DE2517231C2 - - Google Patents
Info
- Publication number
- DE2517231C2 DE2517231C2 DE2517231A DE2517231A DE2517231C2 DE 2517231 C2 DE2517231 C2 DE 2517231C2 DE 2517231 A DE2517231 A DE 2517231A DE 2517231 A DE2517231 A DE 2517231A DE 2517231 C2 DE2517231 C2 DE 2517231C2
- Authority
- DE
- Germany
- Prior art keywords
- catalyst
- weight
- ratio
- fraction
- catalysts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003054 catalyst Substances 0.000 claims description 108
- 238000000034 method Methods 0.000 claims description 31
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 21
- 229930195733 hydrocarbon Natural products 0.000 claims description 20
- 150000002430 hydrocarbons Chemical class 0.000 claims description 20
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 14
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 14
- 229910052751 metal Inorganic materials 0.000 claims description 13
- 239000002184 metal Substances 0.000 claims description 12
- 239000004215 Carbon black (E152) Substances 0.000 claims description 11
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 11
- 229910052739 hydrogen Inorganic materials 0.000 claims description 11
- 239000001257 hydrogen Substances 0.000 claims description 11
- 238000005984 hydrogenation reaction Methods 0.000 claims description 11
- YBYIRNPNPLQARY-UHFFFAOYSA-N 1H-indene Chemical compound C1=CC=C2CC=CC2=C1 YBYIRNPNPLQARY-UHFFFAOYSA-N 0.000 claims description 10
- 150000002739 metals Chemical class 0.000 claims description 9
- 229930195734 saturated hydrocarbon Natural products 0.000 claims description 9
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 8
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 8
- 229910052794 bromium Inorganic materials 0.000 claims description 8
- 229910021529 ammonia Inorganic materials 0.000 claims description 7
- 229910052750 molybdenum Inorganic materials 0.000 claims description 7
- 229910052759 nickel Inorganic materials 0.000 claims description 7
- 238000004230 steam cracking Methods 0.000 claims description 7
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims description 6
- 229910052721 tungsten Inorganic materials 0.000 claims description 6
- 238000010521 absorption reaction Methods 0.000 claims description 5
- 239000010937 tungsten Substances 0.000 claims description 5
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 4
- 229910017052 cobalt Inorganic materials 0.000 claims description 4
- 239000010941 cobalt Substances 0.000 claims description 4
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- 239000011733 molybdenum Substances 0.000 claims description 4
- 238000006386 neutralization reaction Methods 0.000 claims description 3
- 210000003918 fraction a Anatomy 0.000 claims 1
- 230000003197 catalytic effect Effects 0.000 description 22
- 239000000047 product Substances 0.000 description 21
- 238000002474 experimental method Methods 0.000 description 16
- 238000012360 testing method Methods 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 10
- 239000000446 fuel Substances 0.000 description 5
- 229910000476 molybdenum oxide Inorganic materials 0.000 description 5
- 229910000480 nickel oxide Inorganic materials 0.000 description 5
- PQQKPALAQIIWST-UHFFFAOYSA-N oxomolybdenum Chemical compound [Mo]=O PQQKPALAQIIWST-UHFFFAOYSA-N 0.000 description 5
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 229910052717 sulfur Inorganic materials 0.000 description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- QGLKJKCYBOYXKC-UHFFFAOYSA-N nonaoxidotritungsten Chemical compound O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1 QGLKJKCYBOYXKC-UHFFFAOYSA-N 0.000 description 3
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 3
- 238000006116 polymerization reaction Methods 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- 229910001930 tungsten oxide Inorganic materials 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- 125000004429 atom Chemical group 0.000 description 2
- 150000001869 cobalt compounds Chemical class 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 229920001971 elastomer Polymers 0.000 description 2
- 230000002779 inactivation Effects 0.000 description 2
- 239000003350 kerosene Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000005078 molybdenum compound Substances 0.000 description 2
- 150000002752 molybdenum compounds Chemical class 0.000 description 2
- 150000002816 nickel compounds Chemical class 0.000 description 2
- 239000003348 petrochemical agent Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 238000002407 reforming Methods 0.000 description 2
- 150000003658 tungsten compounds Chemical class 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- FBAZCZFUGZHBMZ-UHFFFAOYSA-O [NH4+].[Ni].[O-][N+]([O-])=O Chemical compound [NH4+].[Ni].[O-][N+]([O-])=O FBAZCZFUGZHBMZ-UHFFFAOYSA-O 0.000 description 1
- -1 alkenyl aromatic compounds Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000001491 aromatic compounds Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 229910000428 cobalt oxide Inorganic materials 0.000 description 1
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 150000002469 indenes Chemical class 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 229910052976 metal sulfide Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- KBJMLQFLOWQJNF-UHFFFAOYSA-N nickel(ii) nitrate Chemical compound [Ni+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O KBJMLQFLOWQJNF-UHFFFAOYSA-N 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000004434 sulfur atom Chemical group 0.000 description 1
- 125000000101 thioether group Chemical group 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
- C10G45/44—Hydrogenation of the aromatic hydrocarbons
- C10G45/46—Hydrogenation of the aromatic hydrocarbons characterised by the catalyst used
- C10G45/48—Hydrogenation of the aromatic hydrocarbons characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof
- C10G45/50—Hydrogenation of the aromatic hydrocarbons characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof in combination with chromium, molybdenum or tungsten metal, or compounds thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/85—Chromium, molybdenum or tungsten
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G65/00—Treatment of hydrocarbon oils by two or more hydrotreatment processes only
- C10G65/02—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only
- C10G65/04—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only including only refining steps
- C10G65/08—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only including only refining steps at least one step being a hydrogenation of the aromatic hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7414536A FR2268860B1 (en, 2012) | 1974-04-24 | 1974-04-24 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2517231A1 DE2517231A1 (de) | 1975-11-13 |
| DE2517231C2 true DE2517231C2 (en, 2012) | 1987-05-21 |
Family
ID=9138153
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752517231 Granted DE2517231A1 (de) | 1974-04-24 | 1975-04-18 | Verfahren zur hydrierung von stark ungesaettigten schweren kohlenwasserstoff- fraktionen |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4019976A (en, 2012) |
| BE (1) | BE827893A (en, 2012) |
| CA (1) | CA1066725A (en, 2012) |
| DE (1) | DE2517231A1 (en, 2012) |
| FR (1) | FR2268860B1 (en, 2012) |
| GB (1) | GB1504951A (en, 2012) |
| IT (1) | IT1037615B (en, 2012) |
| NL (1) | NL7504827A (en, 2012) |
| PL (1) | PL93624B1 (en, 2012) |
| ZA (1) | ZA752661B (en, 2012) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2480773A1 (fr) * | 1980-04-21 | 1981-10-23 | Inst Francais Du Petrole | Procede de conversion d'huiles lourdes d'hydrocarbures, contenant des asphaltenes, en fractions plus legeres, comportant un recyclage des fractions lourdes non converties |
| FR2480774A1 (fr) * | 1980-04-21 | 1981-10-23 | Inst Francais Du Petrole | Procede de conversion d'huiles lourdes d'hydrocarbures, contenant des asphaltenes, en fractions plus legeres |
| DE3114990A1 (de) * | 1980-04-21 | 1982-02-04 | Institut Français du Pétrole, 92502 Rueil-Malmaison, Hauts-de-Seine | Verfahren zur umwandlung von asphaltenhaltigen schweren kohlenwasserstoffoelen in leichtere fraktionen |
| DE3232395A1 (de) * | 1982-08-31 | 1984-03-01 | Linde Ag, 6200 Wiesbaden | Verfahren zur herstellung von olefinen |
| FR2538814B1 (fr) * | 1982-12-30 | 1986-06-27 | Inst Francais Du Petrole | Procede de traitement d'une huile lourde ou d'une fraction d'huile lourde pour les convertir en fractions plus legeres |
| FR2538811A1 (fr) * | 1982-12-30 | 1984-07-06 | Inst Francais Du Petrole | Procede de traitement d'une huile lourde ou d'une fraction d'huile lourde pour les convertir en fractions plus legeres |
| US4849093A (en) * | 1987-02-02 | 1989-07-18 | Union Oil Company Of California | Catalytic aromatic saturation of hydrocarbons |
| US5068025A (en) * | 1990-06-27 | 1991-11-26 | Shell Oil Company | Aromatics saturation process for diesel boiling-range hydrocarbons |
| JP2958234B2 (ja) * | 1994-02-19 | 1999-10-06 | 株式会社コスモ総合研究所 | 重質炭化水素油の水素化処理方法 |
| US5841013A (en) * | 1994-05-17 | 1998-11-24 | Exxon Research And Engineering Company | Aromatics hydrogenation with a new class of metal oxides |
| US5780381A (en) * | 1994-12-15 | 1998-07-14 | Syncrude Technology Inc. | Cobalt/molybdenum/zirconium catalyst for Fischer-Tropsch synthesis |
| FR2734575B1 (fr) * | 1995-05-22 | 1997-08-22 | Total Raffinage Distribution | Carbureacteur et procede de preparation de ce carbureacteur |
| EP1120453A3 (en) * | 2000-01-25 | 2002-01-30 | Haldor Topsoe A/S | Process for reduction of content of sulphur compounds and poly-aromatic hydrocarbons in distillate fuels |
| US7816299B2 (en) * | 2003-11-10 | 2010-10-19 | Exxonmobil Research And Engineering Company | Hydrotreating catalyst system suitable for use in hydrotreating hydrocarbonaceous feedstreams |
| US20050113250A1 (en) * | 2003-11-10 | 2005-05-26 | Schleicher Gary P. | Hydrotreating catalyst system suitable for use in hydrotreating hydrocarbonaceous feedstreams |
| US20050109679A1 (en) * | 2003-11-10 | 2005-05-26 | Schleicher Gary P. | Process for making lube oil basestocks |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2459465A (en) * | 1945-05-11 | 1949-01-18 | Standard Oil Dev Co | Two-stage hydrogenation treatment for hydrocarbon oils |
| US2765617A (en) * | 1952-10-22 | 1956-10-09 | Monsanto Chemicals | Method of operating a turbojet engine |
| US2744052A (en) * | 1955-02-25 | 1956-05-01 | Shell Dev | Hydrogenation of hydrocarbon oils, tungsten, molybdenum, and nickel containing catalysts therefor and their preparation |
| GB940290A (en) * | 1961-04-28 | 1963-10-30 | Universal Oil Prod Co | Process for the hydrorefining of aromatic hydrocarbon distillates |
| US3313859A (en) * | 1964-10-19 | 1967-04-11 | Phillips Petroleum Co | Process for hydrogenating aromatic hydrocarbons |
| NL145595B (nl) * | 1964-11-19 | 1975-04-15 | Shell Int Research | Werkwijze ter verlaging van het aromaatgehalte van zwavelbevattende koolwaterstofoliedestillaten. |
| US3493493A (en) * | 1968-10-01 | 1970-02-03 | Gulf Research Development Co | Process for enhancing lubricating oils and a catalyst for use in the process |
| FR2087391A5 (en) * | 1970-05-15 | 1971-12-31 | Inst Francais Du Petrole | Prepn. of aromatics esp. BTX - from pyrolysis and steam-cracked naphthas |
| US3728250A (en) * | 1970-07-02 | 1973-04-17 | Union Oil Co | Integral hydrofining-hydrogenation process |
-
1974
- 1974-04-24 FR FR7414536A patent/FR2268860B1/fr not_active Expired
-
1975
- 1975-04-14 BE BE1006590A patent/BE827893A/xx not_active IP Right Cessation
- 1975-04-18 DE DE19752517231 patent/DE2517231A1/de active Granted
- 1975-04-21 US US05/569,788 patent/US4019976A/en not_active Expired - Lifetime
- 1975-04-23 PL PL1975179888A patent/PL93624B1/xx unknown
- 1975-04-23 NL NL7504827A patent/NL7504827A/xx not_active Application Discontinuation
- 1975-04-23 CA CA225,256A patent/CA1066725A/fr not_active Expired
- 1975-04-24 IT IT22715/75A patent/IT1037615B/it active
- 1975-04-24 GB GB17061/75A patent/GB1504951A/en not_active Expired
- 1975-04-24 ZA ZA00752661A patent/ZA752661B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL93624B1 (en, 2012) | 1977-06-30 |
| GB1504951A (en) | 1978-03-22 |
| ZA752661B (en) | 1976-04-28 |
| AU8044075A (en) | 1976-10-28 |
| US4019976A (en) | 1977-04-26 |
| FR2268860A1 (en, 2012) | 1975-11-21 |
| BE827893A (fr) | 1975-10-14 |
| IT1037615B (it) | 1979-11-20 |
| NL7504827A (nl) | 1975-10-28 |
| CA1066725A (fr) | 1979-11-20 |
| FR2268860B1 (en, 2012) | 1977-06-24 |
| DE2517231A1 (de) | 1975-11-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |