DE2049448C3 - Verfahren zur Herstellung einer viskosen wäßrigen Lösung auf Basis von Aluminium-hydroxo-chlorid-Komplexen - Google Patents
Verfahren zur Herstellung einer viskosen wäßrigen Lösung auf Basis von Aluminium-hydroxo-chlorid-KomplexenInfo
- Publication number
- DE2049448C3 DE2049448C3 DE2049448A DE2049448A DE2049448C3 DE 2049448 C3 DE2049448 C3 DE 2049448C3 DE 2049448 A DE2049448 A DE 2049448A DE 2049448 A DE2049448 A DE 2049448A DE 2049448 C3 DE2049448 C3 DE 2049448C3
- Authority
- DE
- Germany
- Prior art keywords
- solution
- aluminum
- acid
- temperature
- poise
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 19
- 239000007864 aqueous solution Substances 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title claims description 3
- 239000000243 solution Substances 0.000 claims description 58
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 25
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 22
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 19
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 18
- 229910052782 aluminium Inorganic materials 0.000 claims description 18
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 8
- 229940075614 colloidal silicon dioxide Drugs 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 230000002378 acidificating effect Effects 0.000 claims description 7
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 7
- 239000004327 boric acid Substances 0.000 claims description 7
- 230000002401 inhibitory effect Effects 0.000 claims description 6
- 238000007711 solidification Methods 0.000 claims description 6
- 230000008023 solidification Effects 0.000 claims description 6
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 5
- 239000000470 constituent Substances 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 claims description 3
- 230000008020 evaporation Effects 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000000052 vinegar Substances 0.000 claims description 2
- 239000003039 volatile agent Substances 0.000 claims 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000007788 liquid Substances 0.000 description 6
- 229960000583 acetic acid Drugs 0.000 description 5
- 239000007795 chemical reaction product Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000000377 silicon dioxide Substances 0.000 description 4
- 235000012239 silicon dioxide Nutrition 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000004090 dissolution Methods 0.000 description 3
- 239000012362 glacial acetic acid Substances 0.000 description 3
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 3
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 239000008119 colloidal silica Substances 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 239000011253 protective coating Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 229910052810 boron oxide Inorganic materials 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- -1 for example Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/0004—Preparation of sols
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/48—Halides, with or without other cations besides aluminium
- C01F7/56—Chlorides
- C01F7/57—Basic aluminium chlorides, e.g. polyaluminium chlorides
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C13/00—Fibre or filament compositions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/62227—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
- C04B35/62231—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on oxide ceramics
- C04B35/62236—Fibres based on aluminium oxide
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Ceramic Engineering (AREA)
- Dispersion Chemistry (AREA)
- Structural Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Colloid Chemistry (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Fireproofing Substances (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US818446A US3579361A (en) | 1969-04-22 | 1969-04-22 | Viscous liquid material and process for making same |
| JP45014727A JPS4937346B1 (enExample) | 1969-04-22 | 1970-02-21 | |
| GB09320/70A GB1283833A (en) | 1969-04-22 | 1970-04-22 | Viscous liquid composition comprising chemically combined aluminium |
| BE749351D BE749351A (fr) | 1969-04-22 | 1970-04-22 | Composition liquide visqueuse |
| FR7034403A FR2062527A5 (enExample) | 1969-04-22 | 1970-09-23 | |
| CA094184A CA935256A (en) | 1969-04-22 | 1970-09-28 | Viscous liquid material and process for making same |
| DE2049448A DE2049448C3 (de) | 1969-04-22 | 1970-10-08 | Verfahren zur Herstellung einer viskosen wäßrigen Lösung auf Basis von Aluminium-hydroxo-chlorid-Komplexen |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US81844669A | 1969-04-22 | 1969-04-22 | |
| FR7034403A FR2062527A5 (enExample) | 1969-04-22 | 1970-09-23 | |
| CA094184A CA935256A (en) | 1969-04-22 | 1970-09-28 | Viscous liquid material and process for making same |
| DE2049448A DE2049448C3 (de) | 1969-04-22 | 1970-10-08 | Verfahren zur Herstellung einer viskosen wäßrigen Lösung auf Basis von Aluminium-hydroxo-chlorid-Komplexen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2049448A1 DE2049448A1 (de) | 1972-04-13 |
| DE2049448B2 DE2049448B2 (de) | 1978-09-21 |
| DE2049448C3 true DE2049448C3 (de) | 1979-09-20 |
Family
ID=27425409
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2049448A Expired DE2049448C3 (de) | 1969-04-22 | 1970-10-08 | Verfahren zur Herstellung einer viskosen wäßrigen Lösung auf Basis von Aluminium-hydroxo-chlorid-Komplexen |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US3579361A (enExample) |
| JP (1) | JPS4937346B1 (enExample) |
| BE (1) | BE749351A (enExample) |
| CA (1) | CA935256A (enExample) |
| DE (1) | DE2049448C3 (enExample) |
| FR (1) | FR2062527A5 (enExample) |
| GB (1) | GB1283833A (enExample) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5259139U (enExample) * | 1975-10-24 | 1977-04-28 |
-
1969
- 1969-04-22 US US818446A patent/US3579361A/en not_active Expired - Lifetime
-
1970
- 1970-02-21 JP JP45014727A patent/JPS4937346B1/ja active Pending
- 1970-04-22 BE BE749351D patent/BE749351A/xx not_active IP Right Cessation
- 1970-04-22 GB GB09320/70A patent/GB1283833A/en not_active Expired
- 1970-09-23 FR FR7034403A patent/FR2062527A5/fr not_active Expired
- 1970-09-28 CA CA094184A patent/CA935256A/en not_active Expired
- 1970-10-08 DE DE2049448A patent/DE2049448C3/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2049448A1 (de) | 1972-04-13 |
| CA935256A (en) | 1973-10-16 |
| FR2062527A5 (enExample) | 1971-06-25 |
| US3579361A (en) | 1971-05-18 |
| GB1283833A (en) | 1972-08-02 |
| DE2049448B2 (de) | 1978-09-21 |
| BE749351A (fr) | 1970-10-22 |
| JPS4937346B1 (enExample) | 1974-10-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE1467019B2 (de) | Verfahren zur Herstellung von feinteiliger Kieselsäure durch Umsetzung von Alkalisilikatlösungen mit Säurelösungen | |
| EP3110822B1 (de) | Verfahren zur herstellung von wässrigen hydrolysaten von aminoalkyltrialkoxysilanen | |
| DE4035418C2 (de) | Wolframoxid/Zinnoxid-Verbundsol sowie Metalloxidsol und Verfahren zu ihrer Herstellung | |
| DD269374A5 (de) | Stabilisierter roter phosphor sowie verfahren zu seiner herstellung | |
| DE69500793T2 (de) | Synthetisches Silikaglaspulver | |
| DE1767006C3 (de) | Kristallines Zinkborat mit geringem Hydratwassergehalt, Verfahren zu seiner Herstellung und seine Verwendung | |
| EP0143933B1 (de) | Verfahren zur Herstellung von basischem Kupferphosphat mit heller Eigenfarbe und einer mittleren Korngrösse kleiner als 10 um | |
| DE2049448C3 (de) | Verfahren zur Herstellung einer viskosen wäßrigen Lösung auf Basis von Aluminium-hydroxo-chlorid-Komplexen | |
| EP0080227A1 (de) | Verfahren zur Herstellung von Kupfer-II-hydroxid | |
| DE2343026A1 (de) | Verfahren zur herstellung waessriger alkalipolysilikatloesungen | |
| DE2751076C2 (de) | Verfahren zur Herstellung von stabilen wäßrigen Formaldehydsuspensionen | |
| WO1993000321A1 (de) | Verfahren zur herstellung einer alkali- und/oder erdalkalihaltigen aluminiumtriformiatlösung, hochkonzentrierte alkali- und/oder erdalkalihaltige aluminiumtriformiatlösungen und ihre verwendung | |
| DE1939619C3 (de) | Verfahren zur Herstellung einer wäßrigen Dispersion von SiO2.TeUchen | |
| DE2107970C3 (de) | Verfahren zur Herstellung sulfathaltiger, basischer Aluminiumchloride | |
| DE887945C (de) | Verfahren zur Herstellung von reinstem Aluminiumacetat mit niedrigem Essigsaeuregehalt | |
| EP0166185A1 (de) | Verfahren zur Herstellung von Kupfer-II-hydroxid | |
| CH623827A5 (enExample) | ||
| CH624428A5 (enExample) | ||
| DE69227377T2 (de) | Stabilisierte wässrige lösung | |
| DE636211C (de) | Abtrennung von Fluor und Aluminium aus Loesungen, die durch Aufschluss von Phosphat mit Saeuren erhalten werden | |
| DE1173880B (de) | Verfahren zur Herstellung stabiler Kieselsaeuresole | |
| DE2230505C2 (de) | Telomere und deren Verwendung zum Stabilisieren wässeriger Formaldehydlösungen | |
| DE2028281A1 (en) | Obtaining tin from solutions contg - ionic or free tin | |
| AT156812B (de) | Verfahren zur Herstellung von leichtlöslichen Formaldehydpräparaten. | |
| DE2926099B1 (de) | Verfahren zur Herstellung von Aluminiumfluorid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |