DE197161C - - Google Patents
Info
- Publication number
- DE197161C DE197161C DENDAT197161D DE197161DA DE197161C DE 197161 C DE197161 C DE 197161C DE NDAT197161 D DENDAT197161 D DE NDAT197161D DE 197161D A DE197161D A DE 197161DA DE 197161 C DE197161 C DE 197161C
- Authority
- DE
- Germany
- Prior art keywords
- parts
- isoborneol
- camphor
- permanganate
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims description 10
- DTGKSKDOIYIVQL-MRTMQBJTSA-N Isoborneol Natural products C1C[C@@]2(C)[C@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-MRTMQBJTSA-N 0.000 claims description 10
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 claims description 10
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 claims description 10
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims description 9
- 241000723346 Cinnamomum camphora Species 0.000 claims description 9
- 229930008380 camphor Natural products 0.000 claims description 9
- 229960000846 camphor Drugs 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 230000003647 oxidation Effects 0.000 claims description 4
- 238000007254 oxidation reaction Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- 239000003929 acidic solution Substances 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 229960000583 acetic acid Drugs 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 239000012362 glacial acetic acid Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 150000008043 acidic salts Chemical class 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 229910000365 copper sulfate Inorganic materials 0.000 description 2
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000010626 work up procedure Methods 0.000 description 2
- 241000272496 Galliformes Species 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- -1 bisulfates Chemical class 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-M bisulphate group Chemical group S([O-])(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-M 0.000 description 1
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 1
- 229940093915 gynecological organic acid Drugs 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- WBHQBSYUUJJSRZ-UHFFFAOYSA-M sodium bisulfate Chemical compound [Na+].OS([O-])(=O)=O WBHQBSYUUJJSRZ-UHFFFAOYSA-M 0.000 description 1
- 229910000342 sodium bisulfate Inorganic materials 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/29—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
- C07C45/298—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups with manganese derivatives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE197161C true DE197161C (enrdf_load_stackoverflow) |
Family
ID=460071
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT197161D Active DE197161C (enrdf_load_stackoverflow) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE197161C (enrdf_load_stackoverflow) |
-
0
- DE DENDAT197161D patent/DE197161C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE197161C (enrdf_load_stackoverflow) | ||
| DE2228804A1 (de) | Verfahren zur Herstellung von Den vaten der beta Phenylbrenztraubensaure | |
| DE620904C (de) | Verfahren zur Darstellung cyclischer ª‡-Cyanketimide und cyclischer ª‡-Cyanketone | |
| DE186526C (enrdf_load_stackoverflow) | ||
| DE117251C (enrdf_load_stackoverflow) | ||
| DE422948C (de) | Verfahren zur Darstellung von C-Benzyloxynaphthalinen | |
| DE2127898C3 (de) | Verfahren zur Herstellung von ge gebenenfalls inert substituierten o und p Aminothiophenolen | |
| DE269338C (enrdf_load_stackoverflow) | ||
| DE255772C (enrdf_load_stackoverflow) | ||
| DE119756C (enrdf_load_stackoverflow) | ||
| DE727051C (de) | Verfahren zur Darstellung monocyclischer Lactone mit 14í¬18 Ringgliedern | |
| DE1952375C3 (de) | Verfahren zur Herstellung von halogenierten Benzilsäurealkylestern | |
| DE175295C (enrdf_load_stackoverflow) | ||
| DE157590C (enrdf_load_stackoverflow) | ||
| DE444014C (de) | Verfahren zur Darstellung von Thiuramdisulfiden | |
| DE925584C (de) | Verfahren zur Herstellung sauerstoffreicher Verbindungen der Cyclopentanopolyhydrophenanthrenreihe | |
| DE37730C (de) | Verfahren zur Darstellung von Dialkylamidothiobenzoesäurechloriden resp. den entsprechenden Säuren und von Tetraalkyldiamidothioketonen aus Kohlenstoffsulfochlorid und tertiären aromatischen Aminen | |
| DE221849C (enrdf_load_stackoverflow) | ||
| DE106504C (enrdf_load_stackoverflow) | ||
| DE216269C (enrdf_load_stackoverflow) | ||
| DE180832C (enrdf_load_stackoverflow) | ||
| DE158717C (enrdf_load_stackoverflow) | ||
| DE202790C (enrdf_load_stackoverflow) | ||
| DE175423C (enrdf_load_stackoverflow) | ||
| DE1251734B (de) | Verfahren zur Herstellung von Monochloressigsaure |