DE2022920A1 - Nitrocellulosetabletten und Verfahren zu ihrer Herstellung - Google Patents
Nitrocellulosetabletten und Verfahren zu ihrer HerstellungInfo
- Publication number
- DE2022920A1 DE2022920A1 DE19702022920 DE2022920A DE2022920A1 DE 2022920 A1 DE2022920 A1 DE 2022920A1 DE 19702022920 DE19702022920 DE 19702022920 DE 2022920 A DE2022920 A DE 2022920A DE 2022920 A1 DE2022920 A1 DE 2022920A1
- Authority
- DE
- Germany
- Prior art keywords
- nitrocellulose
- diphenylamine
- alkyl
- suspension
- tablets
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920001220 nitrocellulos Polymers 0.000 title claims description 76
- 239000000020 Nitrocellulose Substances 0.000 title claims description 75
- 238000000034 method Methods 0.000 title claims description 18
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical class C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 claims description 43
- 239000000725 suspension Substances 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 150000001412 amines Chemical class 0.000 claims description 13
- UUNBFTCKFYBASS-UHFFFAOYSA-N C(CCCCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCCCC Chemical compound C(CCCCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCCCC UUNBFTCKFYBASS-UHFFFAOYSA-N 0.000 claims description 11
- 125000000217 alkyl group Chemical group 0.000 claims description 11
- 239000002360 explosive Substances 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Natural products CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 125000004432 carbon atom Chemical group C* 0.000 claims description 6
- 235000019441 ethanol Nutrition 0.000 claims description 6
- 239000000835 fiber Substances 0.000 claims description 6
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 239000001257 hydrogen Substances 0.000 claims description 5
- 238000002844 melting Methods 0.000 claims description 4
- 230000008018 melting Effects 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 2
- 125000005909 ethyl alcohol group Chemical group 0.000 claims 1
- 125000001183 hydrocarbyl group Chemical group 0.000 claims 1
- FJWGYAHXMCUOOM-QHOUIDNNSA-N [(2s,3r,4s,5r,6r)-2-[(2r,3r,4s,5r,6s)-4,5-dinitrooxy-2-(nitrooxymethyl)-6-[(2r,3r,4s,5r,6s)-4,5,6-trinitrooxy-2-(nitrooxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-3,5-dinitrooxy-6-(nitrooxymethyl)oxan-4-yl] nitrate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O)O[C@H]1[C@@H]([C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@@H](CO[N+]([O-])=O)O1)O[N+]([O-])=O)CO[N+](=O)[O-])[C@@H]1[C@@H](CO[N+]([O-])=O)O[C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O FJWGYAHXMCUOOM-QHOUIDNNSA-N 0.000 description 67
- 229940079938 nitrocellulose Drugs 0.000 description 67
- 229940035422 diphenylamine Drugs 0.000 description 26
- 239000003826 tablet Substances 0.000 description 24
- 239000000243 solution Substances 0.000 description 8
- 238000010521 absorption reaction Methods 0.000 description 6
- 238000000576 coating method Methods 0.000 description 6
- -1 by dipping Substances 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- CDYHCLPQXKUDMV-UHFFFAOYSA-N n-decyl-n-phenylaniline Chemical compound C=1C=CC=CC=1N(CCCCCCCCCC)C1=CC=CC=C1 CDYHCLPQXKUDMV-UHFFFAOYSA-N 0.000 description 3
- 239000003380 propellant Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- QVXGKJYMVLJYCL-UHFFFAOYSA-N 2,3-di(nonyl)-N-phenylaniline Chemical compound C(CCCCCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCCCCC QVXGKJYMVLJYCL-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000035515 penetration Effects 0.000 description 2
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000010802 sludge Substances 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- RNBMWJIBIBMXDK-UHFFFAOYSA-N 2,3-dibutyl-N-phenylaniline Chemical compound C(CCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCC RNBMWJIBIBMXDK-UHFFFAOYSA-N 0.000 description 1
- CCTHJKWIHDXLHF-UHFFFAOYSA-N C(CCCC)C=1C(=C(C=CC=1)NC1=CC=CC=C1)CCCCC Chemical compound C(CCCC)C=1C(=C(C=CC=1)NC1=CC=CC=C1)CCCCC CCTHJKWIHDXLHF-UHFFFAOYSA-N 0.000 description 1
- IHUPKJXOZVBCNC-UHFFFAOYSA-N C(CCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCC Chemical compound C(CCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCC IHUPKJXOZVBCNC-UHFFFAOYSA-N 0.000 description 1
- LKDKCTLTRLXBKU-UHFFFAOYSA-N C(CCCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCCC Chemical compound C(CCCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCCC LKDKCTLTRLXBKU-UHFFFAOYSA-N 0.000 description 1
- NRSPMOUYOHSNOY-UHFFFAOYSA-N C(CCCCCCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCCCCCC Chemical compound C(CCCCCCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCCCCCC NRSPMOUYOHSNOY-UHFFFAOYSA-N 0.000 description 1
- RVKKRRXSXPNVLU-UHFFFAOYSA-N C(CCCCCCCCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCCCCCCCC Chemical compound C(CCCCCCCCCCC)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCCCCCCCC RVKKRRXSXPNVLU-UHFFFAOYSA-N 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- PZIMIYVOZBTARW-UHFFFAOYSA-N centralite Chemical compound C=1C=CC=CC=1N(CC)C(=O)N(CC)C1=CC=CC=C1 PZIMIYVOZBTARW-UHFFFAOYSA-N 0.000 description 1
- 230000001427 coherent effect Effects 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000007891 compressed tablet Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- VYQNWZOUAUKGHI-UHFFFAOYSA-N monobenzone Chemical compound C1=CC(O)=CC=C1OCC1=CC=CC=C1 VYQNWZOUAUKGHI-UHFFFAOYSA-N 0.000 description 1
- 229960000990 monobenzone Drugs 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- LVZUNTGFCXNQAF-UHFFFAOYSA-N n-nonyl-n-phenylaniline Chemical compound C=1C=CC=CC=1N(CCCCCCCCC)C1=CC=CC=C1 LVZUNTGFCXNQAF-UHFFFAOYSA-N 0.000 description 1
- MDCRQGZQPMIMEP-UHFFFAOYSA-N n-phenyl-n-undecylaniline Chemical compound C=1C=CC=CC=1N(CCCCCCCCCCC)C1=CC=CC=C1 MDCRQGZQPMIMEP-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 239000001508 potassium citrate Substances 0.000 description 1
- 229960002635 potassium citrate Drugs 0.000 description 1
- 235000011082 potassium citrates Nutrition 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000011814 protection agent Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B25/00—Compositions containing a nitrated organic compound
- C06B25/18—Compositions containing a nitrated organic compound the compound being nitrocellulose present as 10% or more by weight of the total composition
- C06B25/20—Compositions containing a nitrated organic compound the compound being nitrocellulose present as 10% or more by weight of the total composition with a non-explosive or a non-explosive or a non-thermic component
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B23/00—Compositions characterised by non-explosive or non-thermic constituents
- C06B23/006—Stabilisers (e.g. thermal stabilisers)
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
- Medicinal Preparation (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Cosmetics (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US82503369A | 1969-05-15 | 1969-05-15 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2022920A1 true DE2022920A1 (de) | 1971-01-14 |
Family
ID=25242959
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19702022920 Pending DE2022920A1 (de) | 1969-05-15 | 1970-05-11 | Nitrocellulosetabletten und Verfahren zu ihrer Herstellung |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US3597288A (cg-RX-API-DMAC7.html) |
| AU (1) | AU1505170A (cg-RX-API-DMAC7.html) |
| BE (1) | BE750421A (cg-RX-API-DMAC7.html) |
| CA (1) | CA924512A (cg-RX-API-DMAC7.html) |
| DE (1) | DE2022920A1 (cg-RX-API-DMAC7.html) |
| DK (1) | DK124745B (cg-RX-API-DMAC7.html) |
| ES (1) | ES380506A1 (cg-RX-API-DMAC7.html) |
| FR (1) | FR2047804A5 (cg-RX-API-DMAC7.html) |
| GB (1) | GB1295987A (cg-RX-API-DMAC7.html) |
| NL (1) | NL7006436A (cg-RX-API-DMAC7.html) |
| ZA (1) | ZA703273B (cg-RX-API-DMAC7.html) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109438146B (zh) * | 2018-10-15 | 2021-05-04 | 北方化学工业股份有限公司 | 一种室内烟花用硝化棉的料浆法生产工艺 |
| CN113683470A (zh) * | 2021-08-23 | 2021-11-23 | 姚鲁 | 一种改善射钉装药制造的安全和环保方法 |
-
1969
- 1969-05-15 US US825033A patent/US3597288A/en not_active Expired - Lifetime
-
1970
- 1970-04-30 CA CA081598A patent/CA924512A/en not_active Expired
- 1970-05-01 NL NL7006436A patent/NL7006436A/xx unknown
- 1970-05-11 DE DE19702022920 patent/DE2022920A1/de active Pending
- 1970-05-14 ZA ZA703273A patent/ZA703273B/xx unknown
- 1970-05-14 AU AU15051/70A patent/AU1505170A/en not_active Expired
- 1970-05-14 FR FR7017709A patent/FR2047804A5/fr not_active Expired
- 1970-05-14 BE BE750421D patent/BE750421A/xx unknown
- 1970-05-14 ES ES380506A patent/ES380506A1/es not_active Expired
- 1970-05-14 GB GB1295987D patent/GB1295987A/en not_active Expired
- 1970-05-14 DK DK245770AA patent/DK124745B/da unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NL7006436A (cg-RX-API-DMAC7.html) | 1970-11-17 |
| DK124745B (da) | 1972-11-20 |
| US3597288A (en) | 1971-08-03 |
| ZA703273B (en) | 1971-10-27 |
| GB1295987A (cg-RX-API-DMAC7.html) | 1972-11-08 |
| ES380506A1 (es) | 1972-10-16 |
| BE750421A (fr) | 1970-10-16 |
| CA924512A (en) | 1973-04-17 |
| AU1505170A (en) | 1971-11-18 |
| FR2047804A5 (cg-RX-API-DMAC7.html) | 1971-03-12 |
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