DE2516243A1 - Verfahren zur isolierung von krypton-xenon-konzentrat aus der luft - Google Patents
Verfahren zur isolierung von krypton-xenon-konzentrat aus der luftInfo
- Publication number
- DE2516243A1 DE2516243A1 DE19752516243 DE2516243A DE2516243A1 DE 2516243 A1 DE2516243 A1 DE 2516243A1 DE 19752516243 DE19752516243 DE 19752516243 DE 2516243 A DE2516243 A DE 2516243A DE 2516243 A1 DE2516243 A1 DE 2516243A1
- Authority
- DE
- Germany
- Prior art keywords
- krypton
- xenon
- air
- oxygen
- hydrocarbons
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 28
- 239000012141 concentrate Substances 0.000 title claims description 27
- PDEXVOWZLSWEJB-UHFFFAOYSA-N krypton xenon Chemical compound [Kr].[Xe] PDEXVOWZLSWEJB-UHFFFAOYSA-N 0.000 title claims description 18
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 56
- 229910052743 krypton Inorganic materials 0.000 claims description 53
- DNNSSWSSYDEUBZ-UHFFFAOYSA-N krypton atom Chemical compound [Kr] DNNSSWSSYDEUBZ-UHFFFAOYSA-N 0.000 claims description 53
- 229910052724 xenon Inorganic materials 0.000 claims description 43
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 claims description 43
- 239000003463 adsorbent Substances 0.000 claims description 33
- 229930195733 hydrocarbon Natural products 0.000 claims description 31
- 150000002430 hydrocarbons Chemical class 0.000 claims description 31
- 229910052760 oxygen Inorganic materials 0.000 claims description 31
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 30
- 239000001301 oxygen Substances 0.000 claims description 30
- 229910052757 nitrogen Inorganic materials 0.000 claims description 28
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 23
- 239000007789 gas Substances 0.000 claims description 19
- 238000003795 desorption Methods 0.000 claims description 14
- 238000001179 sorption measurement Methods 0.000 claims description 13
- 239000010457 zeolite Substances 0.000 claims description 5
- 239000000499 gel Substances 0.000 claims description 4
- 238000002955 isolation Methods 0.000 claims description 4
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 3
- 239000000741 silica gel Substances 0.000 description 15
- 229910002027 silica gel Inorganic materials 0.000 description 15
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical class O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 8
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 8
- 229910021536 Zeolite Inorganic materials 0.000 description 4
- 239000002360 explosive Substances 0.000 description 4
- 238000009413 insulation Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 238000009738 saturating Methods 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- -1 methane) Chemical class 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000007420 reactivation Effects 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04642—Recovering noble gases from air
- F25J3/04745—Krypton and/or Xenon
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04642—Recovering noble gases from air
- F25J3/04745—Krypton and/or Xenon
- F25J3/04751—Producing pure krypton and/or xenon recovered from a crude krypton/xenon mixture
- F25J3/04757—Producing pure krypton and/or xenon recovered from a crude krypton/xenon mixture using a hybrid system, e.g. using adsorption, permeation or catalytic reaction
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2205/00—Processes or apparatus using other separation and/or other processing means
- F25J2205/60—Processes or apparatus using other separation and/or other processing means using adsorption on solid adsorbents, e.g. by temperature-swing adsorption [TSA] at the hot or cold end
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2220/00—Processes or apparatus involving steps for the removal of impurities
- F25J2220/40—Separating high boiling, i.e. less volatile components from air, e.g. CO2, hydrocarbons
Landscapes
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Mechanical Engineering (AREA)
- Thermal Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Separation By Low-Temperature Treatments (AREA)
- Separation Of Gases By Adsorption (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU2015806 | 1974-04-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2516243A1 true DE2516243A1 (de) | 1975-10-30 |
Family
ID=20581883
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752516243 Pending DE2516243A1 (de) | 1974-04-26 | 1975-04-14 | Verfahren zur isolierung von krypton-xenon-konzentrat aus der luft |
Country Status (8)
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0096610A1 (en) * | 1982-05-24 | 1983-12-21 | Union Carbide Corporation | Air separation process for the production of krypton and xenon |
| US11796514B2 (en) * | 2018-01-24 | 2023-10-24 | Sri International | Apparatuses and methods involving extraction of heavy rare gases |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2948515C2 (de) * | 1979-12-01 | 1983-12-22 | Kernforschungszentrum Karlsruhe Gmbh, 7500 Karlsruhe | Verfahren zur Fixierung von radioaktiven Edelgasen |
| US4816041A (en) * | 1984-05-22 | 1989-03-28 | Kernforschungsanlage Julich Gesellschaft Mit Beschrankter Haftung | Process and installation for the adsorptive separation of krypton from a krypton nitrogen gas mixture |
| JPS6272504A (ja) * | 1985-09-27 | 1987-04-03 | Hitachi Ltd | 高純度窒素の製造方法 |
| JPS62297206A (ja) * | 1986-03-05 | 1987-12-24 | Kyodo Sanso Kk | キセノン製造方法 |
| JPS62266381A (ja) * | 1986-05-10 | 1987-11-19 | 共同酸素株式会社 | キセノン製造方法 |
| JPH0516187Y2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1987-08-06 | 1993-04-28 | ||
| JP2630350B2 (ja) * | 1987-08-20 | 1997-07-16 | 共同酸素株式会社 | キセノンの製造方法 |
| US4874592A (en) * | 1988-08-23 | 1989-10-17 | Kyodo Oxygen Co., Ltd. | Production process of xenon |
| TWI223608B (en) * | 2001-11-19 | 2004-11-11 | Air Prod & Chem | Process and adsorbent for the recovery of krypton and xenon from a gas or liquid stream |
| US6658894B2 (en) | 2001-11-19 | 2003-12-09 | Air Products And Chemicals, Inc. | Process and adsorbent for the recovery of krypton and xenon from a gas or liquid stream |
| US6694775B1 (en) | 2002-12-12 | 2004-02-24 | Air Products And Chemicals, Inc. | Process and apparatus for the recovery of krypton and/or xenon |
| US7285154B2 (en) * | 2004-11-24 | 2007-10-23 | Air Products And Chemicals, Inc. | Xenon recovery system |
| US7381244B2 (en) * | 2005-08-03 | 2008-06-03 | Air Products And Chemicals, Inc. | Apparatus and process for air cleaning |
| DE102005037576A1 (de) * | 2005-08-09 | 2007-02-15 | Linde Ag | Verfahren und Vorrichtung zur Gewinnung von Krypton und/oder Xenon |
| EP2476645B1 (en) * | 2009-09-09 | 2018-10-10 | Panasonic Corporation | Xenon adsorption device |
| JP2011057491A (ja) * | 2009-09-09 | 2011-03-24 | Panasonic Corp | ガス回収方法 |
| US10295255B2 (en) | 2016-08-23 | 2019-05-21 | Praxair Technology, Inc. | Cryogenic adsorption process for xenon recovery |
| US11650010B2 (en) | 2018-01-11 | 2023-05-16 | Praxair Technology, Inc. | Adsorptive xenon recovery process from a gas or liquid stream at cryogenic temperature |
| ES2972484T3 (es) | 2018-05-08 | 2024-06-13 | Curium Us Llc | Sistemas y métodos para la producción de xenón-133 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2793507A (en) * | 1950-04-28 | 1957-05-28 | Amoco Chemicals Corp | Recovery of krypton and xenon |
| US3890121A (en) * | 1974-02-19 | 1975-06-17 | Us Energy | Noble gas absorption process |
-
1975
- 1975-03-18 US US05/559,410 patent/US3971640A/en not_active Expired - Lifetime
- 1975-03-27 GB GB1283075A patent/GB1473276A/en not_active Expired
- 1975-04-03 IT IT21980/75A patent/IT1044280B/it active
- 1975-04-08 JP JP50041940A patent/JPS51117997A/ja active Granted
- 1975-04-14 DE DE19752516243 patent/DE2516243A1/de active Pending
- 1975-04-17 FR FR7511967A patent/FR2269045B1/fr not_active Expired
- 1975-04-23 CS CS7500002812A patent/CS184070B1/cs unknown
- 1975-04-24 DD DD185675A patent/DD119463A1/xx unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0096610A1 (en) * | 1982-05-24 | 1983-12-21 | Union Carbide Corporation | Air separation process for the production of krypton and xenon |
| US11796514B2 (en) * | 2018-01-24 | 2023-10-24 | Sri International | Apparatuses and methods involving extraction of heavy rare gases |
Also Published As
| Publication number | Publication date |
|---|---|
| IT1044280B (it) | 1980-03-20 |
| GB1473276A (en) | 1977-05-11 |
| FR2269045A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1975-11-21 |
| JPS51117997A (en) | 1976-10-16 |
| FR2269045B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1977-04-15 |
| JPS5428314B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1979-09-14 |
| DD119463A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1976-04-20 |
| CS184070B1 (en) | 1978-07-31 |
| US3971640A (en) | 1976-07-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHW | Rejection |