| DE102019205276A1 (de) * | 2019-04-11 | 2020-10-15 | Christof-Herbert Diener | Beschichtungsverfahren eines energetischen Materials und Beschichtungsanlage zur Beschichtung des energetischen Materials durch ein solches Beschichtungsverfahren |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2820704A1 (de) | 1978-11-16 |
| US4430132A (en) | 1984-02-07 |
| NO145837B (no) | 1982-03-01 |
| NO145837C (no) | 1982-06-09 |
| FR2390405A1 (fr) | 1978-12-08 |
| FR2390405B1 (US07122547-20061017-C00032.png) | 1983-10-21 |
| GB1596402A (en) | 1981-08-26 |
| NO781642L (no) | 1978-11-14 |
| CH634807A5 (de) | 1983-02-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: ROYAL ORDNANCE PLC, LONDON, GB |
|
| 8328 | Change in the person/name/address of the agent |
Free format text: BEETZ SEN., R., DIPL.-ING. BEETZ JUN., R., DIPL.-ING. DR.-ING. TIMPE, W., DR.-ING. SIEGFRIED, J., DIPL.-ING. SCHMITT-FUMIAN, W., PRIVATDOZENT, DIPL.-CHEM. DR.RER.NAT., PAT.-ANW., 8000 MUENCHEN |
|
| 8363 | Opposition against the patent | ||
| 8366 | Restricted maintained after opposition proceedings | ||
| 8305 | Restricted maintenance of patent after opposition | ||
| D4 | Patent maintained restricted |