DE2051963C2 - Verfahren zur Herstellung von Titantetrachlorid - Google Patents
Verfahren zur Herstellung von TitantetrachloridInfo
- Publication number
- DE2051963C2 DE2051963C2 DE2051963A DE2051963A DE2051963C2 DE 2051963 C2 DE2051963 C2 DE 2051963C2 DE 2051963 A DE2051963 A DE 2051963A DE 2051963 A DE2051963 A DE 2051963A DE 2051963 C2 DE2051963 C2 DE 2051963C2
- Authority
- DE
- Germany
- Prior art keywords
- fecb
- reaction gases
- condenser
- fecl
- chlorination furnace
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 21
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 title claims description 6
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 239000007789 gas Substances 0.000 claims description 52
- 238000006243 chemical reaction Methods 0.000 claims description 39
- 238000005660 chlorination reaction Methods 0.000 claims description 25
- 229910010165 TiCu Inorganic materials 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 15
- 239000007787 solid Substances 0.000 claims description 13
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 12
- 229910000831 Steel Inorganic materials 0.000 claims description 7
- 239000010959 steel Substances 0.000 claims description 7
- 229910052742 iron Inorganic materials 0.000 claims description 6
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 5
- 239000010936 titanium Substances 0.000 claims description 5
- 229910052719 titanium Inorganic materials 0.000 claims description 5
- 239000012495 reaction gas Substances 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 2
- 239000010410 layer Substances 0.000 description 8
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 6
- 229910052801 chlorine Inorganic materials 0.000 description 6
- 239000000460 chlorine Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 6
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical class Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 description 6
- 238000005260 corrosion Methods 0.000 description 5
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 4
- 238000009833 condensation Methods 0.000 description 4
- 230000005494 condensation Effects 0.000 description 4
- 239000002826 coolant Substances 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical class Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000000446 fuel Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 2
- 239000000571 coke Substances 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical compound O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 description 2
- 238000007711 solidification Methods 0.000 description 2
- 230000008023 solidification Effects 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 230000008646 thermal stress Effects 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910015449 FeCU Inorganic materials 0.000 description 1
- MFLCLMHBOLWTHH-UHFFFAOYSA-N Panial Natural products COc1ccc2C=CC(=O)Oc2c1C(O)C=C(/C)C=O MFLCLMHBOLWTHH-UHFFFAOYSA-N 0.000 description 1
- 241000282320 Panthera leo Species 0.000 description 1
- 241000158147 Sator Species 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000010494 dissociation reaction Methods 0.000 description 1
- 230000005593 dissociations Effects 0.000 description 1
- 239000010408 film Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
- C22B34/1231—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes treatment or purification of titanium containing products obtained by dry processes, e.g. condensation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US86834169A | 1969-10-22 | 1969-10-22 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2051963A1 DE2051963A1 (de) | 1971-04-29 |
| DE2051963C2 true DE2051963C2 (de) | 1985-03-28 |
Family
ID=25351476
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2051963A Expired DE2051963C2 (de) | 1969-10-22 | 1970-10-22 | Verfahren zur Herstellung von Titantetrachlorid |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US3628913A (enExample) |
| JP (1) | JPS4930350B1 (enExample) |
| CA (1) | CA935272A (enExample) |
| DE (1) | DE2051963C2 (enExample) |
| FR (1) | FR2065461B1 (enExample) |
| GB (1) | GB1320189A (enExample) |
| ZA (1) | ZA706962B (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3865920A (en) * | 1973-03-14 | 1975-02-11 | Rutile & Zircon Mines Newcastl | Process for beneficiating a titaniferous ore and production of chlorine and iron oxide |
| US4066424A (en) * | 1976-10-13 | 1978-01-03 | E. I. Du Pont De Nemours And Company | Selectively recovering metal chlorides from gaseous effluent |
| SE406984B (sv) * | 1976-11-19 | 1979-03-05 | Bergkvist Lars A | Indentifieringsanordning |
| DE2818881C3 (de) * | 1977-09-21 | 1981-08-06 | Mineral Process Licensing Corp. B.V., Den Haag | Verfahren zur Chlorierung von Eisen und insbesondere auch Titan enthaltenden Materialien |
| FR2467821A1 (fr) * | 1979-10-18 | 1981-04-30 | Zaporozhsky Titano Magnievy | Dispositif pour la separation du tetrachlorure de titane se trouvant dans un melange vapeurs-gaz |
| US4961911A (en) * | 1989-03-02 | 1990-10-09 | E. I. Du Pont De Nemours And Company | Process for reducing carbon monoxide emissions from a fluidized bed titanium dioxide chlorinator |
| DE4130808C2 (de) * | 1991-09-17 | 1998-02-19 | Kronos Titan Gmbh | Verfahren zum Erhöhen der Reinheit von technischem Eisenchlorid |
| EP1657218A1 (en) * | 2004-11-10 | 2006-05-17 | Kerr-McGee Pigments (Holland) B.V. | Process and apparatus for producing purified titanium tetrachloride |
| US7368096B2 (en) * | 2005-06-07 | 2008-05-06 | E.I. Du Pont De Nemours And Company | Process for separating solids from a purification purge stream |
| CN103058270B (zh) * | 2012-12-26 | 2014-08-06 | 攀钢集团攀枝花钢铁研究院有限公司 | 用于低温沸腾氯化炉的控制系统及控制方法 |
| JP6297404B2 (ja) * | 2014-05-14 | 2018-03-20 | 東邦チタニウム株式会社 | スポンジチタンの製造方法およびこれを用いたチタンインゴットの製造方法 |
| CN104310465B (zh) * | 2014-10-17 | 2016-03-02 | 金川集团股份有限公司 | 一种用于沸腾氯化炉的耐高温耐腐蚀炉体及其制作方法 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1069126B (de) * | 1959-11-19 | The New Jersey Zinc Company, New York, N. Y. (V. St. A.) | Verfahren zur Gewiinnung von Titantetirachlorid aus gasformigen Gemischen, von Titantetrachlorid mit normalerweise festen Eisen- und/oder AHuminiuimchloiid | |
| US1814392A (en) * | 1929-01-07 | 1931-07-14 | Frank S Low | Chlorination of ferrochrome |
| US2245358A (en) * | 1939-07-14 | 1941-06-10 | Pittsburgh Plate Glass Co | Chlorination of titanium bearing materials |
| US2675891A (en) * | 1949-04-01 | 1954-04-20 | Schweizerhall Saeurefab | Process for the separation of metal chlorides from chlorination gases |
| US2668424A (en) * | 1950-10-26 | 1954-02-09 | Du Pont | Process for cooling vaporous materials |
| US2925145A (en) * | 1954-08-06 | 1960-02-16 | British Titan Products | Separation of metallic halides |
| US2953218A (en) * | 1955-10-25 | 1960-09-20 | British Titan Products | Separation of metallic halides |
| GB806052A (en) * | 1955-10-25 | 1958-12-17 | British Titan Products | Improvements in or relating to the separation of metallic halides |
| US2792077A (en) * | 1956-01-18 | 1957-05-14 | Thann Fab Prod Chem | Recovery of titanium tetrachloride |
| US2940541A (en) * | 1956-10-15 | 1960-06-14 | Columbia Southern Chem Corp | Method of purifying gases |
| US2999733A (en) * | 1957-01-16 | 1961-09-12 | British Titan Products | Chlorination processes |
| US2849083A (en) * | 1957-01-31 | 1958-08-26 | American Cyanamid Co | Separation of iron chloride from gaseous iron chloride-titanium tetrachloride mixtures |
| US2897918A (en) * | 1957-07-02 | 1959-08-04 | Titanium Metals Corp | Separation of halides |
| US3261664A (en) * | 1963-11-21 | 1966-07-19 | Du Pont | Process for the production and separation of titanium tetrachloride from crystalline ferrous chloride |
-
1969
- 1969-10-22 US US868341A patent/US3628913A/en not_active Expired - Lifetime
-
1970
- 1970-10-02 CA CA094719A patent/CA935272A/en not_active Expired
- 1970-10-13 ZA ZA706962A patent/ZA706962B/xx unknown
- 1970-10-20 GB GB4972670A patent/GB1320189A/en not_active Expired
- 1970-10-21 FR FR7037990A patent/FR2065461B1/fr not_active Expired
- 1970-10-22 JP JP45092500A patent/JPS4930350B1/ja active Pending
- 1970-10-22 DE DE2051963A patent/DE2051963C2/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US3628913A (en) | 1971-12-21 |
| JPS4930350B1 (enExample) | 1974-08-12 |
| CA935272A (en) | 1973-10-16 |
| FR2065461B1 (enExample) | 1974-08-23 |
| FR2065461A1 (enExample) | 1971-07-30 |
| GB1320189A (en) | 1973-06-13 |
| ZA706962B (en) | 1971-08-25 |
| DE2051963A1 (de) | 1971-04-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition |