DE210917T1 - Verfahren zur herstellung eines cellulose-ethers mit einem verminderten polymerisationsgrad. - Google Patents
Verfahren zur herstellung eines cellulose-ethers mit einem verminderten polymerisationsgrad.Info
- Publication number
- DE210917T1 DE210917T1 DE1986401621 DE86401621T DE210917T1 DE 210917 T1 DE210917 T1 DE 210917T1 DE 1986401621 DE1986401621 DE 1986401621 DE 86401621 T DE86401621 T DE 86401621T DE 210917 T1 DE210917 T1 DE 210917T1
- Authority
- DE
- Germany
- Prior art keywords
- cellulose ether
- hydrogen chloride
- reactant
- chloride solution
- amount
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920003086 cellulose ether Polymers 0.000 title claims 8
- 238000006116 polymerization reaction Methods 0.000 title claims 3
- 238000004519 manufacturing process Methods 0.000 title 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 7
- 239000000376 reactant Substances 0.000 claims 5
- 238000000034 method Methods 0.000 claims 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 239000001913 cellulose Substances 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 229920003124 powdered cellulose Polymers 0.000 claims 1
- 235000019814 powdered cellulose Nutrition 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/20—Post-etherification treatments of chemical or physical type, e.g. mixed etherification in two steps, including purification
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- A61K9/28—Dragees; Coated pills or tablets, e.g. with film or compression coating
- A61K9/2806—Coating materials
- A61K9/2833—Organic macromolecular compounds
- A61K9/286—Polysaccharides, e.g. gums; Cyclodextrin
- A61K9/2866—Cellulose; Cellulose derivatives, e.g. hydroxypropyl methylcellulose
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16354985A JPS6225101A (ja) | 1985-07-24 | 1985-07-24 | 低重合度セルロ−スエ−テルの製造方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE210917T1 true DE210917T1 (de) | 1988-02-04 |
Family
ID=15776006
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1986401621 Pending DE210917T1 (de) | 1985-07-24 | 1986-07-21 | Verfahren zur herstellung eines cellulose-ethers mit einem verminderten polymerisationsgrad. |
| DE8686401621T Revoked DE3675993D1 (de) | 1985-07-24 | 1986-07-21 | Verfahren zur herstellung eines cellulose-ethers mit einem verminderten polymerisationsgrad. |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8686401621T Revoked DE3675993D1 (de) | 1985-07-24 | 1986-07-21 | Verfahren zur herstellung eines cellulose-ethers mit einem verminderten polymerisationsgrad. |
Country Status (4)
| Country | Link |
|---|---|
| EP (1) | EP0210917B1 (en:Method) |
| JP (1) | JPS6225101A (en:Method) |
| AU (1) | AU583139B2 (en:Method) |
| DE (2) | DE210917T1 (en:Method) |
Families Citing this family (59)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5476668A (en) * | 1990-08-24 | 1995-12-19 | Shin-Etsu Chemical Co., Ltd. | Base for film-coating pharmaceuticals and method for preparing same |
| CA2071488C (en) * | 1990-08-24 | 1996-05-07 | Kazuto Kobayashi | Base for film-coating pharmaceuticals and method for preparing same |
| US6261218B1 (en) * | 1998-12-01 | 2001-07-17 | The Dow Chemical Company | Process and apparatus for making low molecular weight cellulose ethers |
| US6294008B1 (en) | 1999-04-21 | 2001-09-25 | The Dow Chemical Company | Haze-free cellulose ether capsules and process for making |
| US6306333B1 (en) | 1999-06-24 | 2001-10-23 | The Dow Chemical Company | Process for making cellulose ethers having reduced yellowing and discoloration |
| DE10009642C1 (de) * | 2000-03-01 | 2001-06-13 | Clariant Gmbh | Verfahren zur sauer katalysierten, hydrolytischen Depolymerisierung von Celluloseethern und Verwendung einer emaillierten Drucknutsche zur Depolymerisierung von Celluloseethern |
| KR100461565B1 (ko) * | 2001-09-22 | 2004-12-14 | 삼성정밀화학 주식회사 | 저점도 히드록시프로필메틸 셀룰로오스의 제조방법 |
| WO2007023513A1 (ja) * | 2005-08-22 | 2007-03-01 | Shin-Etsu Chemical Co., Ltd. | 溶解性の改善されたセルロース誘導体の製造製法 |
| US8865432B2 (en) | 2004-02-26 | 2014-10-21 | Shin-Etsu Chemical Co., Ltd. | Method for preparing cellulose derivatives having solubility improved |
| ATE519785T1 (de) * | 2006-06-14 | 2011-08-15 | Dow Global Technologies Llc | Verfahren zur verringerung des mittleren molekulargewichts von celluloseethern |
| JP5902697B2 (ja) | 2010-10-12 | 2016-04-13 | ダウ グローバル テクノロジーズ エルエルシー | 新規なセルロースエーテルおよびその使用 |
| JP5681330B2 (ja) | 2011-07-27 | 2015-03-04 | ダウ グローバル テクノロジーズ エルエルシー | セルロースエーテルからアルキレンハロゲノヒドリンを除去する方法 |
| US20140168771A1 (en) | 2011-08-12 | 2014-06-19 | Dow Global Technologies Llc | Optical retardation film and method of manufacturing |
| EP2768321B1 (en) | 2011-10-19 | 2020-05-27 | Dow Global Technologies LLC | Methods and compositions for inducing satiety |
| WO2013154981A1 (en) | 2012-04-11 | 2013-10-17 | Dow Global Technologies Llc | Melt-extruded composition comprising a cellulose ether |
| WO2013154607A1 (en) | 2012-04-11 | 2013-10-17 | Dow Global Technologies Llc | Esterified cellulose ethers having a specific substituent distribution |
| KR102065326B1 (ko) | 2012-04-11 | 2020-01-13 | 다우 글로벌 테크놀로지스 엘엘씨 | 유기 희석제와 셀룰로즈 에테르를 포함하는 조성물 |
| BR112014032017A2 (pt) | 2012-07-17 | 2017-06-27 | Dow Global Technologies Llc | dispersão sólida, dispersão sólida extrudada e processo para produzir uma dispersão sólida |
| JP6166372B2 (ja) | 2012-08-24 | 2017-07-19 | ダウ グローバル テクノロジーズ エルエルシー | アルカリ金属カルボン酸塩および脂肪族カルボン酸の存在下でエステル化セルロースエーテルを調製するためのプロセス |
| CN104755503B (zh) | 2012-08-24 | 2018-03-06 | 陶氏环球技术有限责任公司 | 在脂族羧酸的存在下制备纤维素醚的酯的方法 |
| EP2888289B1 (en) | 2012-08-24 | 2019-08-07 | Dow Global Technologies LLC | Partially cross-linked esterified cellulose ethers |
| WO2014052213A1 (en) | 2012-09-25 | 2014-04-03 | Dow Global Technologies Llc | Process for producing cellulose derivatives of high bulk density, good flowability and/or dispersibility in cold water as well as low solution color |
| WO2014168917A1 (en) | 2013-04-12 | 2014-10-16 | Dow Global Technologies Llc | Process for preparing an aqueous solution of saccharides and methylcellulose |
| EP2986671B1 (en) | 2013-04-12 | 2017-07-12 | Dow Global Technologies LLC | Process for preparing an aqueous solution of a methylcellulose |
| WO2014168914A1 (en) | 2013-04-12 | 2014-10-16 | Dow Global Technologies Llc | Water-soluble polysaccharides of improved palatability |
| US9890221B2 (en) | 2013-05-14 | 2018-02-13 | Dow Global Technologies Llc | Cellulose ethers esterified with dicarboxylic acid |
| KR102348393B1 (ko) | 2014-01-16 | 2022-01-11 | 다우 글로벌 테크놀로지스 엘엘씨 | 적층 제조용 지지 물질의 회수 |
| WO2015108768A1 (en) | 2014-01-16 | 2015-07-23 | Dow Global Technologies Llc | Support materials for 3d printing |
| MX375728B (es) | 2014-01-16 | 2025-03-06 | Nutrition & Biosciences Usa 1 Llc | Composición cerámica moldeable con calor que contiene una hidroxipropilmetilcelulosa. |
| MX2016010140A (es) | 2014-02-20 | 2016-11-15 | Dow Global Technologies Llc | Nuevos eteres de celulosa esterificados de alto peso molecular y homogeneidad. |
| BR112017003191A2 (pt) | 2014-08-27 | 2017-11-28 | Dow Global Technologies Llc | éteres de celulose esterificados com baixo teor de insolúveis em acetona |
| EP3241873B1 (en) | 2014-09-10 | 2018-11-14 | PPG Industries Ohio, Inc. | Aqueous separation liquid and process for removing paint overspray from a paint spray booth |
| US10196461B2 (en) | 2014-10-31 | 2019-02-05 | Dow Global Technologies Llc | Efficient process for preparing an ester of a cellulose ether |
| KR101839295B1 (ko) | 2014-10-31 | 2018-04-27 | 다우 글로벌 테크놀로지스 엘엘씨 | 셀룰로오스 에테르의 에스테르를 제조하기 위한 방법 |
| JP6291137B2 (ja) | 2014-10-31 | 2018-03-14 | ダウ グローバル テクノロジーズ エルエルシー | セルロースエーテルアセテートサクシネートを生成するための方法 |
| KR20170128358A (ko) | 2015-03-16 | 2017-11-22 | 다우 글로벌 테크놀로지스 엘엘씨 | 낮은 중화도를 갖는 수용성 에스테르화 셀룰로오스 에테르 |
| JP6295380B2 (ja) | 2015-03-16 | 2018-03-14 | ダウ グローバル テクノロジーズ エルエルシー | 脂肪族カルボン酸の存在下でエステル化セルロースエーテルを調製するためのプロセス |
| BR112017018367A2 (pt) | 2015-03-16 | 2018-04-10 | Dow Global Technologies Llc | gelificação de éteres de celulose esterificados |
| CN107567462B (zh) | 2015-05-15 | 2020-10-16 | 陶氏环球技术有限责任公司 | 用于制造具有极高分子量和低粘度的酯化纤维素醚的方法 |
| KR20180008523A (ko) | 2015-05-15 | 2018-01-24 | 다우 글로벌 테크놀로지스 엘엘씨 | 고분자량의 에스테르화된 셀룰로오스 에테르의 제조 방법 |
| EP3307839B1 (en) | 2015-06-09 | 2019-02-27 | Dow Global Technologies LLC | Support materials for 3d printing |
| JP6426878B2 (ja) | 2015-09-24 | 2018-11-21 | ダウ グローバル テクノロジーズ エルエルシー | 酢酸及び反応触媒の存在下でセルロースエーテルのエステルを調製するためのプロセス |
| EP3216807B2 (en) | 2016-03-09 | 2022-05-18 | Shin-Etsu Chemical Co., Ltd. | Coating composition containing methyl cellulose, method for producing the same, and solid preparation |
| WO2017223018A1 (en) | 2016-06-23 | 2017-12-28 | Dow Global Technologies Llc | Esterified cellulose ethers comprising trimellityl groups |
| EP3475309B1 (en) | 2016-06-23 | 2020-07-29 | Dow Global Technologies, LLC | Esterified cellulose ethers comprising phthalyl groups |
| WO2018039214A1 (en) | 2016-08-23 | 2018-03-01 | Dow Global Technologies Llc | Esterified cellulose ethers comprising maleyl groups |
| EP3504246B1 (en) | 2016-08-23 | 2020-07-22 | Dow Global Technologies LLC | Cellulose ether acetate phthalates |
| KR102373750B1 (ko) * | 2016-10-06 | 2022-03-15 | 신에쓰 가가꾸 고교 가부시끼가이샤 | 저중합도 셀룰로오스 에테르의 제조 방법 |
| CN109803984A (zh) | 2016-10-18 | 2019-05-24 | 陶氏环球技术有限责任公司 | 制备酯化纤维素醚的有效方法 |
| EP3897730A1 (en) | 2018-12-18 | 2021-10-27 | DDP Specialty Electronic Materials US, Inc. | A sustained release composition comprising a methylcellulose |
| US20220031623A1 (en) | 2018-12-18 | 2022-02-03 | DDP Specialty Electronic Materials US, Inc. | A sustained release composition comprising a methylcellulose |
| WO2020131800A1 (en) | 2018-12-18 | 2020-06-25 | DDP Specialty Electronic Materials US, Inc. | A sustained release composition comprising an ethylcellulose |
| US20220088037A1 (en) | 2018-12-18 | 2022-03-24 | DDP Specialty Electronic Materials US, Inc. | A sustained release composition comprising a hydroxyalkyl methylcellulose |
| WO2021118917A1 (en) | 2019-12-09 | 2021-06-17 | Nutrition & Biosciences Usa 1, Llc | Composition comprising a highly substituted hydroxypropyl methylcellulose and a sugar alcohol |
| JP7414685B2 (ja) * | 2020-10-22 | 2024-01-16 | 信越化学工業株式会社 | 解重合されたセルロースエーテルの製造方法 |
| JP7414686B2 (ja) | 2020-10-22 | 2024-01-16 | 信越化学工業株式会社 | 解重合されたセルロースエーテルの製造方法 |
| EP4323444A1 (en) | 2021-04-09 | 2024-02-21 | Nutrition & Biosciences USA 1, LLC | A methylcellulose with high powder dissolution temperature |
| EP4352109A1 (en) | 2021-06-08 | 2024-04-17 | Nutrition & Biosciences USA 1, LLC | A process for producing a methylcellulose or hydroxyalkyl methylcellulose |
| EP4392464A1 (en) | 2021-08-26 | 2024-07-03 | Nutrition & Biosciences USA 1, LLC | Novel hydroxyalkyl methylcellulose and its use |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1679943A (en) * | 1925-12-21 | 1928-08-07 | Eastman Kodak Co | Process for reducing the viscosity characteristics of cellulose ethers and products thereof |
| US1943461A (en) * | 1930-04-16 | 1934-01-16 | Ici Ltd | Cellulose ether and method of making same |
| JPS4841037B1 (en:Method) * | 1964-10-26 | 1973-12-04 | ||
| GB1296853A (en:Method) * | 1969-01-31 | 1972-11-22 | ||
| US4061859A (en) * | 1976-06-14 | 1977-12-06 | The Dow Chemical Company | Viscosity reduction of cellulose derivatives |
-
1985
- 1985-07-24 JP JP16354985A patent/JPS6225101A/ja active Granted
-
1986
- 1986-07-21 DE DE1986401621 patent/DE210917T1/de active Pending
- 1986-07-21 AU AU60390/86A patent/AU583139B2/en not_active Ceased
- 1986-07-21 DE DE8686401621T patent/DE3675993D1/de not_active Revoked
- 1986-07-21 EP EP19860401621 patent/EP0210917B1/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| AU6039086A (en) | 1987-01-29 |
| EP0210917B1 (en) | 1990-12-05 |
| JPS6225101A (ja) | 1987-02-03 |
| EP0210917A2 (en) | 1987-02-04 |
| DE3675993D1 (de) | 1991-01-17 |
| JPH0476361B2 (en:Method) | 1992-12-03 |
| AU583139B2 (en) | 1989-04-20 |
| EP0210917A3 (en) | 1987-09-02 |
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