DE2410474A1 - Herstellung von polyamiden durch kontinuierliche polymerisation - Google Patents

Herstellung von polyamiden durch kontinuierliche polymerisation

Info

Publication number
DE2410474A1
DE2410474A1 DE2410474A DE2410474A DE2410474A1 DE 2410474 A1 DE2410474 A1 DE 2410474A1 DE 2410474 A DE2410474 A DE 2410474A DE 2410474 A DE2410474 A DE 2410474A DE 2410474 A1 DE2410474 A1 DE 2410474A1
Authority
DE
Germany
Prior art keywords
separator
prepolymer
polyamide
reaction zone
heat exchanger
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DE2410474A
Other languages
German (de)
English (en)
Other versions
DE2410474C2 (US07902200-20110308-C00004.png
Inventor
Iqbalsingh Jaswal
Kalev Pugi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DuPont Canada Inc
Original Assignee
DuPont Canada Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DuPont Canada Inc filed Critical DuPont Canada Inc
Publication of DE2410474A1 publication Critical patent/DE2410474A1/de
Application granted granted Critical
Publication of DE2410474C2 publication Critical patent/DE2410474C2/de
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/04—Preparatory processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/322—Reboiler specifications
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/2435—Loop-type reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00083—Coils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
    • B01J2219/0011—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling involving reactant liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/002—Methods
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/80—Component parts, details or accessories; Auxiliary operations
    • B29B7/82—Heating or cooling
    • B29B7/826—Apparatus therefor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyamides (AREA)
DE2410474A 1973-03-05 1974-03-05 Herstellung von polyamiden durch kontinuierliche polymerisation Granted DE2410474A1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CA165,282A CA1015894A (en) 1973-03-05 1973-03-05 Preparation of polyamides by continuous polymerization

Publications (2)

Publication Number Publication Date
DE2410474A1 true DE2410474A1 (de) 1974-09-19
DE2410474C2 DE2410474C2 (US07902200-20110308-C00004.png) 1987-10-01

Family

ID=4096001

Family Applications (1)

Application Number Title Priority Date Filing Date
DE2410474A Granted DE2410474A1 (de) 1973-03-05 1974-03-05 Herstellung von polyamiden durch kontinuierliche polymerisation

Country Status (7)

Country Link
US (1) US3900450A (US07902200-20110308-C00004.png)
JP (1) JPS5646487B2 (US07902200-20110308-C00004.png)
CA (1) CA1015894A (US07902200-20110308-C00004.png)
DE (1) DE2410474A1 (US07902200-20110308-C00004.png)
FR (1) FR2220554B1 (US07902200-20110308-C00004.png)
GB (1) GB1453485A (US07902200-20110308-C00004.png)
IT (1) IT1011020B (US07902200-20110308-C00004.png)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996033234A1 (de) * 1995-04-15 1996-10-24 Basf Aktiengesellschaft Verfahren zur herstellung eines polyamids auf der basis einer dicarbonsäure und eines diamins
WO2003068359A2 (de) * 2002-02-15 2003-08-21 Basf Aktiengesellschaft Reaktionskolonne in spezieller kombination mit naturumlaufverdampfer

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5388093A (en) * 1977-01-14 1978-08-03 Ube Ind Ltd Continuous production of nylon 66
US4380615A (en) * 1981-03-05 1983-04-19 E. I. Du Pont De Nemours And Company Diamine recovery process
JPS5889424A (ja) * 1981-11-24 1983-05-27 Yamaha Motor Co Ltd 車輛の排気管系取付構造
DE3223823A1 (de) * 1982-06-25 1983-12-29 Bayer Ag, 5090 Leverkusen Verfahren zur kontinuierlichen herstellung von polyamiden
DE3321581A1 (de) * 1983-06-15 1984-12-20 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen herstellung von polyamiden
DE3321579A1 (de) * 1983-06-15 1984-12-20 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen herstellung von polyamiden
US5169582A (en) * 1985-05-08 1992-12-08 Ems-Inventa Ag Method and apparatus for the production of thermoplastic caprolactam containing molding compositions
JPS6247425U (US07902200-20110308-C00004.png) * 1985-09-13 1987-03-24
US5411710A (en) * 1993-06-30 1995-05-02 E. I. Dupont De Nemours And Company Apparatus for processing materials
DE19513940A1 (de) * 1994-07-14 1996-01-18 Inventa Ag Verfahren zur Herstellung von Vorkondensaten teilkristalliner oder amorpher, thermoplastisch verarbeitbarer teilaromatischer Polyamide bzw. Copolyamide
US5502154A (en) * 1994-11-30 1996-03-26 E. I. Du Pont De Nemours And Company Apparatus for processing materials
DE19808407A1 (de) * 1998-02-27 1999-09-09 Basf Ag Herstellung von Polyamiden durch Reaktivdestillation
JP2002528581A (ja) * 1998-10-26 2002-09-03 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー オメガ−アミノニトリルからポリアミドを製造する連続重合方法
US6627046B1 (en) * 2000-01-21 2003-09-30 E. I. Du Pont De Nemours And Company Separation of the products of polyamide ammonolysis
DE60119595T2 (de) 2000-01-21 2006-09-14 Mitsubishi Gas Chemical Co., Inc. Verfahren zur Herstellung von Polyamid
FR2835832B1 (fr) * 2002-02-08 2004-03-19 Atofina Procede d'oligomerisation d'acide lactique
CN113830951A (zh) 2013-05-01 2021-12-24 英威达纺织（英国）有限公司 用于从聚酰胺合成工艺回收水的方法和系统
CN104129880B (zh) 2013-05-01 2018-11-23 英威达纺织（英国）有限公司 用于从聚酰胺合成工艺回收水的方法和系统
TW201500404A (zh) * 2013-05-01 2015-01-01 Invista Tech Sarl 用於在聚醯胺合成方法中監測凝膠形成之方法及系統
JP6521950B2 (ja) 2013-06-12 2019-05-29 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 脂肪族又は部分芳香族のポリアミドオリゴマーを連続的に製造する方法
MX368538B (es) * 2013-06-12 2019-10-07 Basf Se Proceso para la preparacion continua de una poliamida alifatica o parcialmente aromatica.
KR102219463B1 (ko) * 2013-06-12 2021-02-25 바스프 에스이 폴리아미드 올리고머의 연속 제조 방법 및 열가소적으로 가공될 수 있는 반결정질 또는 비정질 폴리아미드의 제조 방법
JP2024504228A (ja) 2020-11-16 2024-01-31 インヴィスタ テキスタイルズ（ユー．ケー．）リミテッド ポリアミドポリマーを調製するための誘導加熱要素を備える装置

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD62912A (US07902200-20110308-C00004.png) *
US2689839A (en) * 1951-08-22 1954-09-21 Du Pont Dispersion of delusterants in polyamides
CA659196A (en) * 1963-03-12 J. Maan Christiaan Process and an apparatus for the continuous preparation of linear polycondensation products
US3296217A (en) * 1964-06-01 1967-01-03 Monsanto Co Continuous polymerization process for polyamide preparation
GB1114476A (en) * 1965-06-01 1968-05-22 Vickers Zimmer Ag Polycondensation reactor
US3402152A (en) * 1964-05-15 1968-09-17 Monsanto Co Process for preparing a polyamide

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE484840A (US07902200-20110308-C00004.png) * 1947-11-28
NL266575A (US07902200-20110308-C00004.png) * 1960-07-01
GB1145286A (en) * 1965-04-30 1969-03-12 Ici Ltd Polyamide preparation
US3501441A (en) * 1968-05-06 1970-03-17 Monsanto Co Process for preparing a polyamide

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD62912A (US07902200-20110308-C00004.png) *
CA659196A (en) * 1963-03-12 J. Maan Christiaan Process and an apparatus for the continuous preparation of linear polycondensation products
US2689839A (en) * 1951-08-22 1954-09-21 Du Pont Dispersion of delusterants in polyamides
US3402152A (en) * 1964-05-15 1968-09-17 Monsanto Co Process for preparing a polyamide
US3296217A (en) * 1964-06-01 1967-01-03 Monsanto Co Continuous polymerization process for polyamide preparation
GB1114476A (en) * 1965-06-01 1968-05-22 Vickers Zimmer Ag Polycondensation reactor

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996033234A1 (de) * 1995-04-15 1996-10-24 Basf Aktiengesellschaft Verfahren zur herstellung eines polyamids auf der basis einer dicarbonsäure und eines diamins
US6187877B1 (en) 1995-04-15 2001-02-13 Basf Aktiengesellschaft Process for producing a polyamide based on a dicarboxylic acid and a diamine
CN1090199C (zh) * 1995-04-15 2002-09-04 巴斯福股份公司 制备基于二羧酸和二胺的聚酰胺的方法
WO2003068359A2 (de) * 2002-02-15 2003-08-21 Basf Aktiengesellschaft Reaktionskolonne in spezieller kombination mit naturumlaufverdampfer
WO2003068359A3 (de) * 2002-02-15 2003-11-06 Basf Ag Reaktionskolonne in spezieller kombination mit naturumlaufverdampfer
KR100832822B1 (ko) * 2002-02-15 2008-05-28 바스프 에스이 증류 컬럼 및/또는 용기 및 순환식 증발기를 포함하는 배열의 사용 방법
US7544832B2 (en) 2002-02-15 2009-06-09 Basf Aktiengesellschaft Reaction column in a special combination with a natural circulation evaporator

Also Published As

Publication number Publication date
FR2220554B1 (US07902200-20110308-C00004.png) 1980-11-21
CA1015894A (en) 1977-08-16
GB1453485A (en) 1976-10-20
JPS5646487B2 (US07902200-20110308-C00004.png) 1981-11-04
US3900450A (en) 1975-08-19
FR2220554A1 (US07902200-20110308-C00004.png) 1974-10-04
DE2410474C2 (US07902200-20110308-C00004.png) 1987-10-01
JPS502092A (US07902200-20110308-C00004.png) 1975-01-10
IT1011020B (it) 1977-01-20

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Legal Events

Date Code Title Description
OGA New person/name/address of the applicant
8110 Request for examination paragraph 44
D2 Grant after examination
8364 No opposition during term of opposition