DE204653C - - Google Patents

Info

Publication number

DE204653C

DE204653C DENDAT204653D DE204653DA DE204653C DE 204653 C DE204653 C DE 204653C DE NDAT204653 D DENDAT204653 D DE NDAT204653D DE 204653D A DE204653D A DE 204653DA DE 204653 C DE204653 C DE 204653C

Authority

DE

Germany

Prior art keywords

nitrobenzene

azoxybenzene

percent

azoxy

heated

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• 125000005337 azoxy group Chemical group [N+]([O-])(=N*)* 0.000 claims description 3
• 229910001385 heavy metal Inorganic materials 0.000 claims description 3
• 238000000034 method Methods 0.000 claims description 2
• 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims description 2
• 125000001997 phenyl group Chemical class [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 2
• 239000003960 organic solvent Substances 0.000 claims 1
• 150000003568 thioethers Chemical class 0.000 claims 1
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
• LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 10
• XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 8
• GAUZCKBSTZFWCT-UHFFFAOYSA-N azoxybenzene Chemical compound C=1C=CC=CC=1[N+]([O-])=NC1=CC=CC=C1 GAUZCKBSTZFWCT-UHFFFAOYSA-N 0.000 description 4
• 229910052742 iron Inorganic materials 0.000 description 4
• 235000011121 sodium hydroxide Nutrition 0.000 description 4
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
• 150000004763 sulfides Chemical class 0.000 description 3
• DMLAVOWQYNRWNQ-UHFFFAOYSA-N azobenzene Chemical compound C1=CC=CC=C1N=NC1=CC=CC=C1 DMLAVOWQYNRWNQ-UHFFFAOYSA-N 0.000 description 2
• 239000002904 solvent Substances 0.000 description 2
• 241000295146 Gallionellaceae Species 0.000 description 1
• 239000003513 alkali Substances 0.000 description 1
• 150000001555 benzenes Chemical class 0.000 description 1
• 239000003085 diluting agent Substances 0.000 description 1
• 238000000605 extraction Methods 0.000 description 1
• VLZLOWPYUQHHCG-UHFFFAOYSA-N nitromethylbenzene Chemical compound [O-][N+](=O)CC1=CC=CC=C1 VLZLOWPYUQHHCG-UHFFFAOYSA-N 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• WGPCGCOKHWGKJJ-UHFFFAOYSA-N sulfanylidenezinc Chemical compound [Zn]=S WGPCGCOKHWGKJJ-UHFFFAOYSA-N 0.000 description 1
• 150000003464 sulfur compounds Chemical class 0.000 description 1
• 229910052984 zinc sulfide Inorganic materials 0.000 description 1