DE195656C - - Google Patents

Info

Publication number

DE195656C

DE195656C DENDAT195656D DE195656DA DE195656C DE 195656 C DE195656 C DE 195656C DE NDAT195656 D DENDAT195656 D DE NDAT195656D DE 195656D A DE195656D A DE 195656DA DE 195656 C DE195656 C DE 195656C

Authority

DE

Germany

Prior art keywords

hydroxylamine

acetic acid

ethyl acetate

dioxyphenylglyoxime

water

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 18
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
• AVXURJPOCDRRFD-UHFFFAOYSA-N hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 claims description 6
• 238000006243 chemical reaction Methods 0.000 claims description 3
• 238000000034 method Methods 0.000 claims description 3
• 239000002253 acid Substances 0.000 claims description 2
• 150000002576 ketones Chemical class 0.000 claims description 2
• 238000002360 preparation method Methods 0.000 claims description 2
• 230000004048 modification Effects 0.000 claims 1
• 238000006011 modification reaction Methods 0.000 claims 1
• XEKOWRVHYACXOJ-UHFFFAOYSA-N acetic acid ethyl ester Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 18
• BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 2
• VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• UIIMBOGNXHQVGW-UHFFFAOYSA-M NaHCO3 Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
• RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
• PMZURENOXWZQFD-UHFFFAOYSA-L na2so4 Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
• 229910052938 sodium sulfate Inorganic materials 0.000 description 2
• 235000011152 sodium sulphate Nutrition 0.000 description 2
• BCDGQXUMWHRQCB-UHFFFAOYSA-N 1-Amino-2-propanone Chemical class CC(=O)CN BCDGQXUMWHRQCB-UHFFFAOYSA-N 0.000 description 1
• WTDHULULXKLSOZ-UHFFFAOYSA-N Hydroxylamine hydrochloride Chemical compound Cl.ON WTDHULULXKLSOZ-UHFFFAOYSA-N 0.000 description 1
• RUFIRPVAEJIIIS-OWOJBTEDSA-N N-[(E)-2-nitrosoethenyl]hydroxylamine Chemical compound ON\C=C\N=O RUFIRPVAEJIIIS-OWOJBTEDSA-N 0.000 description 1
• 150000007513 acids Chemical class 0.000 description 1
• 150000001412 amines Chemical class 0.000 description 1
• 239000003610 charcoal Substances 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 238000004140 cleaning Methods 0.000 description 1
• 150000001875 compounds Chemical class 0.000 description 1
• 238000001914 filtration Methods 0.000 description 1
• 150000002443 hydroxylamines Chemical class 0.000 description 1
• MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
• 229910052760 oxygen Inorganic materials 0.000 description 1
• 239000001301 oxygen Substances 0.000 description 1
• 239000003208 petroleum Substances 0.000 description 1
• 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
• 239000000047 product Substances 0.000 description 1
• 239000012261 resinous substance Substances 0.000 description 1
• 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
• 235000017557 sodium bicarbonate Nutrition 0.000 description 1
• CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
• 230000000576 supplementary Effects 0.000 description 1
• 238000010792 warming Methods 0.000 description 1