DE2757477A1 - Verfahren zur reaktivierung von platingruppenmetall-katalysatoren - Google Patents

Verfahren zur reaktivierung von platingruppenmetall-katalysatoren

Info

Publication number
DE2757477A1
DE2757477A1 DE19772757477 DE2757477A DE2757477A1 DE 2757477 A1 DE2757477 A1 DE 2757477A1 DE 19772757477 DE19772757477 DE 19772757477 DE 2757477 A DE2757477 A DE 2757477A DE 2757477 A1 DE2757477 A1 DE 2757477A1
Authority
DE
Germany
Prior art keywords
catalyst
treatment
hours
sodium
inorganic base
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE19772757477
Other languages
German (de)
English (en)
Inventor
Yukihiko Morimoto
Katsumi Nakai
Toshikatu Sasaki
Kiaki Yamauchi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Osaka Gas Co Ltd
Original Assignee
Osaka Gas Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP15551276A external-priority patent/JPS5378990A/ja
Priority claimed from JP1563577A external-priority patent/JPS53100987A/ja
Priority claimed from JP4828577A external-priority patent/JPS53132492A/ja
Priority claimed from JP4828677A external-priority patent/JPS53132493A/ja
Priority claimed from JP4950777A external-priority patent/JPS53133596A/ja
Application filed by Osaka Gas Co Ltd filed Critical Osaka Gas Co Ltd
Publication of DE2757477A1 publication Critical patent/DE2757477A1/de
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/40—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts characterised by the catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/90—Regeneration or reactivation
    • B01J23/96—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the noble metals
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/386—Catalytic partial combustion
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C10G47/14—Inorganic carriers the catalyst containing platinum group metals or compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • B01J38/64—Liquid treating or treating in liquid phase, e.g. dissolved or suspended using alkaline material; using salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0233—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being a steam reforming step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/025—Processes for making hydrogen or synthesis gas containing a partial oxidation step
    • C01B2203/0261—Processes for making hydrogen or synthesis gas containing a partial oxidation step containing a catalytic partial oxidation step [CPO]
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1041—Composition of the catalyst
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1041—Composition of the catalyst
    • C01B2203/1047—Group VIII metal catalysts
    • C01B2203/1064—Platinum group metal catalysts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1041—Composition of the catalyst
    • C01B2203/1082—Composition of support materials
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205—Composition of the feed
    • C01B2203/1211—Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1217—Alcohols
    • C01B2203/1223—Methanol
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205—Composition of the feed
    • C01B2203/1211—Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1235—Hydrocarbons
    • C01B2203/1241—Natural gas or methane
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205—Composition of the feed
    • C01B2203/1211—Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1235—Hydrocarbons
    • C01B2203/1247—Higher hydrocarbons
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S502/00—Catalyst, solid sorbent, or support therefor: product or process of making
    • Y10S502/515—Specific contaminant removal
    • Y10S502/517—Sulfur or sulfur compound removal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE19772757477 1976-12-22 1977-12-22 Verfahren zur reaktivierung von platingruppenmetall-katalysatoren Withdrawn DE2757477A1 (de)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
JP15551276A JPS5378990A (en) 1976-12-22 1976-12-22 Catalyst regenerating method
JP1563577A JPS53100987A (en) 1977-02-15 1977-02-15 Caralyst regenerating method
JP4828577A JPS53132492A (en) 1977-04-25 1977-04-25 Catalyst regeneration method
JP4828677A JPS53132493A (en) 1977-04-25 1977-04-25 Catalyst regeveration method
JP4950777A JPS53133596A (en) 1977-04-27 1977-04-27 Catalyst regeneration method

Publications (1)

Publication Number Publication Date
DE2757477A1 true DE2757477A1 (de) 1978-07-06

Family

ID=27519731

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19772757477 Withdrawn DE2757477A1 (de) 1976-12-22 1977-12-22 Verfahren zur reaktivierung von platingruppenmetall-katalysatoren

Country Status (4)

Country Link
US (2) US4147660A (enExample)
DE (1) DE2757477A1 (enExample)
FR (1) FR2374954A1 (enExample)
GB (1) GB1579984A (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0048335A1 (de) * 1980-09-18 1982-03-31 Hoechst Aktiengesellschaft Verfahren zur Herstellung von Carbonsäurehalogeniden

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU910184A1 (ru) * 1979-06-15 1982-03-07 Предприятие П/Я Р-6913 Способ регенерации родийсодержащего катализатора деалкилировани алкилбензолов
US4417972A (en) * 1981-11-04 1983-11-29 Exxon Research And Engineering Co. Recovery of coal liquefaction catalysts
US4414140A (en) * 1981-12-23 1983-11-08 United Technologies Corporation Catalyst for steam reforming
US4422954A (en) * 1982-03-31 1983-12-27 Allied Corporation Method to restore the metal content of a noble metal hydrogenation catalyst
GB8411210D0 (en) * 1984-05-02 1984-06-06 British Petroleum Co Plc Conversion process
EP0204750A4 (en) * 1984-11-08 1987-12-02 Chevron Res REACTIVATION OF A DISABLED CATALYST.
US5321168A (en) * 1993-09-16 1994-06-14 Exxon Chemical Patents Inc. Activation of cobalt preformer catalyst for oxo process
US6339191B1 (en) * 1994-03-11 2002-01-15 Silicon Bandwidth Inc. Prefabricated semiconductor chip carrier
TW319771B (enExample) * 1994-04-05 1997-11-11 Mitsubishi Chem Corp
WO2000018508A1 (fr) * 1998-09-29 2000-04-06 Idemitsu Kosan Co., Ltd. Procede de regeneration d'un catalyseur d'hydrogenation
JP2000351606A (ja) * 1999-06-08 2000-12-19 Matsushita Electric Ind Co Ltd 燃料改質装置
US8007954B2 (en) * 2000-11-09 2011-08-30 The Trustees Of The University Of Pennsylvania Use of sulfur-containing fuels for direct oxidation fuel cells
JP2006510189A (ja) * 2002-12-16 2006-03-23 ザ・トラスティーズ・オブ・ザ・ユニバーシティ・オブ・ペンシルバニア 高性能セラミックアノード及びその製造方法
RU2339712C2 (ru) * 2006-11-23 2008-11-27 Федеральное государственное образовательное учреждение высшего профессионального образования "Сибирский федеральный университет " Способ извлечения палладия (ii) из отработанных катализаторов
JP5368883B2 (ja) * 2009-05-29 2013-12-18 住友化学株式会社 塩素製造用触媒の賦活方法および塩素の製造方法
EP2440490A1 (de) * 2009-06-10 2012-04-18 Basf Se Verfahren zur chlorwasserstoffoxidation an einem katalysator mit geringer oberflächenrauhigkeit
RU2442833C1 (ru) * 2010-10-12 2012-02-20 Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Московский государственный университет тонких химических технологий имени М.В. Ломоносова" (МИТХТ) Способ извлечения палладия (ii) из отработанных катализаторов
RU2488638C1 (ru) * 2011-12-01 2013-07-27 Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина" Способ извлечения платины из шлама, получаемого при растворении платиносодержащего чугуна в серной кислоте
RU2613970C2 (ru) 2012-02-20 2017-03-22 ДАУ ГЛОБАЛ ТЕКНОЛОДЖИЗ ЭлЭлСи Восстановленный катализатор дегидрирования, демонстрирующий замедленную потерю активности по сравнению со свежим катализатором
RU2493275C1 (ru) * 2012-06-29 2013-09-20 Леонид Асхатович Мазитов Способ переработки палладиевых отработанных катализаторов
RU2640350C1 (ru) * 2017-04-05 2017-12-28 Открытое акционерное общество "Электростальское научно-производственное объединение "Неорганика" (ОАО "ЭНПО "Неорганика") Способ регенерации отработанного алюмопалладиевого катализатора окисления оксида углерода
RU2663394C1 (ru) * 2017-12-13 2018-08-03 Открытое акционерное общество "Красноярский завод цветных металлов имени В.Н. Гулидова" Способ растворения концентрата благородных металлов

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US2752289A (en) * 1950-01-27 1956-06-26 Universal Oil Prod Co Conditioning catalysts employed in the reforming of hydrocarbons
FR1556524A (enExample) * 1966-06-10 1969-02-07 Nat Distillers Chem Corp

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US1980829A (en) * 1933-06-22 1934-11-13 Grasselli Chemical Co Purification and regeneration of platinum catalysts
US3374182A (en) * 1964-05-22 1968-03-19 Union Oil Co Caustic-treated zeolites
US3650983A (en) * 1969-12-23 1972-03-21 Nat Distillers Chem Corp Alkaline wash reactivation of palladium catalysts used in vinyl acetate synthesis
US3824193A (en) * 1972-03-30 1974-07-16 Eastman Kodak Co Alkaline reactivation of alumina supported palladium catalysts
JPS493758A (enExample) * 1972-05-04 1974-01-14
US3879311A (en) * 1973-04-26 1975-04-22 Nat Distillers Chem Corp Catalyst regeneration
US3901822A (en) * 1973-11-14 1975-08-26 Fmc Corp Process of regenerating a noble metal hydrogenation catalyst used in hydrogen peroxide production by the anthraquinone process
US3959382A (en) * 1974-11-26 1976-05-25 Allied Chemical Corporation Method for reactivating palladium catalysts
US4148750A (en) * 1977-01-10 1979-04-10 Exxon Research & Engineering Co. Redispersion of noble metals on supported catalysts

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2752289A (en) * 1950-01-27 1956-06-26 Universal Oil Prod Co Conditioning catalysts employed in the reforming of hydrocarbons
FR1556524A (enExample) * 1966-06-10 1969-02-07 Nat Distillers Chem Corp

Non-Patent Citations (9)

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Title
Chem.Abstr., 1974, Vol. 81, Nr. 20, 127337t *
Chem.Abstr., 1976, Vol. 84, Nr. 2, 9427m *
Chem.Abstr., 1976, Vol. 85, Nr. 6, 37674d *
Chem.Ztr.Bl., 1935, II, 1758 *
Chem.Ztr.Bl., 1957, S. 7830 *
Chem.Ztr.Bl., 1959, S. 1240 *
Chem.Ztr.Bl., 1963, S. 2199 *
Chem.Ztr.Bl., 1967, Nr. 32, 2580 *
Chem.Ztr.Bl., 1968, Nr. 14, 2584 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0048335A1 (de) * 1980-09-18 1982-03-31 Hoechst Aktiengesellschaft Verfahren zur Herstellung von Carbonsäurehalogeniden

Also Published As

Publication number Publication date
US4228033A (en) 1980-10-14
GB1579984A (en) 1980-11-26
FR2374954B1 (enExample) 1982-02-19
US4147660A (en) 1979-04-03
FR2374954A1 (fr) 1978-07-21

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