DE2420775C3 - Verfahren zur Herstellung von Mangan (Ill)acetylacetonat - Google Patents
Verfahren zur Herstellung von Mangan (Ill)acetylacetonatInfo
- Publication number
- DE2420775C3 DE2420775C3 DE2420775A DE2420775A DE2420775C3 DE 2420775 C3 DE2420775 C3 DE 2420775C3 DE 2420775 A DE2420775 A DE 2420775A DE 2420775 A DE2420775 A DE 2420775A DE 2420775 C3 DE2420775 C3 DE 2420775C3
- Authority
- DE
- Germany
- Prior art keywords
- manganese
- acetylacetonate
- iii
- acetylacetone
- potassium permanganate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 12
- RDMHXWZYVFGYSF-LNTINUHCSA-N (z)-4-hydroxypent-3-en-2-one;manganese Chemical compound [Mn].C\C(O)=C\C(C)=O.C\C(O)=C\C(C)=O.C\C(O)=C\C(C)=O RDMHXWZYVFGYSF-LNTINUHCSA-N 0.000 title claims description 8
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 claims description 26
- 239000012286 potassium permanganate Substances 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 5
- POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 claims description 3
- MMIPFLVOWGHZQD-UHFFFAOYSA-N manganese(3+) Chemical compound [Mn+3] MMIPFLVOWGHZQD-UHFFFAOYSA-N 0.000 claims description 2
- 238000003756 stirring Methods 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 description 2
- 239000011572 manganese Substances 0.000 description 2
- JHWIEAWILPSRMU-UHFFFAOYSA-N 2-methyl-3-pyrimidin-4-ylpropanoic acid Chemical compound OC(=O)C(C)CC1=CC=NC=N1 JHWIEAWILPSRMU-UHFFFAOYSA-N 0.000 description 1
- 241000210648 Luciobarbus esocinus Species 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- WAEMQWOKJMHJLA-UHFFFAOYSA-N Manganese(2+) Chemical class [Mn+2] WAEMQWOKJMHJLA-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007334 copolymerization reaction Methods 0.000 description 1
- -1 cyclic imides Chemical class 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 150000003951 lactams Chemical class 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 150000003673 urethanes Chemical class 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/16—Catalysts
- C08G18/22—Catalysts containing metal compounds
- C08G18/222—Catalysts containing metal compounds metal compounds not provided for in groups C08G18/225 - C08G18/26
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/77—Preparation of chelates of aldehydes or ketones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F13/00—Compounds containing elements of Groups 7 or 17 of the Periodic Table
- C07F13/005—Compounds without a metal-carbon linkage
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2420775A DE2420775C3 (de) | 1974-04-29 | 1974-04-29 | Verfahren zur Herstellung von Mangan (Ill)acetylacetonat |
| NL7503149A NL7503149A (nl) | 1974-04-29 | 1975-03-17 | Werkwijze voor de bereiding van mangaan(iii)- acetylacetonaat. |
| GB1410075A GB1437773A (en) | 1974-04-29 | 1975-04-07 | Manufacture of manganese iii acetylacetonate |
| IT49229/75A IT1035408B (it) | 1974-04-29 | 1975-04-22 | Procedimento per la produzione di acetilacetonato di manganese |
| FR7513180A FR2268777B1 (enExample) | 1974-04-29 | 1975-04-28 | |
| BE155849A BE828474A (fr) | 1974-04-29 | 1975-04-28 | Procede de preparation d'acetylacetonate de manganese (iii) |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2420775A DE2420775C3 (de) | 1974-04-29 | 1974-04-29 | Verfahren zur Herstellung von Mangan (Ill)acetylacetonat |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2420775A1 DE2420775A1 (de) | 1975-11-06 |
| DE2420775B2 DE2420775B2 (de) | 1979-05-17 |
| DE2420775C3 true DE2420775C3 (de) | 1980-01-31 |
Family
ID=5914278
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2420775A Expired DE2420775C3 (de) | 1974-04-29 | 1974-04-29 | Verfahren zur Herstellung von Mangan (Ill)acetylacetonat |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE828474A (enExample) |
| DE (1) | DE2420775C3 (enExample) |
| FR (1) | FR2268777B1 (enExample) |
| GB (1) | GB1437773A (enExample) |
| IT (1) | IT1035408B (enExample) |
| NL (1) | NL7503149A (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2002368493A1 (en) * | 2002-12-23 | 2004-07-14 | Council Of Scientific And Industrial Research | Process for the preparation of metal acetylacetonates |
| FR3081868B1 (fr) * | 2018-06-05 | 2020-11-06 | Michelin & Cie | Procede de preparation de l'acetylacetonate d'un element chimique hydrate ou anhydre |
-
1974
- 1974-04-29 DE DE2420775A patent/DE2420775C3/de not_active Expired
-
1975
- 1975-03-17 NL NL7503149A patent/NL7503149A/xx not_active Application Discontinuation
- 1975-04-07 GB GB1410075A patent/GB1437773A/en not_active Expired
- 1975-04-22 IT IT49229/75A patent/IT1035408B/it active
- 1975-04-28 FR FR7513180A patent/FR2268777B1/fr not_active Expired
- 1975-04-28 BE BE155849A patent/BE828474A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| GB1437773A (en) | 1976-06-03 |
| DE2420775B2 (de) | 1979-05-17 |
| IT1035408B (it) | 1979-10-20 |
| FR2268777A1 (enExample) | 1975-11-21 |
| NL7503149A (nl) | 1975-10-31 |
| BE828474A (fr) | 1975-10-28 |
| FR2268777B1 (enExample) | 1977-04-15 |
| DE2420775A1 (de) | 1975-11-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |