DE1948487A1 - Verfahren zur Herstellung von Viskosefasern mit neuartigen Faerbeeigenschaften - Google Patents
Verfahren zur Herstellung von Viskosefasern mit neuartigen FaerbeeigenschaftenInfo
- Publication number
- DE1948487A1 DE1948487A1 DE19691948487 DE1948487A DE1948487A1 DE 1948487 A1 DE1948487 A1 DE 1948487A1 DE 19691948487 DE19691948487 DE 19691948487 DE 1948487 A DE1948487 A DE 1948487A DE 1948487 A1 DE1948487 A1 DE 1948487A1
- Authority
- DE
- Germany
- Prior art keywords
- viscose
- components
- spinning mass
- dyes
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920000297 Rayon Polymers 0.000 title claims description 27
- 238000000034 method Methods 0.000 title claims description 21
- 239000000835 fiber Substances 0.000 title claims description 14
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 238000004040 coloring Methods 0.000 title description 5
- 239000000463 material Substances 0.000 claims description 16
- 229920002678 cellulose Polymers 0.000 claims description 15
- 239000001913 cellulose Substances 0.000 claims description 15
- 229920000768 polyamine Polymers 0.000 claims description 14
- 238000004043 dyeing Methods 0.000 claims description 10
- 238000009987 spinning Methods 0.000 claims description 10
- 239000007795 chemical reaction product Substances 0.000 claims description 8
- 150000001408 amides Chemical class 0.000 claims description 7
- 239000000654 additive Substances 0.000 claims description 6
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims description 6
- 239000003995 emulsifying agent Substances 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 5
- 238000001556 precipitation Methods 0.000 claims description 5
- 235000021122 unsaturated fatty acids Nutrition 0.000 claims description 5
- 150000004670 unsaturated fatty acids Chemical class 0.000 claims description 5
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims description 4
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 claims description 4
- 229920001281 polyalkylene Polymers 0.000 claims description 4
- 229920000642 polymer Polymers 0.000 claims description 4
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 claims description 3
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 230000000996 additive effect Effects 0.000 claims 1
- 239000002152 aqueous-organic solution Substances 0.000 claims 1
- 239000000975 dye Substances 0.000 description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 210000002268 wool Anatomy 0.000 description 10
- 238000002360 preparation method Methods 0.000 description 9
- 239000000203 mixture Substances 0.000 description 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 150000001412 amines Chemical class 0.000 description 6
- 235000014113 dietary fatty acids Nutrition 0.000 description 6
- 239000000194 fatty acid Substances 0.000 description 6
- 229930195729 fatty acid Natural products 0.000 description 6
- 150000004665 fatty acids Chemical class 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 5
- 239000004593 Epoxy Substances 0.000 description 5
- 229910052804 chromium Inorganic materials 0.000 description 5
- 239000011651 chromium Substances 0.000 description 5
- 239000000986 disperse dye Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 230000002378 acidificating effect Effects 0.000 description 4
- 239000004744 fabric Substances 0.000 description 4
- 239000002657 fibrous material Substances 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 229960000583 acetic acid Drugs 0.000 description 3
- 239000012736 aqueous medium Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000012362 glacial acetic acid Substances 0.000 description 3
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 3
- 229920000647 polyepoxide Polymers 0.000 description 3
- 229920000728 polyester Polymers 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- XINQFOMFQFGGCQ-UHFFFAOYSA-L (2-dodecoxy-2-oxoethyl)-[6-[(2-dodecoxy-2-oxoethyl)-dimethylazaniumyl]hexyl]-dimethylazanium;dichloride Chemical compound [Cl-].[Cl-].CCCCCCCCCCCCOC(=O)C[N+](C)(C)CCCCCC[N+](C)(C)CC(=O)OCCCCCCCCCCCC XINQFOMFQFGGCQ-UHFFFAOYSA-L 0.000 description 2
- 101000623895 Bos taurus Mucin-15 Proteins 0.000 description 2
- 229920003043 Cellulose fiber Polymers 0.000 description 2
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 2
- 239000004952 Polyamide Substances 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- 125000003277 amino group Chemical group 0.000 description 2
- 150000004700 cobalt complex Chemical class 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 125000003700 epoxy group Chemical group 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 235000020778 linoleic acid Nutrition 0.000 description 2
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 2
- -1 p-hydroxyphenyl Chemical group 0.000 description 2
- 229920002647 polyamide Polymers 0.000 description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 238000007127 saponification reaction Methods 0.000 description 2
- XKZQKPRCPNGNFR-UHFFFAOYSA-N 2-(3-hydroxyphenyl)phenol Chemical compound OC1=CC=CC(C=2C(=CC=CC=2)O)=C1 XKZQKPRCPNGNFR-UHFFFAOYSA-N 0.000 description 1
- KUBDPQJOLOUJRM-UHFFFAOYSA-N 2-(chloromethyl)oxirane;4-[2-(4-hydroxyphenyl)propan-2-yl]phenol Chemical compound ClCC1CO1.C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 KUBDPQJOLOUJRM-UHFFFAOYSA-N 0.000 description 1
- WFZFMHDDZRBTFH-CZEFNJPISA-N 2-[(e)-2-(5-carbamimidoyl-1-benzofuran-2-yl)ethenyl]-1-benzofuran-5-carboximidamide;dihydrochloride Chemical compound Cl.Cl.NC(=N)C1=CC=C2OC(/C=C/C=3OC4=CC=C(C=C4C=3)C(=N)N)=CC2=C1 WFZFMHDDZRBTFH-CZEFNJPISA-N 0.000 description 1
- 238000005698 Diels-Alder reaction Methods 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 150000004056 anthraquinones Chemical class 0.000 description 1
- CREMABGTGYGIQB-UHFFFAOYSA-N carbon carbon Chemical compound C.C CREMABGTGYGIQB-UHFFFAOYSA-N 0.000 description 1
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 239000000982 direct dye Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000006266 etherification reaction Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000006317 isomerization reaction Methods 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 150000004668 long chain fatty acids Chemical class 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000434 metal complex dye Substances 0.000 description 1
- 150000002763 monocarboxylic acids Chemical class 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 150000002924 oxiranes Chemical class 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- WBHHMMIMDMUBKC-XLNAKTSKSA-N ricinelaidic acid Chemical compound CCCCCC[C@@H](O)C\C=C\CCCCCCCC(O)=O WBHHMMIMDMUBKC-XLNAKTSKSA-N 0.000 description 1
- 229960003656 ricinoleic acid Drugs 0.000 description 1
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 229910052979 sodium sulfide Inorganic materials 0.000 description 1
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003784 tall oil Substances 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- DTOSIQBPPRVQHS-UHFFFAOYSA-N α-Linolenic acid Chemical compound CCC=CCC=CCC=CCCCCCCCC(O)=O DTOSIQBPPRVQHS-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/06—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from viscose
- D01F2/08—Composition of the spinning solution or the bath
- D01F2/10—Addition to the spinning solution or spinning bath of substances which exert their effect equally well in either
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Artificial Filaments (AREA)
- Coloring (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH1466068A CH508060A (de) | 1968-10-01 | 1968-10-01 | Verfahren zur Herstellung von modifizierten Viskosefasern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1948487A1 true DE1948487A1 (de) | 1970-04-09 |
Family
ID=4402775
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19691948487 Pending DE1948487A1 (de) | 1968-10-01 | 1969-09-25 | Verfahren zur Herstellung von Viskosefasern mit neuartigen Faerbeeigenschaften |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3793419A (enrdf_load_stackoverflow) |
| AT (1) | AT297910B (enrdf_load_stackoverflow) |
| BE (1) | BE739578A (enrdf_load_stackoverflow) |
| BR (1) | BR6912890D0 (enrdf_load_stackoverflow) |
| CH (1) | CH508060A (enrdf_load_stackoverflow) |
| DE (1) | DE1948487A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2019535A1 (enrdf_load_stackoverflow) |
| GB (1) | GB1258483A (enrdf_load_stackoverflow) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0665311A1 (de) * | 1994-01-29 | 1995-08-02 | Hoechst Aktiengesellschaft | Aminierte cellulosische Synthesefasern |
| EP0692559A1 (de) | 1994-06-30 | 1996-01-17 | Hoechst Aktiengesellschaft | Mit polymeren Aminverbindungen modifizierte synthetische cellulosische Fasern |
| EP0692558A1 (de) | 1994-06-30 | 1996-01-17 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von aminierten Fasern aus Regeneratcellulose |
| EP0703305A1 (de) | 1994-09-23 | 1996-03-27 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von aminierter Regeneratcellulose |
| EP0705924A2 (de) | 1994-10-04 | 1996-04-10 | Hoechst Aktiengesellschaft | Verfahren zum Färben von modifizierten Viskosefasern mit Säure- oder Direktfarbstoffen |
| US5565007A (en) * | 1994-05-17 | 1996-10-15 | Hoechst Aktiengesellschaft | Amination of rayon |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4767807A (en) * | 1985-08-21 | 1988-08-30 | Nippon Shokubai Kagaku Kogyo Co. Ltd. | Coloring agent for dope-dyeing viscose rayon |
-
1968
- 1968-10-01 CH CH1466068A patent/CH508060A/de not_active IP Right Cessation
-
1969
- 1969-09-03 FR FR6930083A patent/FR2019535A1/fr not_active Withdrawn
- 1969-09-16 GB GB1258483D patent/GB1258483A/en not_active Expired
- 1969-09-25 DE DE19691948487 patent/DE1948487A1/de active Pending
- 1969-09-30 BE BE739578D patent/BE739578A/xx unknown
- 1969-09-30 AT AT923769A patent/AT297910B/de not_active IP Right Cessation
- 1969-10-01 BR BR212890/69A patent/BR6912890D0/pt unknown
-
1972
- 1972-01-31 US US00222319A patent/US3793419A/en not_active Expired - Lifetime
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0665311A1 (de) * | 1994-01-29 | 1995-08-02 | Hoechst Aktiengesellschaft | Aminierte cellulosische Synthesefasern |
| US5565007A (en) * | 1994-05-17 | 1996-10-15 | Hoechst Aktiengesellschaft | Amination of rayon |
| EP0692559A1 (de) | 1994-06-30 | 1996-01-17 | Hoechst Aktiengesellschaft | Mit polymeren Aminverbindungen modifizierte synthetische cellulosische Fasern |
| EP0692558A1 (de) | 1994-06-30 | 1996-01-17 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von aminierten Fasern aus Regeneratcellulose |
| US5529585A (en) * | 1994-06-30 | 1996-06-25 | Hoechst Ag | Rayon modified with polymeric amine compounds |
| EP0703305A1 (de) | 1994-09-23 | 1996-03-27 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von aminierter Regeneratcellulose |
| EP0705924A2 (de) | 1994-10-04 | 1996-04-10 | Hoechst Aktiengesellschaft | Verfahren zum Färben von modifizierten Viskosefasern mit Säure- oder Direktfarbstoffen |
| US5542955A (en) * | 1994-10-04 | 1996-08-06 | Hoechst Aktiengesellschaft | Dyeing modified viscose fibers with acid or direct dyes |
Also Published As
| Publication number | Publication date |
|---|---|
| BR6912890D0 (pt) | 1973-01-16 |
| FR2019535A1 (enrdf_load_stackoverflow) | 1970-07-03 |
| US3793419A (en) | 1974-02-19 |
| BE739578A (enrdf_load_stackoverflow) | 1970-03-31 |
| GB1258483A (enrdf_load_stackoverflow) | 1971-12-30 |
| CH508060A (de) | 1971-05-31 |
| AT297910B (de) | 1972-04-10 |
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